Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_O\Data\PO022118\ Data File : PO042519.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 20 Feb 2018 20:27 Operator : SM/UA Sample : AR1660ICC050 Misc : ALS Vial : 7 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 21 08:53:23 2018 Quant Method : P:\HPCHEM1\ECD_O\methods\PO022118.M Quant Title : GC EXTRACTABLES QLast Update : Wed Feb 21 08:41:26 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Small noise peaks clipped Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30Mx0.32mmx 0.50µ Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 4.101 3.348 1126999 1687597 4.549 4.576m 2) SA Decachlor... 9.484 8.136 1299074 1873207 5.140 4.858 Target Compounds 3) L1 AR-1016-1 4.969 4.170 332261 419839 49.474 43.838 4) L1 AR-1016-2 5.310 4.607 455233 349566 50.836 41.275m 5) L1 AR-1016-3 5.405 4.646 326157 495812 44.935 49.135m 6) L1 AR-1016-4 5.827 4.811 253907 537767 35.558m 48.944m# 7) L1 AR-1016-5 6.058 5.148 443477 447064 63.806m 42.294 # 31) L7 AR-1260-1 6.789 5.804 693562 1184543 50.413 49.164m 32) L7 AR-1260-2 7.040 5.991 907029 1644301 49.587 48.767m 33) L7 AR-1260-3 7.316 6.136 999014 1380766 48.148m 48.443m 34) L7 AR-1260-4 7.394 6.307 724752 1674209 48.909m 48.972 35) L7 AR-1260-5 7.915 6.837 1640717 3181808 48.374 47.016 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.