Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO022118\ Data File : PO042521.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 20 Feb 2018 20:57 Sample : AR1232ICC500 Misc : ALS Vial : 9 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.163 3.137 3.205 PV 270030 5164396 1.25% 0.225% 2 3.224 3.205 3.249 VV 455688 5391099 1.30% 0.234% 3 3.298 3.249 3.328 VV 129183 3500270 0.84% 0.152% 4 3.396 3.356 3.423 VV 91913 1696763 0.41% 0.074% 5 3.481 3.423 3.511 PV 88445 2159187 0.52% 0.094% 6 3.589 3.511 3.623 VV 1210220 19273454 4.65% 0.838% 7 3.639 3.623 3.694 VV 179338 4771957 1.15% 0.207% 8 3.715 3.694 3.758 VB 102924 2400298 0.58% 0.104% 9 3.796 3.760 3.835 BV 399635 9272874 2.24% 0.403% 10 3.877 3.835 3.941 VV 228128 10680020 2.58% 0.464% 11 3.967 3.941 3.996 VV 312850 4612481 1.11% 0.201% 12 4.102 4.061 4.207 PV 36856247 408609756 98.61% 17.765% 13 4.302 4.260 4.354 VV 1764894 27532329 6.64% 1.197% 14 4.386 4.354 4.424 VV 1858697 25137706 6.07% 1.093% 15 4.459 4.424 4.520 VV 6490328 78107509 18.85% 3.396% 16 4.550 4.520 4.580 VV 204838 5720097 1.38% 0.249% 17 4.603 4.580 4.659 VV 419439 8434635 2.04% 0.367% 18 4.783 4.755 4.799 VV 3481315 37898270 9.15% 1.648% 19 4.811 4.799 4.853 VV 2010611 27049757 6.53% 1.176% 20 4.868 4.853 4.885 VV 478868 5683200 1.37% 0.247% 21 4.920 4.904 4.944 VV 639530 7332038 1.77% 0.319% 22 4.969 4.944 5.001 VV 3348523 38314930 9.25% 1.666% 23 5.035 5.001 5.052 VV 167403 3455527 0.83% 0.150% 24 5.070 5.052 5.111 VV 287349 6615273 1.60% 0.288% 25 5.133 5.111 5.147 VV 1033049 12203402 2.94% 0.531% 26 5.171 5.147 5.197 VV 1572492 25387945 6.13% 1.104% 27 5.227 5.197 5.237 VV 5050448 55403197 13.37% 2.409% 28 5.249 5.237 5.286 VV 6687608 87120536 21.02% 3.788% 29 5.309 5.286 5.353 VV 4217388 57287155 13.82% 2.491% 30 5.404 5.378 5.449 VV 3557776 48401593 11.68% 2.104% 31 5.467 5.449 5.473 VV 534971 5946875 1.44% 0.259% 32 5.494 5.473 5.516 VV 2380978 31809338 7.68% 1.383% 33 5.538 5.516 5.563 VV 2274533 38819585 9.37% 1.688% 34 5.573 5.563 5.618 VV 1346003 24105183 5.82% 1.048% 35 5.690 5.618 5.715 VV 3893848 76154129 18.38% 3.311% 36 5.730 5.715 5.754 VV 1712234 25009112 6.04% 1.087% 37 5.773 5.754 5.797 VV 1230029 15988116 3.86% 0.695% 38 5.828 5.797 5.865 PV 2740950 45966590 11.09% 1.998% 39 5.891 5.865 5.920 VV 1050052 17386471 4.20% 0.756% 40 5.945 5.920 5.969 VV 388036 9292669 2.24% 0.404% 41 5.974 5.969 5.985 VV 289610 2554594 0.62% 0.111% 42 6.007 5.985 6.030 VV 491473 9720341 2.35% 0.423% 43 6.054 6.030 6.067 VV 2653063 33108270 7.99% 1.439% 44 6.082 6.067 6.101 VV 3674241 48979770 11.82% 2.129% 45 6.119 6.101 6.188 VV 3692434 56092686 13.54% 2.439% 46 6.206 6.188 6.238 VV 452812 8232080 1.99% 0.358% 47 6.273 6.238 6.291 VV 2816447 36832971 8.89% 1.601% 48 6.307 6.291 6.357 VV 1957878 33715116 8.14% 1.466% 49 6.472 6.439 6.496 VV 563862 11031989 2.66% 0.480% 50 6.544 6.521 6.568 VV 737575 12072731 2.91% 0.525% 51 6.588 6.568 6.607 VV 539063 8523273 2.06% 0.371% 52 6.627 6.607 6.661 VV 1176573 17438450 4.21% 0.758% 53 6.746 6.716 6.772 VV 626921 12198789 2.94% 0.530% 54 6.788 6.772 6.817 VV 300714 6304680 1.52% 0.274% 55 6.851 6.817 6.876 VV 291840 7497138 1.81% 0.326% 56 6.906 6.876 6.948 VV 870874 15637150 3.77% 0.680% 57 7.018 6.996 7.046 VV 260615 5668291 1.37% 0.246% 58 7.079 7.046 7.099 VV 220190 4347599 1.05% 0.189% 59 7.120 7.099 7.137 PV 220790 3416859 0.82% 0.149% 60 7.142 7.137 7.146 VV 190375 1068436 0.26% 0.046% 61 7.173 7.146 7.211 VV 825468 14900001 3.60% 0.648% 62 7.216 7.211 7.225 VV 172807 1336375 0.32% 0.058% 63 7.317 7.225 7.338 VV 365399 13721027 3.31% 0.597% 64 7.344 7.338 7.358 VV 188430 2018407 0.49% 0.088% 65 7.366 7.358 7.371 VV 167982 1309827 0.32% 0.057% 66 7.393 7.371 7.410 VV 196335 3854113 0.93% 0.168% 67 7.456 7.410 7.466 VV 162423 4812982 1.16% 0.209% 68 7.521 7.466 7.526 VV 136529 4876994 1.18% 0.212% 69 7.608 7.526 7.638 VV 215302 10535546 2.54% 0.458% 70 7.641 7.638 7.646 VV 138662 581544 0.14% 0.025% 71 7.706 7.646 7.716 VV 165002 5948716 1.44% 0.259% 72 7.721 7.716 7.725 VV 138265 670132 0.16% 0.029% 73 7.793 7.725 7.797 VV 145465 5985935 1.44% 0.260% 74 7.851 7.797 7.863 VV 190572 5704390 1.38% 0.248% 75 7.915 7.863 7.937 VV 327141 8451551 2.04% 0.367% 76 7.976 7.937 7.981 VV 184494 4320451 1.04% 0.188% 77 8.018 7.981 8.028 VV 210901 5523411 1.33% 0.240% 78 8.032 8.028 8.036 VV 199363 907811 0.22% 0.039% 79 8.073 8.036 8.081 VV 194438 4997019 1.21% 0.217% 80 8.103 8.081 8.118 VV 204679 4073453 0.98% 0.177% 81 8.130 8.118 8.135 VV 192053 1889389 0.46% 0.082% 82 8.156 8.135 8.161 VV 179156 2718721 0.66% 0.118% 83 8.205 8.161 8.236 VV 254069 8706259 2.10% 0.379% 84 8.262 8.236 8.267 VV 195296 3334476 0.80% 0.145% 85 8.302 8.267 8.309 VV 159282 4016554 0.97% 0.175% 86 8.347 8.309 8.351 VV 160593 3625508 0.87% 0.158% 87 8.378 8.351 8.385 VV 168698 3040300 0.73% 0.132% 88 8.473 8.385 8.499 VV 382150 13691569 3.30% 0.595% 89 8.568 8.499 8.595 VV 331522 11222773 2.71% 0.488% 90 8.611 8.595 8.635 VV 189297 4128778 1.00% 0.180% 91 8.756 8.635 8.764 VV 158830 12255563 2.96% 0.533% 92 8.846 8.764 8.853 VV 193005 8494831 2.05% 0.369% 93 8.858 8.853 8.868 VV 176597 1376412 0.33% 0.060% 94 8.888 8.868 8.899 VV 165590 2856913 0.69% 0.124% 95 8.918 8.899 8.925 VV 166286 2362119 0.57% 0.103% 96 8.974 8.925 8.990 VV 167671 6193432 1.49% 0.269% 97 8.998 8.990 9.005 VV 149594 1260415 0.30% 0.055% 98 9.197 9.005 9.235 VV 331865 20373366 4.92% 0.886% 99 9.238 9.235 9.241 VV 119760 427796 0.10% 0.019% 100 9.278 9.241 9.286 VV 113077 2667590 0.64% 0.116% 101 9.356 9.286 9.363 VV 99396 4080487 0.98% 0.177% 102 9.367 9.363 9.395 VV 86713 1209373 0.29% 0.053% 103 9.484 9.395 9.556 VV 23878035 414386067 100.00% 18.016% 104 9.560 9.556 9.576 VV 80823 733470 0.18% 0.032% 105 9.581 9.576 9.585 VV 61143 300497 0.07% 0.013% 106 9.588 9.585 9.621 VB 54795 692242 0.17% 0.030% Sum of corrected areas: 2300111519 Signal #2 : ECD2B.CH 1 2.541 2.510 2.566 BV 259821 3501094 0.50% 0.058% 2 2.623 2.566 2.630 PV 135622 3748697 0.54% 0.062% 3 2.639 2.630 2.661 VV 144629 2284127 0.33% 0.038% 4 2.678 2.661 2.710 VV 184221 3966544 0.57% 0.066% 5 2.953 2.929 2.985 PV 1127310 13486598 1.94% 0.224% 6 3.073 3.048 3.131 BV 196495 4687712 0.68% 0.078% 7 3.282 3.253 3.318 PV 334692 4791141 0.69% 0.080% 8 3.349 3.318 3.463 VV 46850709 595176843 85.79% 9.879% 9 3.553 3.530 3.611 VV 2837295 41634445 6.00% 0.691% 10 3.635 3.611 3.678 VV 2719592 37199344 5.36% 0.617% 11 3.706 3.678 3.759 VV 8213503 106506791 15.35% 1.768% 12 3.795 3.759 3.816 VV 344608 8741485 1.26% 0.145% 13 3.863 3.827 3.901 VV 695868 18179232 2.62% 0.302% 14 3.989 3.966 4.040 VV 4588840 96096436 13.85% 1.595% 15 4.063 4.040 4.083 VV 913719 17557069 2.53% 0.291% 16 4.098 4.083 4.113 VV 569080 8756899 1.26% 0.145% 17 4.132 4.113 4.147 VV 1255855 17513943 2.52% 0.291% 18 4.170 4.147 4.206 VV 4239604 68854719 9.92% 1.143% 19 4.264 4.236 4.272 VV 2087709 26495901 3.82% 0.440% 20 4.280 4.272 4.296 VV 2099013 24928581 3.59% 0.414% 21 4.306 4.296 4.348 VV 1389874 25710096 3.71% 0.427% 22 4.396 4.348 4.432 VV 10160896 212984923 30.70% 3.535% 23 4.451 4.432 4.533 VV 5374669 101200230 14.59% 1.680% 24 4.565 4.533 4.589 PV 4881114 65653954 9.46% 1.090% 25 4.608 4.589 4.626 VV 3596465 49372564 7.12% 0.819% 26 4.646 4.626 4.664 VV 4197153 61330682 8.84% 1.018% 27 4.673 4.664 4.733 VV 2017925 41949225 6.05% 0.696% 28 4.811 4.775 4.833 VV 4739219 75570700 10.89% 1.254% 29 4.847 4.833 4.864 VV 2442314 34145894 4.92% 0.567% 30 4.879 4.864 4.910 VV 2135186 38496506 5.55% 0.639% 31 4.952 4.910 5.001 VV 5190479 123292219 17.77% 2.046% 32 5.019 5.001 5.059 VV 1840433 38933793 5.61% 0.646% 33 5.079 5.059 5.094 VV 890225 16376259 2.36% 0.272% 34 5.114 5.094 5.130 VV 3252690 44343266 6.39% 0.736% 35 5.148 5.130 5.168 VV 5848633 77145247 11.12% 1.280% 36 5.186 5.168 5.233 VV 5062094 83005997 11.96% 1.378% 37 5.291 5.260 5.319 VV 1523032 33083196 4.77% 0.549% 38 5.354 5.319 5.377 VV 3424346 63739635 9.19% 1.058% 39 5.395 5.377 5.440 VV 2975185 55644978 8.02% 0.924% 40 5.469 5.440 5.486 VV 867854 21606347 3.11% 0.359% 41 5.511 5.486 5.543 VV 1146192 28225675 4.07% 0.468% 42 5.593 5.561 5.621 VV 1491167 32573471 4.70% 0.541% 43 5.641 5.621 5.659 VV 1180880 20548194 2.96% 0.341% 44 5.679 5.659 5.716 VV 1999054 38336152 5.53% 0.636% 45 5.814 5.763 5.840 VV 1045567 36271484 5.23% 0.602% 46 5.855 5.840 5.881 VV 687308 15136287 2.18% 0.251% 47 5.903 5.881 5.939 VV 1513403 24198659 3.49% 0.402% 48 5.989 5.939 6.009 PV 823538 17550915 2.53% 0.291% 49 6.035 6.009 6.060 VV 547918 15250950 2.20% 0.253% 50 6.135 6.060 6.170 VV 642724 29890391 4.31% 0.496% 51 6.206 6.170 6.236 VV 1452268 29071608 4.19% 0.483% 52 6.253 6.236 6.277 VV 443275 9540828 1.38% 0.158% 53 6.307 6.277 6.326 VV 630403 14018608 2.02% 0.233% 54 6.340 6.326 6.375 VV 445156 11446275 1.65% 0.190% 55 6.392 6.375 6.408 VV 353595 6579625 0.95% 0.109% 56 6.453 6.408 6.466 VV 261694 8686989 1.25% 0.144% 57 6.472 6.466 6.494 VV 245551 3710001 0.53% 0.062% 58 6.565 6.509 6.569 VV 177680 6537198 0.94% 0.109% 59 6.596 6.569 6.618 VV 233121 5347770 0.77% 0.089% 60 6.632 6.618 6.654 VV 229352 3881697 0.56% 0.064% 61 6.683 6.666 6.715 VV 180575 3964420 0.57% 0.066% 62 6.737 6.715 6.743 VV 153189 2077463 0.30% 0.034% 63 6.762 6.743 6.768 VV 154728 1921177 0.28% 0.032% 64 6.772 6.768 6.784 VV 139685 1121766 0.16% 0.019% 65 6.838 6.784 6.866 VV 409668 9863730 1.42% 0.164% 66 7.030 6.866 7.054 VV 130871 10382972 1.50% 0.172% 67 7.076 7.054 7.085 VV 68402 884030 0.13% 0.015% 68 7.107 7.085 7.127 VV 129646 2010368 0.29% 0.033% 69 7.173 7.127 7.204 PV 262200 5407486 0.78% 0.090% 70 7.209 7.204 7.215 VV 77897 413804 0.06% 0.007% 71 7.280 7.215 7.284 VV 63986 2277214 0.33% 0.038% 72 7.292 7.284 7.303 VV 88185 662820 0.10% 0.011% 73 7.321 7.303 7.330 VV 78046 903211 0.13% 0.015% 74 7.368 7.330 7.408 VV 487820 7706853 1.11% 0.128% 75 7.432 7.408 7.438 VV 53797 633254 0.09% 0.011% 76 7.458 7.438 7.489 VV 314654 4301310 0.62% 0.071% 77 7.621 7.489 7.626 PV 62129 3837690 0.55% 0.064% 78 7.663 7.626 7.680 VV 141523 2724840 0.39% 0.045% 79 7.733 7.680 7.741 VV 135285 3767287 0.54% 0.063% 80 7.779 7.741 7.788 VV 121302 3236685 0.47% 0.054% 81 7.883 7.788 7.895 VV 222635 9049123 1.30% 0.150% 82 7.925 7.895 7.956 VV 587181 12225372 1.76% 0.203% 83 8.136 7.956 8.195 VV 48917218 693766354 100.00% 11.515% 84 8.261 8.195 8.274 VV 595468 26302200 3.79% 0.437% 85 8.279 8.274 8.284 VV 546868 3109155 0.45% 0.052% 86 8.577 8.284 8.582 VV 958680 136246501 19.64% 2.261% 87 8.793 8.582 8.797 VV 1264449 144715855 20.86% 2.402% 88 8.890 8.797 8.899 VV 1311152 77884702 11.23% 1.293% 89 9.074 8.899 9.081 VV 1500682 151673458 21.86% 2.517% 90 9.102 9.081 9.107 VV 1511685 22963481 3.31% 0.381% 91 9.135 9.107 9.139 VV 1490883 28676889 4.13% 0.476% 92 9.251 9.139 9.262 VV 1567672 111827871 16.12% 1.856% 93 9.333 9.262 9.338 VV 1598881 71085061 10.25% 1.180% 94 9.402 9.338 9.408 VV 1600895 66293711 9.56% 1.100% 95 9.418 9.408 9.426 VV 1607104 17659283 2.55% 0.293% 96 9.434 9.426 9.445 VV 1628813 17997813 2.59% 0.299% 97 9.473 9.445 9.483 VV 1641378 36398577 5.25% 0.604% 98 9.518 9.483 9.523 VV 1675929 39273367 5.66% 0.652% 99 9.546 9.523 9.551 VV 1659483 27457745 3.96% 0.456% 100 9.592 9.551 9.600 VV 1695467 48450225 6.98% 0.804% 101 9.607 9.600 9.612 VV 1672847 12225486 1.76% 0.203% 102 9.710 9.612 9.715 VV 1683328 102474339 14.77% 1.701% 103 9.751 9.715 9.758 VV 1658560 42865398 6.18% 0.711% 104 9.818 9.758 9.823 VV 1703174 64746904 9.33% 1.075% 105 9.829 9.823 9.833 VV 1715657 10345001 1.49% 0.172% 106 9.841 9.833 9.846 VV 1685321 13242419 1.91% 0.220% 107 9.853 9.846 9.857 VV 1667271 11196706 1.61% 0.186% 108 9.862 9.857 9.865 VV 1675584 7109440 1.02% 0.118% 109 9.877 9.865 9.881 VV 1676456 16413352 2.37% 0.272% 110 9.886 9.881 9.890 VV 1653393 8208920 1.18% 0.136% 111 9.894 9.890 9.900 VV 1648094 10352548 1.49% 0.172% 112 9.915 9.900 9.922 VV 1629169 21081735 3.04% 0.350% 113 9.938 9.922 9.942 VV 1639882 19976473 2.88% 0.332% 114 10.006 9.942 10.012 VV 1655066 68016662 9.80% 1.129% 115 10.028 10.012 10.033 VV 1651305 20405288 2.94% 0.339% 116 10.064 10.033 10.071 VV 1664128 37680177 5.43% 0.625% 117 10.083 10.071 10.088 VV 1649450 16757821 2.42% 0.278% 118 10.095 10.088 10.100 VV 1640936 11416854 1.65% 0.189% 119 10.109 10.100 10.128 VV 1636803 25315699 3.65% 0.420% 120 10.192 10.128 10.196 VV 1608163 63147394 9.10% 1.048% 121 10.209 10.196 10.225 VV 1597686 26720354 3.85% 0.444% 122 10.337 10.225 10.344 VV 1545660 110434910 15.92% 1.833% 123 10.356 10.344 10.378 VV 1531301 30179941 4.35% 0.501% 124 10.392 10.378 10.401 VV 1527864 20389667 2.94% 0.338% 125 10.415 10.401 10.445 VV 1509471 38605992 5.56% 0.641% 126 10.457 10.445 10.463 VV 1460309 15482143 2.23% 0.257% 127 10.469 10.463 10.484 VV 1447401 18236787 2.63% 0.303% 128 10.510 10.484 10.515 VV 1433161 25737238 3.71% 0.427% 129 10.520 10.515 10.524 VV 1425316 8334712 1.20% 0.138% 130 10.542 10.524 10.555 VV 1398045 25643137 3.70% 0.426% 131 10.587 10.555 10.594 VV 1354923 31271665 4.51% 0.519% 132 10.630 10.594 10.661 VV 1331685 51875064 7.48% 0.861% 133 10.664 10.661 10.684 VV 1295821 17571691 2.53% 0.292% 134 10.689 10.684 10.700 VV 1268716 11412303 1.64% 0.189% 135 10.806 10.732 10.826 VV 1168769 65318504 9.42% 1.084% 136 10.988 10.826 11.000 VV 1041209 111571731 16.08% 1.852% 137 11.071 11.000 11.090 VV 987929 52243376 7.53% 0.867% 138 11.173 11.090 11.183 VV 894718 49914998 7.19% 0.828% 139 11.378 11.183 11.404 VV 691938 100784181 14.53% 1.673% 140 11.415 11.404 11.438 VV 632912 12293698 1.77% 0.204% 141 11.483 11.438 11.515 VV 564827 24761488 3.57% 0.411% 142 11.581 11.515 11.608 VV 445986 24267298 3.50% 0.403% 143 11.625 11.608 11.643 VV 392542 7354755 1.06% 0.122% 144 11.664 11.643 11.685 VV 345774 7867800 1.13% 0.131% 145 11.707 11.685 11.733 VV 280818 7044654 1.02% 0.117% 146 11.772 11.733 11.785 VV 196872 5554195 0.80% 0.092% 147 11.823 11.785 11.841 VV 123927 3897499 0.56% 0.065% 148 11.868 11.841 11.894 VV 77696 1383623 0.20% 0.023% Sum of corrected areas: 6024783235