Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO022118\ Data File : PO042514.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 20 Feb 2018 19:12 Sample : I.BLK Misc : ALS Vial : 2 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.117 3.071 3.144 PV 124370 2297162 1.32% 0.167% 2 3.224 3.186 3.250 VV 385925 5129652 2.94% 0.373% 3 3.304 3.250 3.324 VV 182421 4794164 2.75% 0.349% 4 3.393 3.352 3.425 VV 247710 6939794 3.98% 0.505% 5 3.476 3.425 3.502 VV 365984 11927114 6.84% 0.868% 6 3.521 3.502 3.525 VV 341612 3967909 2.28% 0.289% 7 3.563 3.525 3.569 VV 538344 11679516 6.70% 0.850% 8 3.573 3.569 3.613 VV 522180 11730385 6.73% 0.853% 9 3.637 3.613 3.668 VV 506491 13654663 7.83% 0.993% 10 3.718 3.668 3.746 VV 467256 17654150 10.12% 1.284% 11 3.797 3.763 3.833 VV 502871 16427026 9.42% 1.195% 12 3.872 3.833 3.932 VV 546417 24431584 14.01% 1.777% 13 3.947 3.932 3.991 VV 417649 11230472 6.44% 0.817% 14 4.021 3.991 4.052 VV 401520 10855195 6.23% 0.790% 15 4.102 4.052 4.141 VV 15070573 174369641 100.00% 12.684% 16 4.158 4.141 4.207 VV 421601 12232745 7.02% 0.890% 17 4.228 4.207 4.248 VV 383118 7550071 4.33% 0.549% 18 4.296 4.248 4.320 VV 364385 11795322 6.76% 0.858% 19 4.365 4.320 4.380 VV 354666 10985402 6.30% 0.799% 20 4.395 4.380 4.407 VV 438808 6198066 3.55% 0.451% 21 4.427 4.407 4.464 VV 456047 12446995 7.14% 0.905% 22 4.493 4.464 4.512 VV 518448 12177731 6.98% 0.886% 23 4.532 4.512 4.543 VV 656108 10457504 6.00% 0.761% 24 4.553 4.543 4.604 VV 639879 17731994 10.17% 1.290% 25 4.625 4.604 4.662 VV 466034 12173528 6.98% 0.886% 26 4.683 4.662 4.721 VV 453213 11742039 6.73% 0.854% 27 4.743 4.721 4.781 VV 374499 10680389 6.13% 0.777% 28 4.803 4.781 4.825 VV 384944 7777598 4.46% 0.566% 29 4.860 4.825 4.907 VV 317902 10991725 6.30% 0.800% 30 4.928 4.907 4.937 VV 244132 3425649 1.96% 0.249% 31 4.976 4.946 5.007 VV 299342 9400025 5.39% 0.684% 32 5.035 5.007 5.054 VV 436652 9587621 5.50% 0.697% 33 5.069 5.054 5.077 VV 364995 4402873 2.53% 0.320% 34 5.091 5.077 5.120 VV 434166 8801811 5.05% 0.640% 35 5.173 5.120 5.193 VV 1051694 23097441 13.25% 1.680% 36 5.206 5.193 5.233 VV 507187 10442687 5.99% 0.760% 37 5.257 5.233 5.284 VV 492564 12512277 7.18% 0.910% 38 5.308 5.284 5.327 VV 464022 10345015 5.93% 0.753% 39 5.368 5.327 5.385 VV 480076 13982561 8.02% 1.017% 40 5.419 5.385 5.434 VV 503358 13202434 7.57% 0.960% 41 5.472 5.434 5.500 VV 712283 22622073 12.97% 1.646% 42 5.528 5.500 5.551 VV 791400 20633115 11.83% 1.501% 43 5.582 5.551 5.612 VV 1150553 34730786 19.92% 2.526% 44 5.679 5.612 5.798 VV 4057018 149528001 85.75% 10.877% 45 5.848 5.798 5.875 PV 364664 12658332 7.26% 0.921% 46 5.898 5.875 5.901 VV 348425 5177295 2.97% 0.377% 47 5.924 5.901 5.940 VV 376179 8132178 4.66% 0.592% 48 5.976 5.940 5.997 VV 435888 13232234 7.59% 0.963% 49 6.012 5.997 6.027 VV 406979 6929386 3.97% 0.504% 50 6.071 6.027 6.190 VV 1324706 59525493 34.14% 4.330% 51 6.310 6.238 6.369 PV 291408 11306641 6.48% 0.822% 52 6.372 6.369 6.401 VB 59307 657782 0.38% 0.048% 53 6.628 6.559 6.662 PV 127772 2628930 1.51% 0.191% 54 6.840 6.811 6.846 PV 145744 1829534 1.05% 0.133% 55 6.849 6.846 6.879 VV 133892 1228127 0.70% 0.089% 56 7.068 7.038 7.098 VV 243801 5557978 3.19% 0.404% 57 7.126 7.098 7.131 PV 313426 4032926 2.31% 0.293% 58 7.172 7.131 7.179 VV 332723 9023291 5.17% 0.656% 59 7.185 7.179 7.213 VV 324936 6439924 3.69% 0.468% 60 7.235 7.213 7.244 VV 302829 5280972 3.03% 0.384% 61 7.248 7.244 7.252 VV 296322 1427155 0.82% 0.104% 62 7.284 7.252 7.309 VV 362203 10727614 6.15% 0.780% 63 7.326 7.309 7.329 VV 296797 3537111 2.03% 0.257% 64 7.342 7.329 7.347 VV 288759 3096249 1.78% 0.225% 65 7.360 7.347 7.379 VV 286311 5134284 2.94% 0.373% 66 7.404 7.379 7.409 VV 242920 4229726 2.43% 0.308% 67 7.439 7.409 7.444 VV 230731 4688428 2.69% 0.341% 68 7.476 7.444 7.484 VV 219646 5177263 2.97% 0.377% 69 7.584 7.484 7.588 VV 214019 12496833 7.17% 0.909% 70 7.615 7.588 7.626 VV 199789 4449626 2.55% 0.324% 71 7.737 7.626 7.747 VV 207162 13874776 7.96% 1.009% 72 7.750 7.747 7.754 VV 204196 814890 0.47% 0.059% 73 7.759 7.754 7.765 VV 187602 1233082 0.71% 0.090% 74 7.778 7.765 7.794 VV 183535 2900476 1.66% 0.211% 75 7.944 7.794 7.949 VV 173230 12582245 7.22% 0.915% 76 7.999 7.949 8.033 VV 295449 9497370 5.45% 0.691% 77 8.052 8.033 8.089 VV 111336 2778052 1.59% 0.202% 78 8.113 8.089 8.119 VV 50661 787500 0.45% 0.057% 79 8.133 8.119 8.149 VV 32636 310469 0.18% 0.023% 80 8.473 8.390 8.495 PV 70549 1731227 0.99% 0.126% 81 8.574 8.538 8.589 PV 42589 478952 0.27% 0.035% 82 8.715 8.598 8.721 VV 57995 2831779 1.62% 0.206% 83 8.726 8.721 8.740 VV 62849 540139 0.31% 0.039% 84 8.757 8.740 8.775 VV 45030 603705 0.35% 0.044% 85 8.786 8.775 8.802 PV 38906 205857 0.12% 0.015% 86 8.849 8.802 8.854 VV 43825 735084 0.42% 0.053% 87 8.991 8.854 8.995 VV 104770 4942151 2.83% 0.360% 88 9.027 8.995 9.039 VV 103027 2278140 1.31% 0.166% 89 9.044 9.039 9.047 VV 62487 278769 0.16% 0.020% 90 9.050 9.047 9.057 VV 63711 273776 0.16% 0.020% 91 9.105 9.079 9.119 PV 52852 802443 0.46% 0.058% 92 9.159 9.119 9.167 VV 62220 958421 0.55% 0.070% 93 9.265 9.167 9.274 VV 143168 7632914 4.38% 0.555% 94 9.279 9.274 9.284 VV 135512 732644 0.42% 0.053% 95 9.294 9.284 9.299 VV 110308 952948 0.55% 0.069% 96 9.307 9.299 9.326 VV 94262 1312627 0.75% 0.095% 97 9.485 9.341 9.529 VV 8847747 164836875 94.53% 11.991% 98 9.614 9.529 9.632 VV 210313 11771759 6.75% 0.856% 99 9.650 9.632 9.660 VV 214894 3197537 1.83% 0.233% 100 9.672 9.660 9.677 VV 203101 1900940 1.09% 0.138% 101 9.731 9.677 9.743 VV 164986 6169399 3.54% 0.449% 102 9.765 9.743 9.771 VV 184102 2788580 1.60% 0.203% 103 9.815 9.771 9.820 VV 185845 5094937 2.92% 0.371% 104 9.863 9.820 9.894 VV 180765 7155907 4.10% 0.521% 105 9.981 9.894 9.990 VV 151599 7483510 4.29% 0.544% 106 10.034 9.990 10.038 VV 152487 3713101 2.13% 0.270% 107 10.062 10.038 10.084 VV 142155 3357069 1.93% 0.244% 108 10.091 10.084 10.102 VV 116722 1141708 0.65% 0.083% 109 10.158 10.102 10.162 VV 147991 4546696 2.61% 0.331% 110 10.190 10.162 10.198 VV 141352 2746628 1.58% 0.200% 111 10.230 10.198 10.247 VV 143992 3997847 2.29% 0.291% 112 10.300 10.247 10.306 VV 119093 4004626 2.30% 0.291% 113 10.313 10.306 10.323 VV 121753 1031919 0.59% 0.075% 114 10.329 10.323 10.363 VV 100583 1764646 1.01% 0.128% 115 10.408 10.363 10.415 VV 92259 2282170 1.31% 0.166% 116 10.424 10.415 10.429 VV 82752 621928 0.36% 0.045% 117 10.444 10.429 10.449 VV 86649 822253 0.47% 0.060% 118 10.582 10.449 10.592 VV 109314 6211946 3.56% 0.452% 119 10.612 10.592 10.637 VV 96997 2312247 1.33% 0.168% 120 10.659 10.637 10.673 VV 87300 1506433 0.86% 0.110% 121 10.677 10.673 10.694 VV 73856 816447 0.47% 0.059% 122 10.708 10.694 10.716 VV 70532 856304 0.49% 0.062% 123 10.726 10.716 10.737 VV 91181 760089 0.44% 0.055% 124 10.741 10.737 10.747 VV 77489 380039 0.22% 0.028% 125 10.807 10.764 10.817 VV 94127 2261081 1.30% 0.164% 126 10.835 10.817 10.849 VV 79863 1359478 0.78% 0.099% 127 10.872 10.849 10.882 VV 100455 1521179 0.87% 0.111% 128 10.943 10.882 10.951 VV 72820 2548610 1.46% 0.185% 129 10.988 10.951 10.996 VV 70058 1423881 0.82% 0.104% 130 11.013 10.996 11.034 VV 51222 868071 0.50% 0.063% 131 11.046 11.034 11.051 VV 34251 285678 0.16% 0.021% 132 11.073 11.051 11.102 VV 60832 699926 0.40% 0.051% 133 11.314 11.232 11.322 VV 31856 1058724 0.61% 0.077% Sum of corrected areas: 1374719819 Signal #2 : ECD2B.CH 1 3.348 3.314 3.423 PV 18742281 235637208 33.64% 5.924% 2 3.633 3.612 3.667 VV 308309 5711001 0.82% 0.144% 3 3.795 3.740 3.811 PV 214746 5803122 0.83% 0.146% 4 3.862 3.811 3.903 VV 400103 14525294 2.07% 0.365% 5 3.909 3.903 3.925 VV 132429 1351898 0.19% 0.034% 6 3.934 3.925 3.937 VV 92985 570904 0.08% 0.014% 7 3.943 3.937 3.962 VV 83995 740532 0.11% 0.019% 8 4.264 4.231 4.339 VV 1146817 32533695 4.64% 0.818% 9 4.395 4.359 4.407 VV 567606 14354599 2.05% 0.361% 10 4.683 4.532 4.694 PV 845187 64686719 9.23% 1.626% 11 4.714 4.694 4.718 VV 826874 12088739 1.73% 0.304% 12 4.724 4.718 4.741 VV 826557 10844605 1.55% 0.273% 13 4.744 4.741 4.747 VV 800685 3076683 0.44% 0.077% 14 4.850 4.747 4.855 VV 1132419 62682902 8.95% 1.576% 15 4.955 4.855 5.077 VV 4494511 207278463 29.59% 5.211% 16 5.082 5.077 5.117 VV 539126 11433889 1.63% 0.287% 17 5.227 5.156 5.235 VV 361622 15162505 2.16% 0.381% 18 5.277 5.235 5.300 VV 376377 13526609 1.93% 0.340% 19 5.346 5.300 5.350 VV 370234 10122780 1.45% 0.254% 20 5.364 5.350 5.383 VV 391899 6928403 0.99% 0.174% 21 5.385 5.383 5.389 VV 334690 1182076 0.17% 0.030% 22 5.464 5.389 5.580 VV 1182517 56001486 7.99% 1.408% 23 5.598 5.580 5.614 VV 239805 4474195 0.64% 0.112% 24 5.643 5.614 5.772 VB 337485 16178166 2.31% 0.407% 25 5.985 5.939 6.006 PV 852016 22657609 3.23% 0.570% 26 6.059 6.006 6.070 VV 658463 25569660 3.65% 0.643% 27 6.111 6.070 6.117 VV 597943 16882560 2.41% 0.424% 28 6.131 6.117 6.136 VV 581099 6386661 0.91% 0.161% 29 6.139 6.136 6.154 VV 570212 6083962 0.87% 0.153% 30 6.159 6.154 6.162 VV 528918 2422517 0.35% 0.061% 31 6.198 6.162 6.225 VV 592383 20556353 2.93% 0.517% 32 6.270 6.225 6.286 VV 397100 14666490 2.09% 0.369% 33 6.306 6.286 6.315 VV 341234 5792835 0.83% 0.146% 34 6.354 6.315 6.375 VV 288477 10138935 1.45% 0.255% 35 6.394 6.375 6.422 VV 223524 5635203 0.80% 0.142% 36 6.428 6.422 6.432 VV 139547 745236 0.11% 0.019% 37 6.454 6.432 6.483 VV 181028 3918717 0.56% 0.099% 38 6.503 6.495 6.510 VV 52636 225517 0.03% 0.006% 39 6.754 6.701 6.759 PV 36563 1077004 0.15% 0.027% 40 6.767 6.759 6.776 VV 52232 290250 0.04% 0.007% 41 6.819 6.776 6.825 PV 60065 963284 0.14% 0.024% 42 6.831 6.825 6.865 VB 50541 596480 0.09% 0.015% 43 7.025 6.949 7.034 PV 82057 1981343 0.28% 0.050% 44 7.037 7.034 7.060 VV 64425 503419 0.07% 0.013% 45 7.170 7.060 7.179 PV 69712 1221307 0.17% 0.031% 46 7.183 7.179 7.187 VV 66617 248590 0.04% 0.006% 47 7.239 7.187 7.253 VV 58068 1824322 0.26% 0.046% 48 7.373 7.253 7.411 VV 225221 6766317 0.97% 0.170% 49 7.463 7.411 7.470 PV 104138 1353958 0.19% 0.034% 50 7.585 7.470 7.620 VV 102589 7981308 1.14% 0.201% 51 7.761 7.620 7.792 PV 196395 11592456 1.65% 0.291% 52 7.926 7.792 7.954 PV 433746 18297661 2.61% 0.460% 53 8.137 7.954 8.191 VV 18417828 278513651 39.76% 7.002% 54 8.779 8.191 8.787 VV 1255470 281195326 40.14% 7.069% 55 9.449 8.787 9.459 VV 1683224 593645082 84.74% 14.924% 56 9.537 9.459 9.549 VV 1738477 90919538 12.98% 2.286% 57 9.689 9.549 9.699 VV 1778467 155089119 22.14% 3.899% 58 9.730 9.699 9.761 VV 1735443 62958251 8.99% 1.583% 59 10.441 9.761 10.452 VV 1612900 700525833 100.00% 17.611% 60 10.486 10.452 10.507 VV 1567718 51227960 7.31% 1.288% 61 10.646 10.507 10.662 VV 1463902 137572668 19.64% 3.459% 62 10.683 10.662 10.695 VV 1415655 27949381 3.99% 0.703% 63 10.816 10.695 10.847 VV 1305739 118141644 16.86% 2.970% 64 10.891 10.847 10.900 VV 1259156 39360719 5.62% 0.990% 65 10.926 10.900 10.936 VV 1230890 26028498 3.72% 0.654% 66 11.014 10.936 11.030 VV 1170846 64948929 9.27% 1.633% 67 11.256 11.030 11.307 VV 987871 165813313 23.67% 4.169% 68 11.452 11.307 11.468 VV 726405 74062991 10.57% 1.862% 69 11.492 11.468 11.515 VV 672395 17984534 2.57% 0.452% 70 11.582 11.515 11.591 VV 551706 26150043 3.73% 0.657% 71 11.683 11.591 11.695 VV 422377 28380145 4.05% 0.713% 72 11.711 11.695 11.728 VV 396280 7158808 1.02% 0.180% 73 11.739 11.728 11.774 VV 342067 8452644 1.21% 0.213% 74 11.782 11.774 11.789 VV 306009 2566840 0.37% 0.065% 75 11.907 11.789 11.958 VV 140299 15782349 2.25% 0.397% Sum of corrected areas: 3977704694