Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO022118\ Data File : PO042515.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 20 Feb 2018 19:27 Sample : AR1660ICC1000 Misc : ALS Vial : 3 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.162 3.143 3.184 VV 361712 4041748 0.39% 0.030% 2 3.224 3.208 3.256 VV 258429 3139524 0.30% 0.024% 3 3.300 3.267 3.324 VV 218202 3955745 0.38% 0.030% 4 3.394 3.361 3.423 VV 232133 5138313 0.50% 0.039% 5 3.482 3.423 3.509 VV 286988 9655389 0.94% 0.073% 6 3.559 3.509 3.570 VV 456975 11748292 1.14% 0.088% 7 3.587 3.570 3.624 VV 515379 13697215 1.33% 0.103% 8 3.633 3.624 3.651 VV 385672 5314534 0.52% 0.040% 9 3.715 3.690 3.758 VV 391604 13373526 1.30% 0.101% 10 3.797 3.758 3.830 VV 407359 14446105 1.40% 0.109% 11 3.875 3.830 3.922 VV 446747 19111261 1.85% 0.144% 12 4.022 3.995 4.054 VV 298082 7407258 0.72% 0.056% 13 4.102 4.054 4.209 VV 74853361 824140467 79.87% 6.196% 14 4.231 4.209 4.268 VV 284477 7497192 0.73% 0.056% 15 4.299 4.268 4.335 VV 2144204 35851933 3.47% 0.270% 16 4.387 4.335 4.430 VV 3357274 52872018 5.12% 0.397% 17 4.459 4.430 4.520 VV 14011142 170587542 16.53% 1.282% 18 4.547 4.520 4.578 VV 543686 15454708 1.50% 0.116% 19 4.605 4.578 4.667 VV 2126368 34837440 3.38% 0.262% 20 4.682 4.667 4.723 VV 280448 7161806 0.69% 0.054% 21 4.784 4.754 4.799 VV 19168655 208273294 20.19% 1.566% 22 4.812 4.799 4.849 VV 10783076 125258751 12.14% 0.942% 23 4.869 4.849 4.886 VV 2417807 28366116 2.75% 0.213% 24 4.897 4.886 4.907 VV 1031901 10276852 1.00% 0.077% 25 4.920 4.907 4.943 VV 1593756 19461010 1.89% 0.146% 26 4.969 4.943 5.004 VV 18820394 212959549 20.64% 1.601% 27 5.040 5.026 5.054 VV 360351 5192703 0.50% 0.039% 28 5.079 5.054 5.110 VV 841843 16143271 1.56% 0.121% 29 5.133 5.110 5.147 VV 5437360 62111587 6.02% 0.467% 30 5.160 5.147 5.196 VV 3884368 51287415 4.97% 0.386% 31 5.228 5.196 5.237 VV 29290853 307753434 29.83% 2.314% 32 5.249 5.237 5.285 VV 38034247 466031726 45.17% 3.504% 33 5.310 5.285 5.359 VV 22595586 286385791 27.76% 2.153% 34 5.405 5.375 5.447 VV 19861503 244316379 23.68% 1.837% 35 5.468 5.447 5.475 VV 2172654 23389080 2.27% 0.176% 36 5.495 5.475 5.517 VV 14521281 176254440 17.08% 1.325% 37 5.538 5.517 5.564 VV 12496829 204400019 19.81% 1.537% 38 5.574 5.564 5.614 VV 7017748 92956286 9.01% 0.699% 39 5.691 5.614 5.715 VV 19080560 305932519 29.65% 2.300% 40 5.730 5.715 5.754 VV 8194580 107633319 10.43% 0.809% 41 5.775 5.754 5.797 VV 6359928 74884843 7.26% 0.563% 42 5.827 5.797 5.868 VV 15390263 238701775 23.13% 1.795% 43 5.892 5.868 5.920 VV 5120125 64963242 6.30% 0.488% 44 5.947 5.920 5.979 VV 937229 18613108 1.80% 0.140% 45 6.007 5.979 6.028 VV 1143712 19063004 1.85% 0.143% 46 6.057 6.028 6.074 VV 16158589 208192182 20.18% 1.565% 47 6.083 6.074 6.103 VV 7933356 91597757 8.88% 0.689% 48 6.120 6.103 6.181 VV 5515281 80435133 7.80% 0.605% 49 6.208 6.181 6.237 VV 1976499 25671048 2.49% 0.193% 50 6.271 6.237 6.297 PV 14350448 174892531 16.95% 1.315% 51 6.310 6.297 6.394 VV 909510 19906186 1.93% 0.150% 52 6.473 6.439 6.519 VV 544297 9107334 0.88% 0.068% 53 6.543 6.519 6.555 VV 2602837 29123004 2.82% 0.219% 54 6.572 6.555 6.602 VV 6066859 74511265 7.22% 0.560% 55 6.628 6.602 6.658 VV 7172296 87003764 8.43% 0.654% 56 6.686 6.658 6.723 VV 18363376 282464149 27.38% 2.124% 57 6.738 6.723 6.761 VV 4847527 57904871 5.61% 0.435% 58 6.790 6.761 6.829 VV 35071262 413525766 40.08% 3.109% 59 6.906 6.875 6.936 PV 4950043 59640879 5.78% 0.448% 60 6.973 6.936 7.006 VV 6784653 81739008 7.92% 0.615% 61 7.041 7.006 7.063 VV 47431408 549155275 53.22% 4.128% 62 7.081 7.063 7.102 VV 12065625 145272831 14.08% 1.092% 63 7.122 7.102 7.143 VV 10199942 119995803 11.63% 0.902% 64 7.166 7.143 7.186 VV 19878603 237915538 23.06% 1.789% 65 7.197 7.186 7.234 VV 3926891 46905999 4.55% 0.353% 66 7.271 7.234 7.287 VV 3931378 62442767 6.05% 0.469% 67 7.316 7.287 7.339 VV 46252406 633211597 61.37% 4.760% 68 7.347 7.339 7.369 VV 6433409 81110932 7.86% 0.610% 69 7.394 7.369 7.424 VV 37057425 445942064 43.22% 3.353% 70 7.451 7.424 7.504 VV 18614664 225663408 21.87% 1.697% 71 7.544 7.504 7.552 PV 82665 902343 0.09% 0.007% 72 7.580 7.552 7.591 VV 6871290 80910129 7.84% 0.608% 73 7.615 7.591 7.662 VV 31486948 445142400 43.14% 3.347% 74 7.692 7.662 7.725 VV 16450063 221805935 21.50% 1.668% 75 7.743 7.725 7.775 VV 8022359 101010037 9.79% 0.759% 76 7.801 7.775 7.819 PV 1500072 17842732 1.73% 0.134% 77 7.845 7.819 7.875 VV 9489873 120065119 11.64% 0.903% 78 7.915 7.875 7.945 VV 86071159 1031804019 100.00% 7.757% 79 7.962 7.945 7.991 VV 4357865 53701502 5.20% 0.404% 80 8.201 8.150 8.228 BV 37343596 619885370 60.08% 4.660% 81 8.254 8.228 8.265 VV 14826769 222560835 21.57% 1.673% 82 8.271 8.265 8.317 VV 14122227 161708960 15.67% 1.216% 83 8.472 8.367 8.517 PV 1122713 16481259 1.60% 0.124% 84 8.552 8.517 8.581 PV 1171120 24830428 2.41% 0.187% 85 8.607 8.581 8.655 VV 8140225 115502326 11.19% 0.868% 86 8.842 8.791 8.890 PV 19293007 287166668 27.83% 2.159% 87 8.920 8.890 8.955 VV 1051021 17176878 1.66% 0.129% 88 8.962 8.955 8.967 VV 105109 615137 0.06% 0.005% 89 9.022 8.967 9.032 VV 77971 2919289 0.28% 0.022% 90 9.052 9.032 9.059 VV 77646 1054786 0.10% 0.008% 91 9.104 9.059 9.112 VV 72468 2050291 0.20% 0.015% 92 9.151 9.112 9.155 VV 76170 1717734 0.17% 0.013% 93 9.199 9.155 9.254 VV 4709873 75795603 7.35% 0.570% 94 9.287 9.254 9.293 VV 90386 1910065 0.19% 0.014% 95 9.406 9.293 9.418 VV 101383 5834883 0.57% 0.044% 96 9.426 9.418 9.430 VV 94980 638169 0.06% 0.005% 97 9.486 9.430 9.570 VV 43988312 761972391 73.85% 5.728% 98 9.579 9.570 9.585 VV 144844 1105632 0.11% 0.008% 99 9.605 9.585 9.614 VV 132465 2072257 0.20% 0.016% 100 9.649 9.614 9.654 VV 115939 2447045 0.24% 0.018% 101 9.680 9.654 9.690 VV 134361 2593585 0.25% 0.019% 102 9.697 9.690 9.722 VV 111616 1852886 0.18% 0.014% 103 9.747 9.722 9.769 VV 102743 2383164 0.23% 0.018% 104 9.829 9.769 9.835 VV 109798 3630023 0.35% 0.027% 105 9.923 9.835 9.937 VV 97883 5397651 0.52% 0.041% 106 9.951 9.937 9.955 VV 107304 902947 0.09% 0.007% 107 9.968 9.955 9.976 VV 98357 959709 0.09% 0.007% 108 10.013 10.001 10.035 VV 86954 1422168 0.14% 0.011% 109 10.079 10.070 10.092 VV 84084 823583 0.08% 0.006% 110 10.258 10.092 10.267 VV 82028 6618815 0.64% 0.050% 111 10.274 10.267 10.283 VV 61427 437262 0.04% 0.003% 112 10.288 10.283 10.309 VV 43642 490792 0.05% 0.004% 113 10.317 10.309 10.335 VV 54137 494887 0.05% 0.004% 114 10.339 10.335 10.343 VV 54773 122424 0.01% 0.001% 115 11.294 11.186 11.300 PV 31984 1125416 0.11% 0.008% 116 11.333 11.300 11.345 VV 34625 370864 0.04% 0.003% Sum of corrected areas: 13301629017 Signal #2 : ECD2B.CH 1 2.540 2.515 2.592 BV 432114 7153274 0.34% 0.029% 2 2.681 2.658 2.706 VV 323888 6740444 0.32% 0.027% 3 2.746 2.725 2.807 VV 301706 11919992 0.57% 0.048% 4 2.875 2.840 2.899 PV 211858 5702823 0.27% 0.023% 5 2.904 2.899 2.928 VV 159616 2267354 0.11% 0.009% 6 2.951 2.928 2.975 VV 226017 4086101 0.20% 0.017% 7 3.001 2.975 3.040 VV 105618 2499118 0.12% 0.010% 8 3.348 3.318 3.481 PV 95326496 1211665655 57.95% 4.912% 9 3.498 3.481 3.525 VV 203238 4832726 0.23% 0.020% 10 3.552 3.525 3.605 VV 3298085 47612189 2.28% 0.193% 11 3.635 3.605 3.677 VV 4772783 63313226 3.03% 0.257% 12 3.706 3.677 3.755 VV 18044061 226927489 10.85% 0.920% 13 3.795 3.755 3.822 VV 521475 14960617 0.72% 0.061% 14 3.862 3.822 3.962 VV 2806456 61111357 2.92% 0.248% 15 3.989 3.962 4.043 VV 25176983 480632727 22.99% 1.949% 16 4.064 4.043 4.084 VV 3282759 46315265 2.22% 0.188% 17 4.097 4.084 4.115 VV 1598929 21267895 1.02% 0.086% 18 4.132 4.115 4.145 VV 2478940 30178004 1.44% 0.122% 19 4.170 4.145 4.206 VV 22661253 332809469 15.92% 1.349% 20 4.216 4.206 4.246 VV 1279886 21175630 1.01% 0.086% 21 4.282 4.246 4.296 VV 8501749 109702327 5.25% 0.445% 22 4.306 4.296 4.352 VV 5733774 79380164 3.80% 0.322% 23 4.396 4.352 4.432 VV 57214725 1142369066 54.64% 4.631% 24 4.451 4.432 4.533 VV 28917186 457117343 21.86% 1.853% 25 4.565 4.533 4.589 PV 27529049 340845476 16.30% 1.382% 26 4.607 4.589 4.627 VV 21338606 265065749 12.68% 1.075% 27 4.646 4.627 4.664 VV 24334242 326756902 15.63% 1.325% 28 4.674 4.664 4.740 VV 9735720 144530421 6.91% 0.586% 29 4.810 4.770 4.833 VV 26651860 363374720 17.38% 1.473% 30 4.847 4.833 4.864 VV 11650096 148377614 7.10% 0.602% 31 4.879 4.864 4.908 VV 9895612 139409017 6.67% 0.565% 32 4.952 4.908 4.989 VV 25909651 465903685 22.28% 1.889% 33 5.020 4.989 5.054 VV 7577262 128622340 6.15% 0.521% 34 5.080 5.054 5.094 VV 1617683 28076430 1.34% 0.114% 35 5.115 5.094 5.128 VV 6950236 85233890 4.08% 0.346% 36 5.148 5.128 5.172 VV 27535549 349763614 16.73% 1.418% 37 5.187 5.172 5.208 VV 7192561 93898605 4.49% 0.381% 38 5.216 5.208 5.222 VV 1763817 14552523 0.70% 0.059% 39 5.237 5.222 5.265 VV 3067819 44387865 2.12% 0.180% 40 5.291 5.265 5.327 VV 20423840 262530271 12.56% 1.064% 41 5.354 5.327 5.362 VV 1569613 23626657 1.13% 0.096% 42 5.375 5.362 5.425 VV 2135562 44738749 2.14% 0.181% 43 5.466 5.425 5.490 VV 996987 24589564 1.18% 0.100% 44 5.510 5.490 5.565 VV 1040116 21432536 1.03% 0.087% 45 5.593 5.565 5.627 VV 4110971 54888825 2.63% 0.223% 46 5.657 5.627 5.666 VV 9560875 108002954 5.17% 0.438% 47 5.692 5.666 5.714 VV 33517057 515311328 24.65% 2.089% 48 5.732 5.714 5.773 VV 11221823 214137027 10.24% 0.868% 49 5.804 5.773 5.848 VV 57131041 732579950 35.04% 2.970% 50 5.864 5.848 5.882 VV 1125827 15880756 0.76% 0.064% 51 5.903 5.882 5.914 VV 4148876 46525942 2.23% 0.189% 52 5.932 5.914 5.962 VV 11421361 152797285 7.31% 0.619% 53 5.991 5.962 6.073 VV 80758226 1024221579 48.99% 4.152% 54 6.136 6.103 6.185 VV 67998950 873290631 41.77% 3.540% 55 6.209 6.185 6.232 VV 7072260 92301262 4.41% 0.374% 56 6.255 6.232 6.279 VV 19188770 244931164 11.71% 0.993% 57 6.307 6.279 6.326 VV 73864089 1044784368 49.97% 4.236% 58 6.343 6.326 6.375 VV 68236406 946054419 45.25% 3.835% 59 6.396 6.375 6.468 VV 33321677 444465721 21.26% 1.802% 60 6.532 6.500 6.566 VV 11972087 174147136 8.33% 0.706% 61 6.595 6.566 6.621 VV 55373766 724159476 34.64% 2.936% 62 6.631 6.621 6.654 VV 6290088 78186444 3.74% 0.317% 63 6.689 6.654 6.716 VV 28760261 409059918 19.57% 1.658% 64 6.736 6.716 6.752 VV 14347298 182445267 8.73% 0.740% 65 6.765 6.752 6.797 VV 11705992 173731681 8.31% 0.704% 66 6.837 6.797 6.877 VV 158298894 2090754256 100.00% 8.476% 67 6.890 6.877 6.914 VV 3369872 46647530 2.23% 0.189% 68 6.937 6.914 7.002 VV 5221859 75769505 3.62% 0.307% 69 7.109 7.057 7.144 PV 33892942 464591155 22.22% 1.884% 70 7.173 7.144 7.284 VV 97055570 1386898433 66.33% 5.623% 71 7.288 7.284 7.295 VV 142677 879768 0.04% 0.004% 72 7.326 7.295 7.342 VV 149907 3466813 0.17% 0.014% 73 7.368 7.342 7.405 VV 2054574 28233386 1.35% 0.114% 74 7.429 7.405 7.444 VV 1999191 24108971 1.15% 0.098% 75 7.458 7.444 7.500 VV 1536161 20049129 0.96% 0.081% 76 7.529 7.500 7.576 PV 14948333 193428293 9.25% 0.784% 77 7.662 7.576 7.693 VV 38240253 489963338 23.43% 1.986% 78 7.705 7.693 7.752 VV 2003786 29560617 1.41% 0.120% 79 7.857 7.790 7.864 PV 192811 5118558 0.24% 0.021% 80 7.887 7.864 7.892 VV 197229 3023385 0.14% 0.012% 81 7.925 7.892 7.972 VV 8512870 118789638 5.68% 0.482% 82 8.136 7.972 8.217 VV 90901183 1245271479 59.56% 5.049% 83 8.269 8.217 8.274 VV 587349 19505213 0.93% 0.079% 84 8.281 8.274 8.286 VV 561598 4142814 0.20% 0.017% 85 8.310 8.286 8.317 VV 555435 9804119 0.47% 0.040% 86 8.433 8.317 8.458 VV 774699 57784809 2.76% 0.234% 87 8.623 8.458 8.632 VV 1023599 91869701 4.39% 0.372% 88 8.644 8.632 8.650 VV 1006162 11032816 0.53% 0.045% 89 8.758 8.650 8.762 VV 1123371 70486003 3.37% 0.286% 90 8.970 8.762 8.976 VV 1382213 160312062 7.67% 0.650% 91 8.983 8.976 9.008 VV 1351661 25703236 1.23% 0.104% 92 9.173 9.008 9.177 VV 1526227 142398077 6.81% 0.577% 93 9.212 9.177 9.217 VV 1500561 35762184 1.71% 0.145% 94 9.233 9.217 9.242 VV 1471333 21712222 1.04% 0.088% 95 9.262 9.242 9.267 VV 1486879 22326496 1.07% 0.091% 96 9.298 9.267 9.303 VV 1507792 31018715 1.48% 0.126% 97 9.391 9.303 9.405 VV 1536869 91775642 4.39% 0.372% 98 9.447 9.405 9.452 VV 1552022 43463844 2.08% 0.176% 99 9.474 9.452 9.482 VV 1576919 27366788 1.31% 0.111% 100 9.581 9.482 9.594 VV 1646742 106360501 5.09% 0.431% 101 9.634 9.594 9.639 VV 1686274 44660681 2.14% 0.181% 102 9.660 9.639 9.671 VV 1664209 31179976 1.49% 0.126% 103 9.708 9.671 9.718 VV 1633049 45472242 2.17% 0.184% 104 9.821 9.718 9.827 VV 1676607 104829686 5.01% 0.425% 105 9.885 9.827 9.891 VV 1751921 64968010 3.11% 0.263% 106 9.983 9.891 9.991 VV 1671806 99565488 4.76% 0.404% 107 9.998 9.991 10.006 VV 1664425 15333548 0.73% 0.062% 108 10.019 10.006 10.025 VV 1647467 18226647 0.87% 0.074% 109 10.044 10.025 10.050 VV 1660665 25263191 1.21% 0.102% 110 10.075 10.050 10.090 VV 1644171 38782713 1.85% 0.157% 111 10.095 10.090 10.099 VV 1629629 8510301 0.41% 0.035% 112 10.126 10.099 10.132 VV 1632834 31706047 1.52% 0.129% 113 10.222 10.132 10.244 VV 1633209 106995061 5.12% 0.434% 114 10.392 10.244 10.399 VV 1565980 145712193 6.97% 0.591% 115 10.416 10.399 10.439 VV 1556101 36423164 1.74% 0.148% 116 10.466 10.439 10.470 VV 1536885 28436369 1.36% 0.115% 117 10.486 10.470 10.499 VV 1516248 25617984 1.23% 0.104% 118 10.519 10.499 10.523 VV 1492931 21497602 1.03% 0.087% 119 10.528 10.523 10.533 VV 1457288 8439284 0.40% 0.034% 120 10.542 10.533 10.552 VV 1484193 16883846 0.81% 0.068% 121 10.557 10.552 10.562 VV 1461366 8104188 0.39% 0.033% 122 10.581 10.562 10.591 VV 1488043 24952736 1.19% 0.101% 123 10.596 10.591 10.602 VV 1424730 9442671 0.45% 0.038% 124 10.624 10.602 10.631 VV 1417939 24063592 1.15% 0.098% 125 10.649 10.631 10.661 VV 1389487 24674589 1.18% 0.100% 126 10.666 10.661 10.678 VV 1375621 13890450 0.66% 0.056% 127 10.778 10.731 10.787 VV 1231650 39074789 1.87% 0.158% 128 10.805 10.787 10.821 VV 1213245 24113410 1.15% 0.098% 129 10.827 10.821 10.834 VV 1179392 9050125 0.43% 0.037% 130 10.837 10.834 10.850 VV 1156095 11075804 0.53% 0.045% 131 10.865 10.850 10.884 VV 1179174 23069473 1.10% 0.094% 132 10.893 10.884 10.904 VV 1183671 13813767 0.66% 0.056% 133 10.918 10.904 10.928 VV 1153658 16615251 0.79% 0.067% 134 10.937 10.928 10.948 VV 1159006 13676576 0.65% 0.055% 135 10.962 10.948 10.972 VV 1120693 15646962 0.75% 0.063% 136 10.999 10.972 11.004 VV 1130980 21429717 1.02% 0.087% 137 11.012 11.004 11.020 VV 1108054 10579436 0.51% 0.043% 138 11.034 11.020 11.045 VV 1074220 15607840 0.75% 0.063% 139 11.066 11.045 11.074 VV 1059668 17471332 0.84% 0.071% 140 11.092 11.074 11.098 VV 1019986 14731094 0.70% 0.060% 141 11.104 11.098 11.110 VV 1027342 7290892 0.35% 0.030% 142 11.131 11.110 11.137 VV 989267 15477584 0.74% 0.063% 143 11.181 11.137 11.186 VV 986530 27770081 1.33% 0.113% 144 11.200 11.186 11.206 VV 951169 10913386 0.52% 0.044% 145 11.211 11.206 11.219 VV 921971 7371362 0.35% 0.030% 146 11.227 11.219 11.235 VV 916493 8492033 0.41% 0.034% 147 11.242 11.235 11.247 VV 901072 6158775 0.29% 0.025% 148 11.256 11.247 11.268 VV 899304 10697352 0.51% 0.043% 149 11.293 11.268 11.308 VV 884709 20414610 0.98% 0.083% 150 11.314 11.308 11.337 VV 852798 13853116 0.66% 0.056% 151 11.513 11.436 11.532 VV 581996 34002326 1.63% 0.138% 152 11.657 11.532 11.667 VV 419187 37824787 1.81% 0.153% 153 11.871 11.667 11.939 VV 183315 37479530 1.79% 0.152% Sum of corrected areas: 24666073181