Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO022118\ Data File : PO042516.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 20 Feb 2018 19:42 Sample : AR1660ICC750 Misc : ALS Vial : 4 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.163 3.148 3.187 VV 279767 3118725 0.37% 0.029% 2 3.224 3.187 3.249 VV 520499 5678881 0.68% 0.052% 3 3.300 3.267 3.328 VV 163560 2524411 0.30% 0.023% 4 3.396 3.368 3.428 BV 188477 3254485 0.39% 0.030% 5 3.479 3.428 3.511 VV 214533 6610494 0.79% 0.061% 6 3.589 3.511 3.601 VV 459612 15743657 1.89% 0.145% 7 3.607 3.601 3.627 VV 420143 5619058 0.67% 0.052% 8 3.643 3.627 3.685 VV 389892 10450239 1.25% 0.097% 9 3.720 3.685 3.769 VV 347528 14062579 1.69% 0.130% 10 3.800 3.769 3.832 VV 357755 11068900 1.33% 0.102% 11 3.869 3.832 3.941 VV 375581 18506578 2.22% 0.171% 12 4.023 3.993 4.064 VV 211720 6151817 0.74% 0.057% 13 4.102 4.064 4.209 VV 57895169 647439847 77.64% 5.983% 14 4.299 4.268 4.329 VV 1669993 26698785 3.20% 0.247% 15 4.387 4.329 4.421 VV 2619632 39521134 4.74% 0.365% 16 4.459 4.421 4.521 VV 11022011 136096278 16.32% 1.258% 17 4.548 4.521 4.579 VV 427696 11755196 1.41% 0.109% 18 4.605 4.579 4.663 VV 1718901 25809314 3.09% 0.239% 19 4.783 4.749 4.799 VV 14982148 165995305 19.90% 1.534% 20 4.812 4.799 4.848 VV 8605426 99002455 11.87% 0.915% 21 4.868 4.848 4.886 VV 1854917 21836262 2.62% 0.202% 22 4.897 4.886 4.907 VV 759857 7500692 0.90% 0.069% 23 4.920 4.907 4.943 VV 1230278 14035600 1.68% 0.130% 24 4.969 4.943 5.004 VV 15225032 167667348 20.11% 1.549% 25 5.041 5.024 5.054 VV 256567 3677273 0.44% 0.034% 26 5.079 5.054 5.110 VV 643215 11561190 1.39% 0.107% 27 5.133 5.110 5.147 VV 4283545 48430784 5.81% 0.448% 28 5.159 5.147 5.195 VV 3100709 40252131 4.83% 0.372% 29 5.228 5.195 5.237 VV 23074819 241398287 28.95% 2.231% 30 5.249 5.237 5.285 VV 30095329 372310295 44.64% 3.441% 31 5.309 5.285 5.378 VV 17928309 230301975 27.62% 2.128% 32 5.404 5.378 5.446 VV 15788856 192432446 23.07% 1.778% 33 5.468 5.446 5.474 VV 1735183 18044786 2.16% 0.167% 34 5.494 5.474 5.517 VV 11200716 140355522 16.83% 1.297% 35 5.538 5.517 5.564 VV 9992056 163239524 19.57% 1.509% 36 5.574 5.564 5.614 VV 5449290 73555386 8.82% 0.680% 37 5.691 5.614 5.715 VV 15714610 245812894 29.48% 2.272% 38 5.730 5.715 5.753 VV 6571998 86456680 10.37% 0.799% 39 5.774 5.753 5.796 VV 5097428 59442332 7.13% 0.549% 40 5.827 5.796 5.867 VV 12696974 189019635 22.67% 1.747% 41 5.891 5.867 5.920 VV 4053401 52473545 6.29% 0.485% 42 5.946 5.920 5.975 VV 767750 14349109 1.72% 0.133% 43 6.006 5.975 6.029 VV 876049 16425891 1.97% 0.152% 44 6.058 6.029 6.073 VV 13211335 167659693 20.10% 1.549% 45 6.082 6.073 6.102 VV 6477838 73288060 8.79% 0.677% 46 6.120 6.102 6.181 VV 4452064 65652065 7.87% 0.607% 47 6.208 6.181 6.238 VV 1608712 21364522 2.56% 0.197% 48 6.271 6.238 6.297 PV 11832508 141760125 17.00% 1.310% 49 6.310 6.297 6.371 VV 769039 16416738 1.97% 0.152% 50 6.473 6.439 6.496 VV 458403 7192975 0.86% 0.066% 51 6.544 6.519 6.555 VV 2080343 23807424 2.85% 0.220% 52 6.572 6.555 6.601 VV 5039119 60016661 7.20% 0.555% 53 6.628 6.601 6.658 VV 5881939 70653164 8.47% 0.653% 54 6.685 6.658 6.723 VV 14887851 229489382 27.52% 2.121% 55 6.736 6.723 6.761 VV 3975757 47846665 5.74% 0.442% 56 6.789 6.761 6.829 VV 28236391 335179692 40.19% 3.097% 57 6.906 6.875 6.936 PV 3987490 48392281 5.80% 0.447% 58 6.972 6.936 7.008 VV 5346106 66274325 7.95% 0.612% 59 7.040 7.008 7.064 VV 36418662 440729004 52.85% 4.073% 60 7.080 7.064 7.101 VV 10254125 116633883 13.99% 1.078% 61 7.121 7.101 7.143 VV 8055241 97064029 11.64% 0.897% 62 7.166 7.143 7.186 VV 15637636 191689240 22.99% 1.771% 63 7.197 7.186 7.233 VV 3211604 37874139 4.54% 0.350% 64 7.271 7.233 7.287 VV 3226455 50411728 6.04% 0.466% 65 7.316 7.287 7.338 VV 37343117 506945732 60.79% 4.685% 66 7.346 7.338 7.369 VV 5011112 64659194 7.75% 0.598% 67 7.393 7.369 7.424 VV 29450342 358909786 43.04% 3.317% 68 7.450 7.424 7.513 VV 15146301 181888627 21.81% 1.681% 69 7.580 7.513 7.591 VV 5583608 67524920 8.10% 0.624% 70 7.615 7.591 7.662 VV 25743587 358982888 43.05% 3.317% 71 7.692 7.662 7.725 VV 13623269 180683724 21.67% 1.670% 72 7.742 7.725 7.774 VV 6591763 84214102 10.10% 0.778% 73 7.800 7.774 7.818 VV 1335494 17186152 2.06% 0.159% 74 7.843 7.818 7.874 VV 7923539 101639896 12.19% 0.939% 75 7.915 7.874 7.944 VV 69346422 833953206 100.00% 7.707% 76 7.962 7.944 7.993 VV 3780950 49520973 5.94% 0.458% 77 8.200 8.142 8.226 VV 30351990 506035697 60.68% 4.676% 78 8.254 8.226 8.263 VV 12271575 173560158 20.81% 1.604% 79 8.269 8.263 8.321 VV 11985493 145695661 17.47% 1.346% 80 8.473 8.415 8.513 VV 1097029 23805241 2.85% 0.220% 81 8.550 8.513 8.581 VV 1161340 28087909 3.37% 0.260% 82 8.606 8.581 8.648 VV 6883406 101224150 12.14% 0.935% 83 8.778 8.746 8.796 VV 236531 6585428 0.79% 0.061% 84 8.842 8.796 8.889 VV 15536387 242242181 29.05% 2.239% 85 8.917 8.889 8.953 VV 1027138 21029998 2.52% 0.194% 86 8.970 8.953 8.976 VV 280836 3794861 0.46% 0.035% 87 8.984 8.976 8.989 VV 277529 2006348 0.24% 0.019% 88 9.002 8.989 9.010 VV 269777 3245420 0.39% 0.030% 89 9.071 9.010 9.078 VV 270422 10073941 1.21% 0.093% 90 9.088 9.078 9.099 VV 243617 3055016 0.37% 0.028% 91 9.198 9.158 9.237 VV 3852647 67413913 8.08% 0.623% 92 9.272 9.237 9.279 VV 232621 5678291 0.68% 0.052% 93 9.331 9.279 9.338 VV 232582 7504818 0.90% 0.069% 94 9.374 9.338 9.379 VV 196635 4850627 0.58% 0.045% 95 9.484 9.379 9.553 VV 34159719 623376158 74.75% 5.761% 96 9.565 9.553 9.580 VV 212158 2995953 0.36% 0.028% 97 9.585 9.580 9.601 VV 181542 2054281 0.25% 0.019% 98 9.670 9.601 9.713 VV 166866 9397510 1.13% 0.087% 99 9.721 9.713 9.735 VV 123595 1335286 0.16% 0.012% 100 9.795 9.754 9.806 VV 98419 2553056 0.31% 0.024% 101 9.811 9.806 9.838 VV 99885 1392700 0.17% 0.013% 102 9.903 9.838 9.907 VV 79770 2743467 0.33% 0.025% 103 9.913 9.907 9.919 VV 73992 458811 0.06% 0.004% 104 10.009 9.919 10.021 VV 68734 4058515 0.49% 0.038% 105 10.038 10.021 10.046 VV 56854 700277 0.08% 0.006% 106 10.061 10.046 10.066 VV 64954 538363 0.06% 0.005% 107 10.079 10.066 10.089 VV 52304 537050 0.06% 0.005% 108 10.131 10.089 10.135 VV 42536 819469 0.10% 0.008% 109 10.174 10.168 10.181 VV 55621 256779 0.03% 0.002% 110 10.212 10.181 10.217 VV 41280 440525 0.05% 0.004% 111 10.858 10.759 10.867 PV 34076 1067473 0.13% 0.010% 112 10.905 10.867 10.917 PV 45940 656737 0.08% 0.006% 113 11.033 10.917 11.038 VV 102324 4566801 0.55% 0.042% 114 11.063 11.038 11.069 VV 118890 1785059 0.21% 0.016% 115 11.084 11.069 11.106 VV 118786 2063342 0.25% 0.019% 116 11.113 11.106 11.117 VV 79022 467601 0.06% 0.004% 117 11.127 11.117 11.136 VV 84283 733363 0.09% 0.007% 118 11.141 11.136 11.155 VV 95045 716290 0.09% 0.007% 119 11.312 11.155 11.324 VV 149869 11094142 1.33% 0.103% 120 11.347 11.324 11.378 VV 141506 3678579 0.44% 0.034% 121 11.415 11.378 11.426 VV 104331 2306068 0.28% 0.021% 122 11.431 11.426 11.470 VB 86572 1122283 0.13% 0.010% Sum of corrected areas: 10820998314 Signal #2 : ECD2B.CH 1 2.540 2.506 2.583 BV 264474 3001952 0.18% 0.015% 2 2.676 2.648 2.718 VV 199726 4153980 0.25% 0.020% 3 2.954 2.932 2.980 PV 126573 1323991 0.08% 0.007% 4 3.349 3.316 3.488 PV 75508380 950320304 57.13% 4.683% 5 3.552 3.528 3.611 BV 2532723 32572683 1.96% 0.161% 6 3.634 3.611 3.673 VV 3694950 45860707 2.76% 0.226% 7 3.706 3.673 3.757 VV 14327196 177803123 10.69% 0.876% 8 3.793 3.757 3.824 VV 368768 9147677 0.55% 0.045% 9 3.862 3.824 3.931 VV 2200931 41480592 2.49% 0.204% 10 3.989 3.959 4.043 VV 20283698 384605909 23.12% 1.895% 11 4.064 4.043 4.084 VV 2671358 37168552 2.23% 0.183% 12 4.097 4.084 4.114 VV 1303524 17301993 1.04% 0.085% 13 4.132 4.114 4.145 VV 1988912 24320627 1.46% 0.120% 14 4.170 4.145 4.206 VV 18158636 267563956 16.09% 1.318% 15 4.217 4.206 4.243 VV 1075153 17370973 1.04% 0.086% 16 4.282 4.243 4.296 VV 6775056 90704515 5.45% 0.447% 17 4.306 4.296 4.352 VV 4589333 65251951 3.92% 0.322% 18 4.395 4.352 4.432 VV 45873533 911527937 54.80% 4.492% 19 4.451 4.432 4.534 VV 23011423 370665857 22.28% 1.826% 20 4.565 4.534 4.588 PV 21928378 272669052 16.39% 1.344% 21 4.607 4.588 4.626 VV 17147885 214301229 12.88% 1.056% 22 4.646 4.626 4.665 VV 19198885 263833073 15.86% 1.300% 23 4.674 4.665 4.756 VV 7987741 126826878 7.62% 0.625% 24 4.811 4.756 4.833 VV 21130044 300005647 18.04% 1.478% 25 4.847 4.833 4.864 VV 9523190 120863032 7.27% 0.596% 26 4.879 4.864 4.907 VV 7979455 113703490 6.84% 0.560% 27 4.951 4.907 4.988 VV 20393417 378918169 22.78% 1.867% 28 5.020 4.988 5.054 VV 6174924 107885327 6.49% 0.532% 29 5.080 5.054 5.094 VV 1390330 24549936 1.48% 0.121% 30 5.114 5.094 5.127 VV 5711190 68910734 4.14% 0.340% 31 5.147 5.127 5.171 VV 22149204 282118791 16.96% 1.390% 32 5.186 5.171 5.208 VV 5691572 76472125 4.60% 0.377% 33 5.217 5.208 5.222 VV 1501099 12110616 0.73% 0.060% 34 5.237 5.222 5.264 VV 2500594 37363631 2.25% 0.184% 35 5.291 5.264 5.327 VV 16531654 212114226 12.75% 1.045% 36 5.354 5.327 5.361 VV 1294570 19802829 1.19% 0.098% 37 5.375 5.361 5.419 VV 1805686 36956000 2.22% 0.182% 38 5.465 5.419 5.491 VV 834721 23131707 1.39% 0.114% 39 5.509 5.491 5.564 VV 893346 18949892 1.14% 0.093% 40 5.592 5.564 5.625 VV 3285699 45252740 2.72% 0.223% 41 5.656 5.625 5.666 VV 7577814 86738033 5.21% 0.427% 42 5.692 5.666 5.713 VV 26700564 412799734 24.82% 2.034% 43 5.732 5.713 5.776 VV 8925983 172743836 10.39% 0.851% 44 5.804 5.776 5.847 VV 46045931 585072691 35.17% 2.883% 45 5.864 5.847 5.882 VV 936392 13655407 0.82% 0.067% 46 5.902 5.882 5.913 VV 3340856 37569717 2.26% 0.185% 47 5.931 5.913 5.962 VV 9313583 122113984 7.34% 0.602% 48 5.990 5.962 6.099 VV 64609663 817058979 49.12% 4.026% 49 6.136 6.099 6.183 VV 53489797 695102594 41.79% 3.425% 50 6.209 6.183 6.232 VV 5639634 75098188 4.51% 0.370% 51 6.255 6.232 6.279 VV 15188347 196580139 11.82% 0.969% 52 6.307 6.279 6.326 VV 59247624 832145011 50.03% 4.100% 53 6.343 6.326 6.374 VV 54385508 753066102 45.27% 3.711% 54 6.396 6.374 6.474 VV 26474177 357333398 21.48% 1.761% 55 6.531 6.498 6.566 VV 9442568 139248089 8.37% 0.686% 56 6.594 6.566 6.620 VV 44314176 577568715 34.72% 2.846% 57 6.631 6.620 6.654 VV 5018118 62689065 3.77% 0.309% 58 6.689 6.654 6.716 VV 23396583 328047202 19.72% 1.616% 59 6.736 6.716 6.751 VV 11601948 145891689 8.77% 0.719% 60 6.765 6.751 6.796 VV 9577575 139787757 8.40% 0.689% 61 6.837 6.796 6.876 VV 125440049 1663360834 100.00% 8.196% 62 6.890 6.876 6.914 VV 2674549 37417124 2.25% 0.184% 63 6.936 6.914 6.991 VV 4163557 59092800 3.55% 0.291% 64 7.109 7.053 7.144 PV 27974520 371627560 22.34% 1.831% 65 7.173 7.144 7.277 VV 76882926 1106375876 66.51% 5.452% 66 7.286 7.277 7.308 VV 111868 1750263 0.11% 0.009% 67 7.334 7.308 7.341 VV 121556 2106707 0.13% 0.010% 68 7.368 7.341 7.403 VV 1692684 24280504 1.46% 0.120% 69 7.428 7.403 7.445 VV 1614435 20407190 1.23% 0.101% 70 7.458 7.445 7.500 VV 1223304 17184162 1.03% 0.085% 71 7.529 7.500 7.581 PV 11944272 155832355 9.37% 0.768% 72 7.590 7.581 7.598 VV 86997 607245 0.04% 0.003% 73 7.611 7.598 7.624 VV 57721 637288 0.04% 0.003% 74 7.662 7.624 7.694 PV 30068073 384662551 23.13% 1.895% 75 7.706 7.694 7.746 VV 1557183 23672158 1.42% 0.117% 76 7.769 7.746 7.794 VV 155556 3292715 0.20% 0.016% 77 7.877 7.794 7.884 PV 99002 4289227 0.26% 0.021% 78 7.924 7.884 7.979 VV 6792883 94575874 5.69% 0.466% 79 7.990 7.979 7.999 VV 237344 2525680 0.15% 0.012% 80 8.005 7.999 8.009 VV 244970 1360924 0.08% 0.007% 81 8.136 8.009 8.217 VV 72985858 991056744 59.58% 4.883% 82 8.223 8.217 8.227 VV 439670 2548576 0.15% 0.013% 83 8.349 8.227 8.355 VV 630388 40915413 2.46% 0.202% 84 8.438 8.355 8.451 VV 708667 37678361 2.27% 0.186% 85 8.498 8.451 8.502 VV 798262 22224917 1.34% 0.110% 86 8.678 8.502 8.682 VV 1011777 100523878 6.04% 0.495% 87 8.760 8.682 8.764 VV 1164902 53408077 3.21% 0.263% 88 8.780 8.764 8.784 VV 1187475 13620029 0.82% 0.067% 89 9.073 8.784 9.078 VV 1605678 233496271 14.04% 1.151% 90 9.087 9.078 9.094 VV 1607856 15364023 0.92% 0.076% 91 9.205 9.094 9.241 VV 1794746 147922669 8.89% 0.729% 92 9.244 9.241 9.251 VV 1743679 9936325 0.60% 0.049% 93 9.343 9.251 9.354 VV 1907562 110763960 6.66% 0.546% 94 9.378 9.354 9.384 VV 1888692 32783428 1.97% 0.162% 95 9.395 9.384 9.406 VV 1884157 25102634 1.51% 0.124% 96 9.446 9.406 9.460 VV 1856009 59708016 3.59% 0.294% 97 9.509 9.460 9.514 VV 1794990 57526513 3.46% 0.283% 98 9.519 9.514 9.529 VV 1785919 16194447 0.97% 0.080% 99 9.605 9.529 9.619 VV 1831025 95708155 5.75% 0.472% 100 9.646 9.619 9.671 VV 1826989 55572337 3.34% 0.274% 101 9.708 9.671 9.719 VV 1768055 51062784 3.07% 0.252% 102 9.740 9.719 9.752 VV 1769185 33565959 2.02% 0.165% 103 9.759 9.752 9.764 VV 1704260 12814285 0.77% 0.063% 104 9.846 9.764 9.853 VV 1764078 92211292 5.54% 0.454% 105 9.858 9.853 9.862 VV 1709132 8816846 0.53% 0.043% 106 9.920 9.862 9.935 VV 1742706 75725061 4.55% 0.373% 107 9.961 9.935 9.968 VV 1746103 33541452 2.02% 0.165% 108 9.989 9.968 9.994 VV 1742650 27619429 1.66% 0.136% 109 10.013 9.994 10.021 VV 1726062 27240905 1.64% 0.134% 110 10.108 10.021 10.117 VV 1675789 95378696 5.73% 0.470% 111 10.233 10.117 10.238 VV 1607240 117625929 7.07% 0.580% 112 10.246 10.238 10.263 VV 1617335 23942339 1.44% 0.118% 113 10.268 10.263 10.273 VV 1578818 9176769 0.55% 0.045% 114 10.279 10.273 10.294 VV 1564454 19046702 1.15% 0.094% 115 10.314 10.294 10.326 VV 1565212 29737739 1.79% 0.147% 116 10.334 10.326 10.340 VV 1521831 12392765 0.75% 0.061% 117 10.378 10.340 10.394 VV 1528303 49112862 2.95% 0.242% 118 10.403 10.394 10.416 VV 1501229 18947700 1.14% 0.093% 119 10.424 10.416 10.445 VV 1487818 25008292 1.50% 0.123% 120 10.450 10.445 10.454 VV 1433536 7889013 0.47% 0.039% 121 10.472 10.454 10.478 VV 1443759 20214091 1.22% 0.100% 122 10.483 10.478 10.506 VV 1452552 24287553 1.46% 0.120% 123 10.519 10.506 10.526 VV 1383070 15957941 0.96% 0.079% 124 10.545 10.526 10.553 VV 1384662 22038446 1.32% 0.109% 125 10.563 10.553 10.568 VV 1382112 12641178 0.76% 0.062% 126 10.578 10.568 10.616 VV 1356978 37525271 2.26% 0.185% 127 10.621 10.616 10.630 VV 1362521 11271571 0.68% 0.056% 128 10.635 10.630 10.640 VV 1301787 7468433 0.45% 0.037% 129 10.657 10.640 10.662 VV 1284244 17193878 1.03% 0.085% 130 10.685 10.662 10.724 VV 1267126 44639602 2.68% 0.220% 131 10.796 10.724 10.804 VV 1180473 54231284 3.26% 0.267% 132 10.978 10.804 10.999 VV 1032403 124409752 7.48% 0.613% 133 11.272 10.999 11.299 VV 796466 151829681 9.13% 0.748% 134 11.549 11.299 11.567 VV 451491 87808755 5.28% 0.433% 135 11.709 11.567 11.749 VV 232260 30108597 1.81% 0.148% 136 11.830 11.749 11.842 VV 79179 5218061 0.31% 0.026% Sum of corrected areas: 20294011455