Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO022118\ Data File : PO042513.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 20 Feb 2018 18:57 Sample : HEXANE Misc : ALS Vial : 1 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.062 3.024 3.105 BV 580350 7715580 1.11% 0.167% 2 3.133 3.105 3.138 PV 136444 1678948 0.24% 0.036% 3 3.144 3.138 3.155 VV 150314 1303581 0.19% 0.028% 4 3.175 3.155 3.192 VV 186303 3302685 0.48% 0.071% 5 3.228 3.192 3.244 VV 332162 7045557 1.02% 0.152% 6 3.267 3.244 3.299 VV 307123 7716081 1.11% 0.167% 7 3.375 3.299 3.403 VV 616516 25126420 3.63% 0.544% 8 3.444 3.403 3.487 VV 612921 25591041 3.69% 0.554% 9 3.525 3.487 3.582 VV 535429 24966629 3.60% 0.540% 10 3.615 3.582 3.664 VV 514898 20236977 2.92% 0.438% 11 3.688 3.664 3.716 VV 578289 14839825 2.14% 0.321% 12 3.765 3.716 3.799 VV 538923 22867835 3.30% 0.495% 13 3.843 3.826 3.873 VV 542455 13560306 1.96% 0.293% 14 3.919 3.894 3.955 VV 520998 15806904 2.28% 0.342% 15 3.991 3.955 4.041 VV 491392 19613790 2.83% 0.424% 16 4.066 4.041 4.089 VV 436973 9505276 1.37% 0.206% 17 4.138 4.089 4.187 VV 720176 23034497 3.32% 0.498% 18 4.204 4.187 4.248 VV 453669 13260362 1.91% 0.287% 19 4.273 4.248 4.301 VV 454507 11451755 1.65% 0.248% 20 4.336 4.301 4.368 VV 467334 14338346 2.07% 0.310% 21 4.404 4.368 4.433 VV 534577 16881233 2.44% 0.365% 22 4.474 4.433 4.514 VV 1003752 30281436 4.37% 0.655% 23 4.537 4.514 4.579 VV 639183 17995365 2.60% 0.389% 24 4.601 4.579 4.639 VV 499764 13711627 1.98% 0.297% 25 4.664 4.639 4.710 VV 503237 15799347 2.28% 0.342% 26 4.728 4.710 4.747 VV 395841 7836053 1.13% 0.170% 27 4.785 4.767 4.806 VV 415642 8286561 1.20% 0.179% 28 4.903 4.881 4.921 VV 311902 5082473 0.73% 0.110% 29 4.957 4.921 4.999 VV 357120 12540190 1.81% 0.271% 30 5.018 4.999 5.045 VV 474841 9889430 1.43% 0.214% 31 5.073 5.045 5.092 VV 485370 9940810 1.43% 0.215% 32 5.130 5.092 5.154 VV 532355 14404596 2.08% 0.312% 33 5.176 5.154 5.218 VV 2029051 32900901 4.75% 0.712% 34 5.237 5.218 5.251 VV 515570 8100967 1.17% 0.175% 35 5.264 5.251 5.278 VV 444944 6732591 0.97% 0.146% 36 5.290 5.278 5.322 VV 445691 10740794 1.55% 0.232% 37 5.350 5.322 5.386 VV 528205 16960111 2.45% 0.367% 38 5.412 5.386 5.421 VV 525856 10320871 1.49% 0.223% 39 5.456 5.421 5.487 VV 824885 25417280 3.67% 0.550% 40 5.511 5.487 5.538 VV 865257 23519425 3.39% 0.509% 41 5.574 5.538 5.598 VV 3653540 66138471 9.54% 1.431% 42 5.662 5.598 5.787 VV 4911986 174844315 25.23% 3.783% 43 5.814 5.787 5.819 PV 259557 3087917 0.45% 0.067% 44 5.839 5.819 5.864 VV 354604 8734939 1.26% 0.189% 45 5.884 5.864 5.895 VV 389346 6542338 0.94% 0.142% 46 5.919 5.895 5.934 VV 413058 9182664 1.33% 0.199% 47 5.952 5.934 5.968 VV 466140 8918241 1.29% 0.193% 48 5.971 5.968 5.981 VV 462039 3633094 0.52% 0.079% 49 5.999 5.981 6.014 VV 700752 9707886 1.40% 0.210% 50 6.060 6.014 6.159 VV 3799833 88871371 12.83% 1.923% 51 6.299 6.232 6.344 PV 324440 12662130 1.83% 0.274% 52 6.352 6.344 6.359 VV 90195 745317 0.11% 0.016% 53 6.363 6.359 6.399 VB 78222 1090832 0.16% 0.024% 54 6.522 6.498 6.565 VV 458744 17541303 2.53% 0.380% 55 6.630 6.565 6.665 VV 2907966 72759935 10.50% 1.574% 56 6.671 6.665 6.688 VV 1073793 14889655 2.15% 0.322% 57 6.720 6.688 6.739 VV 1309649 38789174 5.60% 0.839% 58 6.753 6.739 6.762 VV 1428491 19377021 2.80% 0.419% 59 6.788 6.762 6.807 VV 1595560 42187079 6.09% 0.913% 60 6.841 6.807 6.881 VV 1929295 68466785 9.88% 1.481% 61 6.913 6.881 6.933 PV 1976557 46662173 6.73% 1.010% 62 6.956 6.933 6.970 VV 1948440 43129428 6.22% 0.933% 63 6.993 6.970 6.999 VV 1926656 33768782 4.87% 0.731% 64 7.008 6.999 7.033 VV 1890398 37046491 5.35% 0.802% 65 7.065 7.033 7.098 VV 1854691 68744147 9.92% 1.487% 66 7.123 7.098 7.131 VV 1839907 34631053 5.00% 0.749% 67 7.169 7.131 7.204 VV 1845922 78913716 11.39% 1.708% 68 7.225 7.204 7.254 VV 1760069 50109014 7.23% 1.084% 69 7.287 7.254 7.329 VV 1787787 75225683 10.86% 1.628% 70 7.359 7.329 7.384 VV 1676830 52689972 7.60% 1.140% 71 7.601 7.384 7.676 VV 1497461 266161096 38.41% 5.759% 72 7.696 7.676 7.723 VV 1413688 38479825 5.55% 0.833% 73 7.787 7.723 7.861 VV 2110303 130621161 18.85% 2.826% 74 7.918 7.861 7.941 VV 1270280 57825510 8.34% 1.251% 75 8.001 7.941 8.068 VV 1310942 88322317 12.75% 1.911% 76 8.207 8.068 8.222 VV 1016756 94816575 13.68% 2.052% 77 8.277 8.222 8.307 VV 1090948 53085733 7.66% 1.149% 78 8.760 8.307 8.773 VV 1545683 359369572 51.86% 7.776% 79 9.489 8.773 9.519 VV 1523240 692942079 100.00% 14.994% 80 9.687 9.519 9.739 VV 1525533 196030863 28.29% 4.242% 81 9.745 9.739 9.804 VV 1408038 51556885 7.44% 1.116% 82 9.853 9.804 10.063 VV 1813687 161636875 23.33% 3.497% 83 10.872 10.063 10.882 VV 812618 363898124 52.51% 7.874% 84 10.901 10.882 10.914 VV 785663 14745323 2.13% 0.319% 85 11.307 10.914 11.318 VV 585989 162985758 23.52% 3.527% 86 11.646 11.318 11.654 VV 330621 87323863 12.60% 1.889% 87 11.700 11.654 11.729 VV 310110 12853747 1.85% 0.278% 88 11.808 11.729 11.901 VV 226079 18943389 2.73% 0.410% 89 11.909 11.901 11.984 VBA 107151 592202 0.09% 0.013% Sum of corrected areas: 4621586279 Signal #2 : ECD2B.CH 1 2.534 2.508 2.599 BV 557037 7913465 1.82% 0.081% 2 2.636 2.599 2.668 PV 172102 3160378 0.73% 0.032% 3 3.019 2.933 3.049 PV 190275 7091095 1.63% 0.073% 4 3.354 3.323 3.427 VV 260994 10061237 2.32% 0.103% 5 3.507 3.427 3.556 PV 605612 19778447 4.56% 0.202% 6 3.568 3.556 3.573 VV 251446 2416640 0.56% 0.025% 7 3.584 3.573 3.599 VV 257642 3787721 0.87% 0.039% 8 3.603 3.599 3.607 VV 260820 1032437 0.24% 0.011% 9 3.616 3.607 3.629 VV 228972 2744791 0.63% 0.028% 10 3.782 3.674 3.805 PV 502033 19310839 4.45% 0.198% 11 3.829 3.805 3.851 VV 214865 4734903 1.09% 0.048% 12 3.866 3.851 3.897 VV 170318 2932077 0.68% 0.030% 13 3.991 3.972 4.010 PB 76930 778718 0.18% 0.008% 14 4.133 4.090 4.165 PV 472481 15783178 3.64% 0.162% 15 4.233 4.165 4.238 VV 1032568 35494877 8.18% 0.363% 16 4.264 4.238 4.315 VV 3074419 79312840 18.27% 0.812% 17 4.342 4.315 4.362 VV 1583777 43540375 10.03% 0.446% 18 4.390 4.362 4.422 VV 1911672 67018048 15.44% 0.686% 19 4.450 4.422 4.508 VV 2160207 104215627 24.01% 1.067% 20 4.529 4.508 4.539 VV 2237284 38321229 8.83% 0.392% 21 4.573 4.539 4.587 VV 2736565 74919423 17.26% 0.767% 22 4.653 4.587 4.658 VV 3399431 132900846 30.62% 1.361% 23 4.692 4.658 4.715 VV 3712934 125087208 28.82% 1.281% 24 4.749 4.715 4.775 VV 4030246 111383851 25.66% 1.140% 25 4.839 4.775 4.863 PV 4536885 178765616 41.19% 1.830% 26 4.904 4.863 4.918 VV 8112780 195022289 44.93% 1.996% 27 4.935 4.918 5.052 VV 8662618 434042507 100.00% 4.443% 28 5.059 5.052 5.083 VV 4041893 72413889 16.68% 0.741% 29 5.088 5.083 5.096 VV 3960544 31385840 7.23% 0.321% 30 5.103 5.096 5.138 VV 3969328 97635939 22.49% 0.999% 31 5.171 5.138 5.233 VV 14316620 348354729 80.26% 3.566% 32 5.239 5.233 5.253 VV 3954672 45905586 10.58% 0.470% 33 5.271 5.253 5.286 VV 3982195 78310436 18.04% 0.802% 34 5.294 5.286 5.327 VV 3944534 90753434 20.91% 0.929% 35 5.449 5.327 5.503 VV 5070412 410125831 94.49% 4.198% 36 5.554 5.503 5.588 PV 3903242 157399072 36.26% 1.611% 37 5.639 5.588 5.665 VV 3953296 176514327 40.67% 1.807% 38 5.672 5.665 5.703 VV 3757790 82149181 18.93% 0.841% 39 5.728 5.703 5.743 VV 3478792 83351131 19.20% 0.853% 40 5.765 5.743 5.774 VV 3431294 62542540 14.41% 0.640% 41 5.807 5.774 5.838 VV 3452860 129957725 29.94% 1.330% 42 5.854 5.838 5.859 VV 3255481 41504400 9.56% 0.425% 43 5.881 5.859 5.933 VV 3207695 132877567 30.61% 1.360% 44 5.986 5.933 6.042 VV 6039766 221705320 51.08% 2.270% 45 6.059 6.042 6.081 VV 2742812 52427533 12.08% 0.537% 46 6.141 6.081 6.157 VV 2791858 113988911 26.26% 1.167% 47 6.180 6.157 6.184 VV 2818489 45041427 10.38% 0.461% 48 6.201 6.184 6.226 VV 2848676 69409132 15.99% 0.711% 49 6.261 6.226 6.266 VV 2691537 62863881 14.48% 0.644% 50 6.279 6.266 6.287 VV 2637000 33138036 7.63% 0.339% 51 6.307 6.287 6.320 VV 2695988 51647670 11.90% 0.529% 52 6.349 6.320 6.365 VV 2611651 70438186 16.23% 0.721% 53 6.370 6.365 6.391 VV 2519712 39315010 9.06% 0.402% 54 6.406 6.391 6.431 VV 2437130 56823400 13.09% 0.582% 55 6.465 6.431 6.487 VV 2356157 77930333 17.95% 0.798% 56 6.509 6.487 6.513 VV 2213655 34805391 8.02% 0.356% 57 6.517 6.513 6.522 VV 2185864 11946895 2.75% 0.122% 58 6.528 6.522 6.537 VV 2175821 18673725 4.30% 0.191% 59 6.569 6.555 6.576 VV 2125788 26254210 6.05% 0.269% 60 6.618 6.576 6.623 VV 2079165 57951535 13.35% 0.593% 61 6.637 6.623 6.651 VV 2067849 34839387 8.03% 0.357% 62 6.770 6.742 6.783 VV 1836907 44192362 10.18% 0.452% 63 6.803 6.783 6.811 VV 1770093 29950973 6.90% 0.307% 64 6.838 6.811 6.863 VV 1825434 54296187 12.51% 0.556% 65 6.873 6.863 6.883 VV 1673738 20281116 4.67% 0.208% 66 6.914 6.883 6.942 VV 1644780 57007952 13.13% 0.584% 67 7.026 6.942 7.057 VV 1599935 104404591 24.05% 1.069% 68 7.134 7.057 7.241 VV 2520981 192227265 44.29% 1.968% 69 7.282 7.241 7.296 VV 1226084 40481764 9.33% 0.414% 70 7.351 7.296 7.359 VV 1319002 47337664 10.91% 0.485% 71 7.377 7.359 7.413 VV 1400417 41148818 9.48% 0.421% 72 7.435 7.413 7.444 VV 1154604 21535222 4.96% 0.220% 73 7.527 7.444 7.541 VV 1228362 64885234 14.95% 0.664% 74 7.547 7.541 7.578 VV 1185133 25339381 5.84% 0.259% 75 7.591 7.578 7.602 VV 1117206 15563963 3.59% 0.159% 76 7.614 7.602 7.636 VV 1025399 20677751 4.76% 0.212% 77 7.773 7.636 7.792 VV 1187001 97666864 22.50% 1.000% 78 7.835 7.792 7.848 VV 1118355 36592533 8.43% 0.375% 79 7.857 7.848 7.873 VV 1076918 15620310 3.60% 0.160% 80 7.915 7.873 7.918 VV 1058515 26902393 6.20% 0.275% 81 7.928 7.918 7.936 VV 1070570 11718957 2.70% 0.120% 82 8.065 7.936 8.103 VV 1494751 129871875 29.92% 1.329% 83 8.140 8.103 8.159 VV 1471625 46256860 10.66% 0.474% 84 8.266 8.159 8.297 VV 1513300 114058897 26.28% 1.168% 85 8.631 8.297 8.645 VV 1892650 336349543 77.49% 3.443% 86 8.660 8.645 8.676 VV 1845851 34196041 7.88% 0.350% 87 8.775 8.676 8.828 VV 2707367 187288374 43.15% 1.917% 88 8.838 8.828 8.848 VV 2091732 24236458 5.58% 0.248% 89 8.853 8.848 8.863 VV 2045544 18208874 4.20% 0.186% 90 8.879 8.863 8.883 VV 2009287 24986319 5.76% 0.256% 91 8.896 8.883 8.900 VV 1963853 19173779 4.42% 0.196% 92 8.918 8.900 8.924 VV 2025864 29196811 6.73% 0.299% 93 8.991 8.924 8.995 VV 2069437 87728121 20.21% 0.898% 94 9.088 8.995 9.098 VV 2146975 128876650 29.69% 1.319% 95 9.115 9.098 9.121 VV 2125095 29545472 6.81% 0.302% 96 9.188 9.121 9.193 VV 2215078 92566128 21.33% 0.948% 97 9.288 9.193 9.296 VV 2253894 137661171 31.72% 1.409% 98 9.318 9.296 9.322 VV 2250808 34776157 8.01% 0.356% 99 9.441 9.322 9.449 VV 2371677 175481790 40.43% 1.796% 100 9.455 9.449 9.467 VV 2368745 25259317 5.82% 0.259% 101 9.606 9.467 9.623 VV 2333407 214800379 49.49% 2.199% 102 9.628 9.623 9.638 VV 2349531 20676963 4.76% 0.212% 103 9.669 9.638 9.682 VV 2342004 62216045 14.33% 0.637% 104 9.706 9.682 9.728 VV 2297076 61515007 14.17% 0.630% 105 9.744 9.728 9.750 VV 2220059 28854654 6.65% 0.295% 106 9.753 9.750 9.780 VV 2183090 39076266 9.00% 0.400% 107 9.883 9.780 9.891 VV 2187417 140720373 32.42% 1.441% 108 9.979 9.891 9.984 VV 2219094 120783627 27.83% 1.236% 109 9.992 9.984 10.018 VV 2229712 44358584 10.22% 0.454% 110 10.071 10.018 10.099 VV 2226321 106190981 24.47% 1.087% 111 10.121 10.099 10.130 VV 2162911 40667152 9.37% 0.416% 112 10.157 10.130 10.161 VV 2131943 39317829 9.06% 0.402% 113 10.168 10.161 10.182 VV 2148609 26194995 6.04% 0.268% 114 10.229 10.182 10.238 VV 2125030 70200012 16.17% 0.719% 115 10.241 10.238 10.246 VV 2104186 10356075 2.39% 0.106% 116 10.262 10.246 10.268 VV 2109417 26955225 6.21% 0.276% 117 10.282 10.268 10.288 VV 2128445 25206628 5.81% 0.258% 118 10.294 10.288 10.299 VV 2096486 13562325 3.12% 0.139% 119 10.306 10.299 10.311 VV 2083079 14725679 3.39% 0.151% 120 10.324 10.311 10.348 VV 2083009 46246673 10.65% 0.473% 121 10.390 10.348 10.409 VV 2027365 72356313 16.67% 0.741% 122 10.415 10.409 10.430 VV 1992445 24525412 5.65% 0.251% 123 10.433 10.430 10.441 VV 1932998 12655221 2.92% 0.130% 124 10.473 10.441 10.478 VV 1909529 42239241 9.73% 0.432% 125 10.501 10.478 10.524 VV 1932671 52364431 12.06% 0.536% 126 10.530 10.524 10.538 VV 1899896 15588368 3.59% 0.160% 127 10.564 10.538 10.574 VV 1892757 40668843 9.37% 0.416% 128 10.581 10.574 10.586 VV 1872522 13304171 3.07% 0.136% 129 10.609 10.586 10.619 VV 1849005 35958678 8.28% 0.368% 130 10.649 10.619 10.678 VV 1854274 63525851 14.64% 0.650% 131 10.684 10.678 10.711 VV 1753234 34607659 7.97% 0.354% 132 10.716 10.711 10.720 VV 1700452 8444561 1.95% 0.086% 133 10.731 10.720 10.737 VV 1666966 16384540 3.77% 0.168% 134 10.765 10.737 10.769 VV 1666768 32109392 7.40% 0.329% 135 10.779 10.769 10.784 VV 1641204 14329273 3.30% 0.147% 136 10.788 10.784 10.791 VV 1615952 6616490 1.52% 0.068% 137 10.797 10.791 10.805 VV 1642233 13542715 3.12% 0.139% 138 10.809 10.805 10.814 VV 1635646 8814520 2.03% 0.090% 139 10.819 10.814 10.845 VV 1623875 28402278 6.54% 0.291% 140 10.916 10.855 10.921 VV 1520803 56874405 13.10% 0.582% 141 10.929 10.921 10.935 VV 1510751 13002853 3.00% 0.133% 142 10.958 10.935 10.963 VV 1517008 24279557 5.59% 0.249% 143 10.971 10.963 10.993 VV 1507442 26163233 6.03% 0.268% 144 11.017 10.993 11.033 VV 1437633 34078448 7.85% 0.349% 145 11.047 11.033 11.055 VV 1398699 18084118 4.17% 0.185% 146 11.059 11.055 11.063 VV 1364328 6907136 1.59% 0.071% 147 11.084 11.063 11.094 VV 1360770 24788545 5.71% 0.254% 148 11.101 11.094 11.114 VV 1361153 15751105 3.63% 0.161% 149 11.118 11.114 11.124 VV 1325302 7770334 1.79% 0.080% 150 11.138 11.124 11.143 VV 1306624 14505596 3.34% 0.148% 151 11.148 11.143 11.153 VV 1287519 6985636 1.61% 0.072% 152 11.165 11.153 11.177 VV 1278091 18261117 4.21% 0.187% 153 11.197 11.177 11.227 VV 1272267 36717470 8.46% 0.376% 154 11.295 11.227 11.333 VV 1145146 71343029 16.44% 0.730% 155 11.346 11.333 11.361 VV 1063777 17526127 4.04% 0.179% 156 11.381 11.361 11.391 VV 1028215 17865800 4.12% 0.183% 157 11.418 11.391 11.430 VV 981567 22062349 5.08% 0.226% 158 11.595 11.430 11.628 VV 688767 90331189 20.81% 0.925% 159 11.690 11.628 11.698 VV 548431 23391744 5.39% 0.239% 160 11.856 11.698 11.891 VV 301212 41935415 9.66% 0.429% 161 11.906 11.891 11.955 VV 207282 5329732 1.23% 0.055% Sum of corrected areas: 9768500576