Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO022118\ Data File : PO042519.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 20 Feb 2018 20:27 Sample : AR1660ICC050 Misc : ALS Vial : 7 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.224 3.206 3.263 VV 254624 2866964 1.38% 0.160% 2 3.477 3.430 3.506 PV 95237 2550318 1.23% 0.142% 3 3.532 3.506 3.540 VV 128589 1614687 0.78% 0.090% 4 3.608 3.540 3.630 VV 291498 10838545 5.21% 0.605% 5 3.636 3.630 3.681 VV 213357 5048955 2.43% 0.282% 6 3.726 3.681 3.755 VV 174625 5803387 2.79% 0.324% 7 3.798 3.755 3.830 VV 172792 4876660 2.35% 0.272% 8 3.879 3.830 3.943 VV 148258 5488666 2.64% 0.307% 9 4.101 4.063 4.201 PV 3401714 40309016 19.38% 2.252% 10 4.298 4.276 4.325 VV 159898 2353046 1.13% 0.131% 11 4.385 4.341 4.412 VV 143391 2551666 1.23% 0.143% 12 4.459 4.431 4.483 VV 663704 7618573 3.66% 0.426% 13 4.553 4.515 4.586 VV 150253 3669178 1.76% 0.205% 14 4.783 4.761 4.799 VV 967444 11069530 5.32% 0.618% 15 4.811 4.799 4.851 VV 584306 7725140 3.71% 0.432% 16 4.969 4.946 5.009 PV 981338 12100525 5.82% 0.676% 17 5.039 5.009 5.060 VV 183578 3791987 1.82% 0.212% 18 5.091 5.060 5.116 VV 172464 4678331 2.25% 0.261% 19 5.134 5.116 5.148 VV 362557 5113036 2.46% 0.286% 20 5.172 5.148 5.192 VV 605684 10589720 5.09% 0.592% 21 5.228 5.192 5.237 VV 1628181 20371996 9.80% 1.138% 22 5.250 5.237 5.285 VV 2028590 29210395 14.05% 1.632% 23 5.309 5.285 5.344 VV 1324965 20823039 10.01% 1.163% 24 5.405 5.381 5.448 VV 1195273 20767239 9.99% 1.160% 25 5.468 5.448 5.473 VV 423803 5109637 2.46% 0.285% 26 5.495 5.473 5.516 VV 986296 16056904 7.72% 0.897% 27 5.538 5.516 5.564 VV 984289 19827060 9.53% 1.108% 28 5.577 5.564 5.613 VV 773730 17613314 8.47% 0.984% 29 5.687 5.613 5.718 VV 2396062 67722941 32.57% 3.783% 30 5.729 5.718 5.757 VV 957014 16302808 7.84% 0.911% 31 5.773 5.757 5.797 VV 576283 8924983 4.29% 0.499% 32 5.828 5.797 5.871 PV 971148 20665433 9.94% 1.154% 33 5.893 5.871 5.921 VV 490313 10729102 5.16% 0.599% 34 5.998 5.921 6.025 VV 319662 17975160 8.64% 1.004% 35 6.058 6.025 6.073 VV 1268653 20752490 9.98% 1.159% 36 6.080 6.073 6.105 VV 980660 14367243 6.91% 0.803% 37 6.118 6.105 6.156 VV 581320 11618087 5.59% 0.649% 38 6.270 6.239 6.292 PV 835557 10925488 5.25% 0.610% 39 6.311 6.292 6.361 VV 173178 4010605 1.93% 0.224% 40 6.503 6.423 6.528 BV 107177 2584464 1.24% 0.144% 41 6.542 6.528 6.555 VV 152320 1697942 0.82% 0.095% 42 6.572 6.555 6.601 VV 347644 4601449 2.21% 0.257% 43 6.628 6.601 6.654 VV 526660 7222965 3.47% 0.404% 44 6.686 6.654 6.725 VV 1066724 18246162 8.77% 1.019% 45 6.736 6.725 6.759 VV 354261 4731632 2.28% 0.264% 46 6.789 6.759 6.825 VV 1969196 26273470 12.63% 1.468% 47 6.906 6.879 6.940 VV 339482 6666667 3.21% 0.372% 48 6.972 6.940 7.006 VV 463262 8915091 4.29% 0.498% 49 7.040 7.006 7.063 VV 2768193 34102794 16.40% 1.905% 50 7.079 7.063 7.101 VV 810755 9675796 4.65% 0.541% 51 7.121 7.101 7.141 PV 688665 8801158 4.23% 0.492% 52 7.166 7.141 7.185 VV 1223008 16294835 7.84% 0.910% 53 7.197 7.185 7.234 VV 327226 5781137 2.78% 0.323% 54 7.272 7.234 7.287 VV 308928 6420433 3.09% 0.359% 55 7.316 7.287 7.338 VV 2590606 36678924 17.64% 2.049% 56 7.348 7.338 7.367 VV 414428 5674308 2.73% 0.317% 57 7.394 7.367 7.424 VV 2061689 26247614 12.62% 1.466% 58 7.449 7.424 7.493 VV 1026240 13257464 6.38% 0.741% 59 7.579 7.546 7.588 BV 384772 4364348 2.10% 0.244% 60 7.614 7.588 7.659 VV 1744747 25829211 12.42% 1.443% 61 7.691 7.659 7.726 VV 960050 14635748 7.04% 0.818% 62 7.742 7.726 7.768 VV 501693 7167739 3.45% 0.400% 63 7.800 7.768 7.820 VV 171909 3695437 1.78% 0.206% 64 7.844 7.820 7.871 VV 609962 9311010 4.48% 0.520% 65 7.915 7.871 7.943 VV 4511327 59502410 28.61% 3.324% 66 7.963 7.943 7.986 VV 406812 7601314 3.66% 0.425% 67 8.008 7.986 8.018 VV 261898 4568167 2.20% 0.255% 68 8.024 8.018 8.029 VV 232285 1498986 0.72% 0.084% 69 8.070 8.029 8.084 VV 236436 7469106 3.59% 0.417% 70 8.090 8.084 8.094 VV 235456 1405749 0.68% 0.079% 71 8.148 8.094 8.155 VV 250555 8699796 4.18% 0.486% 72 8.199 8.155 8.227 VV 2194889 43183590 20.77% 2.412% 73 8.256 8.227 8.307 VV 1064186 32466965 15.61% 1.814% 74 8.310 8.307 8.314 VV 276707 1226939 0.59% 0.069% 75 8.355 8.314 8.360 VV 309508 7580062 3.65% 0.423% 76 8.365 8.360 8.370 VV 305125 1728961 0.83% 0.097% 77 8.440 8.380 8.444 VV 343721 12521065 6.02% 0.699% 78 8.474 8.444 8.490 VV 407941 10138963 4.88% 0.566% 79 8.495 8.490 8.499 VV 355972 1979445 0.95% 0.111% 80 8.570 8.499 8.583 VV 456453 19841995 9.54% 1.108% 81 8.607 8.583 8.641 VV 821510 19612469 9.43% 1.096% 82 8.651 8.641 8.666 VV 424094 6071948 2.92% 0.339% 83 8.676 8.666 8.681 VV 430520 3941813 1.90% 0.220% 84 8.748 8.681 8.753 VV 438153 18264450 8.78% 1.020% 85 8.782 8.753 8.786 VV 441089 8645916 4.16% 0.483% 86 8.841 8.786 8.879 VV 1437031 38716087 18.62% 2.163% 87 8.922 8.879 8.943 VV 527619 18739577 9.01% 1.047% 88 8.983 8.943 8.987 VV 508612 13172530 6.33% 0.736% 89 9.031 8.987 9.040 VV 506306 15373920 7.39% 0.859% 90 9.197 9.040 9.242 VV 723121 63810845 30.69% 3.565% 91 9.321 9.242 9.327 VV 519593 25482636 12.25% 1.424% 92 9.333 9.327 9.338 VV 523951 3382207 1.63% 0.189% 93 9.369 9.338 9.375 VV 524780 11276870 5.42% 0.630% 94 9.484 9.375 9.524 VV 2911733 86491566 41.59% 4.832% 95 9.530 9.524 9.535 VV 547705 3433903 1.65% 0.192% 96 9.541 9.535 9.546 VV 536399 3514760 1.69% 0.196% 97 9.552 9.546 9.559 VV 534812 3952217 1.90% 0.221% 98 9.640 9.559 9.645 VV 531019 26680977 12.83% 1.491% 99 9.652 9.645 9.658 VV 534327 4156658 2.00% 0.232% 100 9.746 9.678 9.751 VV 518978 21975084 10.57% 1.228% 101 9.836 9.776 9.845 VV 513293 20808159 10.01% 1.162% 102 10.676 9.888 10.690 VV 378106 207952426 100.00% 11.617% 103 10.741 10.690 10.750 VV 368387 13247873 6.37% 0.740% 104 11.091 10.750 11.152 VV 274793 71298599 34.29% 3.983% 105 11.288 11.152 11.299 VV 200269 18017388 8.66% 1.007% 106 11.737 11.299 11.756 VV 42925 27274538 13.12% 1.524% Sum of corrected areas: 1790018582 Signal #2 : ECD2B.CH 1 2.996 2.976 3.068 VV 136242 2377829 1.60% 0.054% 2 3.348 3.298 3.420 VV 4369106 58462168 39.31% 1.326% 3 3.552 3.473 3.598 VV 280223 11867573 7.98% 0.269% 4 3.634 3.613 3.675 VV 380016 8944753 6.01% 0.203% 5 3.705 3.675 3.754 VV 1071272 18048358 12.14% 0.409% 6 3.802 3.754 3.809 VV 278590 7066916 4.75% 0.160% 7 3.865 3.809 3.930 VV 488660 26659479 17.93% 0.604% 8 3.952 3.930 3.960 VV 387463 6644147 4.47% 0.151% 9 3.990 3.960 4.037 VV 1595234 39273700 26.41% 0.891% 10 4.063 4.037 4.085 VV 539198 13346573 8.97% 0.303% 11 4.097 4.085 4.117 VV 474080 8306747 5.59% 0.188% 12 4.134 4.117 4.146 VV 490673 7671302 5.16% 0.174% 13 4.171 4.146 4.208 VV 1511973 31706485 21.32% 0.719% 14 4.214 4.208 4.239 VV 532263 9338528 6.28% 0.212% 15 4.265 4.239 4.274 VV 1008360 16025168 10.77% 0.363% 16 4.280 4.274 4.296 VV 970119 11355174 7.63% 0.257% 17 4.306 4.296 4.343 VV 778195 17527288 11.78% 0.397% 18 4.396 4.343 4.432 VV 3387585 83508427 56.15% 1.893% 19 4.451 4.432 4.536 VV 1953035 50021973 33.63% 1.134% 20 4.565 4.536 4.588 PV 1742635 26886140 18.08% 0.610% 21 4.608 4.588 4.626 VV 1587031 24827753 16.69% 0.563% 22 4.646 4.626 4.665 VV 1758351 29112267 19.57% 0.660% 23 4.674 4.665 4.715 VV 1018631 22544856 15.16% 0.511% 24 4.721 4.715 4.745 VV 584973 10170201 6.84% 0.231% 25 4.811 4.745 4.833 VV 1897718 47368296 31.85% 1.074% 26 4.847 4.833 4.864 VV 1161124 17922281 12.05% 0.406% 27 4.879 4.864 4.905 VV 1080575 21784798 14.65% 0.494% 28 4.955 4.905 5.005 VV 2724607 84468624 56.79% 1.915% 29 5.018 5.005 5.056 VV 859026 18574789 12.49% 0.421% 30 5.116 5.097 5.128 VV 579188 8723488 5.87% 0.198% 31 5.148 5.128 5.170 VV 1595230 21649875 14.56% 0.491% 32 5.186 5.170 5.206 VV 455483 7505141 5.05% 0.170% 33 5.240 5.206 5.260 VV 303499 7669345 5.16% 0.174% 34 5.291 5.260 5.323 VV 1159083 17799695 11.97% 0.404% 35 5.354 5.323 5.363 VV 205072 4162101 2.80% 0.094% 36 5.376 5.363 5.396 VV 208624 3347316 2.25% 0.076% 37 5.470 5.434 5.497 VV 362684 8033737 5.40% 0.182% 38 5.512 5.497 5.546 VB 154973 2537841 1.71% 0.058% 39 5.593 5.558 5.631 BV 250132 4194167 2.82% 0.095% 40 5.657 5.631 5.665 VV 619919 7699291 5.18% 0.175% 41 5.692 5.665 5.714 VV 1824956 30393557 20.44% 0.689% 42 5.730 5.714 5.778 VV 676704 14823037 9.97% 0.336% 43 5.805 5.778 5.851 VV 3221002 45881747 30.85% 1.040% 44 5.865 5.851 5.870 VV 288201 2998504 2.02% 0.068% 45 5.901 5.883 5.914 VV 400239 5885805 3.96% 0.133% 46 5.929 5.914 5.951 VV 584228 6881079 4.63% 0.156% 47 5.991 5.951 6.033 PV 4566864 64177644 43.15% 1.455% 48 6.042 6.033 6.045 VV 266942 1881853 1.27% 0.043% 49 6.053 6.045 6.058 VV 267054 1954272 1.31% 0.044% 50 6.083 6.058 6.092 VV 263847 5185575 3.49% 0.118% 51 6.136 6.092 6.179 VV 3677976 57219994 38.47% 1.297% 52 6.209 6.179 6.231 VV 598772 11976747 8.05% 0.272% 53 6.255 6.231 6.278 VV 1196893 18314016 12.31% 0.415% 54 6.307 6.278 6.326 VV 4031142 59723982 40.16% 1.354% 55 6.343 6.326 6.374 VV 3708079 54637350 36.74% 1.239% 56 6.396 6.374 6.437 VV 1938248 28998653 19.50% 0.658% 57 6.532 6.507 6.567 VV 683492 11935356 8.02% 0.271% 58 6.595 6.567 6.621 VV 2951098 39807915 26.77% 0.903% 59 6.631 6.621 6.655 VV 428843 5646753 3.80% 0.128% 60 6.689 6.655 6.715 VV 1571656 23680128 15.92% 0.537% 61 6.736 6.715 6.751 VV 812619 10944238 7.36% 0.248% 62 6.765 6.751 6.796 VV 670799 10699394 7.19% 0.243% 63 6.837 6.796 6.876 VV 7804267 108714275 73.10% 2.465% 64 6.891 6.876 6.910 VV 242937 3576953 2.41% 0.081% 65 6.937 6.910 6.958 VV 322931 5548579 3.73% 0.126% 66 7.028 6.975 7.059 VV 127569 4463134 3.00% 0.101% 67 7.109 7.059 7.136 PV 1769652 24385705 16.40% 0.553% 68 7.173 7.136 7.216 VV 5025296 71591640 48.14% 1.623% 69 7.270 7.216 7.275 VV 61984 1819697 1.22% 0.041% 70 7.293 7.275 7.298 VV 55548 610755 0.41% 0.014% 71 7.371 7.298 7.408 VV 176550 4695218 3.16% 0.106% 72 7.430 7.408 7.446 VV 152180 1798933 1.21% 0.041% 73 7.460 7.446 7.488 VV 106702 1474091 0.99% 0.033% 74 7.499 7.488 7.506 VV 34250 228696 0.15% 0.005% 75 7.528 7.506 7.568 PV 768452 10187385 6.85% 0.231% 76 7.595 7.568 7.600 VV 56483 925997 0.62% 0.021% 77 7.615 7.600 7.621 VV 61197 530386 0.36% 0.012% 78 7.662 7.621 7.695 VV 1931268 26415177 17.76% 0.599% 79 7.710 7.695 7.730 VV 196196 2955455 1.99% 0.067% 80 7.735 7.730 7.738 VV 93349 416490 0.28% 0.009% 81 7.769 7.738 7.792 VV 105837 2522079 1.70% 0.057% 82 7.825 7.792 7.829 PV 128921 1597817 1.07% 0.036% 83 7.835 7.829 7.841 VV 119963 776333 0.52% 0.018% 84 7.926 7.841 7.956 VV 590112 15235116 10.24% 0.345% 85 8.137 7.956 8.186 VV 4888331 96585816 64.94% 2.190% 86 8.203 8.186 8.208 VV 420750 5074410 3.41% 0.115% 87 8.221 8.208 8.224 VV 424019 4101758 2.76% 0.093% 88 8.277 8.224 8.281 VV 552488 17033054 11.45% 0.386% 89 8.382 8.281 8.386 VV 691385 39562779 26.60% 0.897% 90 8.393 8.386 8.400 VV 710838 5542845 3.73% 0.126% 91 8.611 8.400 8.617 VV 1088954 116711961 78.47% 2.646% 92 8.804 8.617 8.809 VV 1246062 132035982 88.78% 2.994% 93 8.876 8.809 8.880 VV 1311600 55104184 37.05% 1.249% 94 8.925 8.880 8.931 VV 1358087 40125161 26.98% 0.910% 95 8.960 8.931 8.965 VV 1394054 27370017 18.40% 0.621% 96 9.123 8.965 9.129 VV 1466683 142001438 95.48% 3.220% 97 9.156 9.129 9.161 VV 1475091 27881317 18.75% 0.632% 98 9.282 9.161 9.290 VV 1605712 118365814 79.59% 2.684% 99 9.300 9.290 9.308 VV 1618864 17209951 11.57% 0.390% 100 9.389 9.308 9.395 VV 1651009 84043331 56.51% 1.906% 101 9.457 9.395 9.480 VV 1701418 84453742 56.78% 1.915% 102 9.520 9.480 9.522 VV 1706296 43167019 29.02% 0.979% 103 9.557 9.522 9.561 VV 1713027 39111360 26.30% 0.887% 104 9.580 9.561 9.586 VV 1724468 24857370 16.71% 0.564% 105 9.626 9.586 9.644 VV 1740961 59011500 39.68% 1.338% 106 9.665 9.644 9.669 VV 1698060 25757794 17.32% 0.584% 107 9.697 9.669 9.716 VV 1737892 47880308 32.19% 1.086% 108 9.764 9.716 9.770 VV 1729594 54815822 36.86% 1.243% 109 9.791 9.770 9.798 VV 1790558 29828514 20.06% 0.676% 110 9.877 9.798 9.882 VV 1767826 88196934 59.30% 2.000% 111 9.888 9.882 9.914 VV 1772096 33755554 22.70% 0.765% 112 9.957 9.914 9.964 VV 1745337 50967658 34.27% 1.156% 113 10.104 9.964 10.110 VV 1690329 148727863 100.00% 3.372% 114 10.116 10.110 10.125 VV 1666876 14489776 9.74% 0.329% 115 10.177 10.125 10.191 VV 1690811 65690694 44.17% 1.489% 116 10.232 10.191 10.244 VV 1648954 51737154 34.79% 1.173% 117 10.256 10.244 10.273 VV 1641321 27609567 18.56% 0.626% 118 10.285 10.273 10.291 VV 1624505 17699237 11.90% 0.401% 119 10.301 10.291 10.324 VV 1626214 30902070 20.78% 0.701% 120 10.369 10.324 10.380 VV 1591177 52649913 35.40% 1.194% 121 10.394 10.380 10.398 VV 1575782 17109689 11.50% 0.388% 122 10.403 10.398 10.407 VV 1568876 8700093 5.85% 0.197% 123 10.414 10.407 10.422 VV 1562219 13313926 8.95% 0.302% 124 10.439 10.422 10.448 VV 1545016 23562818 15.84% 0.534% 125 10.486 10.448 10.493 VV 1533810 40720150 27.38% 0.923% 126 10.497 10.493 10.508 VV 1517273 13978787 9.40% 0.317% 127 10.541 10.508 10.548 VV 1514119 35289166 23.73% 0.800% 128 10.563 10.548 10.569 VV 1499950 18925497 12.72% 0.429% 129 10.579 10.569 10.585 VV 1473474 13065955 8.79% 0.296% 130 10.596 10.585 10.603 VV 1439159 15412414 10.36% 0.349% 131 10.609 10.603 10.611 VV 1417483 7079363 4.76% 0.161% 132 10.645 10.611 10.650 VV 1425313 32549306 21.89% 0.738% 133 10.661 10.650 10.714 VV 1418498 51944219 34.93% 1.178% 134 10.745 10.726 10.750 VV 1301323 17969080 12.08% 0.407% 135 10.793 10.750 10.798 VV 1319039 37393174 25.14% 0.848% 136 10.968 10.798 10.988 VV 1197692 138383399 93.04% 3.138% 137 11.009 10.988 11.038 VV 1137040 33336437 22.41% 0.756% 138 11.179 11.038 11.210 VV 1020154 105026450 70.62% 2.381% 139 11.261 11.210 11.285 VV 914473 41107884 27.64% 0.932% 140 11.374 11.285 11.397 VV 825312 53731087 36.13% 1.218% 141 11.413 11.397 11.428 VV 757644 13163537 8.85% 0.298% 142 11.528 11.428 11.558 VV 629004 49501920 33.28% 1.122% 143 11.566 11.558 11.601 VV 612326 14253913 9.58% 0.323% 144 11.666 11.601 11.723 VV 479011 31787361 21.37% 0.721% 145 11.763 11.723 11.771 VV 344681 9745192 6.55% 0.221% 146 11.780 11.771 11.795 VV 318477 4205254 2.83% 0.095% 147 11.812 11.795 11.822 VV 297031 4654328 3.13% 0.106% 148 11.872 11.822 11.885 VV 228162 8190688 5.51% 0.186% 149 11.959 11.885 11.988 VV 115775 6861449 4.61% 0.156% Sum of corrected areas: 4410274302