Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO022118\ Data File : PO042526.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 20 Feb 2018 22:12 Sample : AR1268ICC500 Misc : ALS Vial : 14 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.162 3.140 3.183 PV 195963 2235013 0.14% 0.038% 2 3.224 3.201 3.248 VV 890465 8703658 0.54% 0.147% 3 3.476 3.426 3.507 PV 75922 2017301 0.12% 0.034% 4 3.611 3.507 3.631 VV 202232 9393150 0.58% 0.158% 5 3.648 3.631 3.686 VV 191171 4868715 0.30% 0.082% 6 3.718 3.686 3.744 VV 158724 4634216 0.29% 0.078% 7 3.790 3.756 3.820 VV 146292 4356709 0.27% 0.073% 8 3.873 3.850 3.936 VV 131954 4461385 0.28% 0.075% 9 4.101 4.063 4.209 BV 38433227 423658769 26.12% 7.138% 10 4.394 4.360 4.468 VV 488456 6930142 0.43% 0.117% 11 4.560 4.521 4.577 PV 95724 1903150 0.12% 0.032% 12 4.595 4.577 4.623 VV 99395 1264183 0.08% 0.021% 13 4.971 4.943 4.991 PV 120246 1860370 0.11% 0.031% 14 5.038 5.004 5.050 VV 143283 3052087 0.19% 0.051% 15 5.069 5.050 5.118 VV 303476 7009611 0.43% 0.118% 16 5.173 5.118 5.210 VV 1106169 18482847 1.14% 0.311% 17 5.228 5.210 5.239 VV 272188 4010434 0.25% 0.068% 18 5.250 5.239 5.289 VV 297104 6557010 0.40% 0.110% 19 5.308 5.289 5.343 VV 281470 6331792 0.39% 0.107% 20 5.405 5.343 5.446 VV 267187 11514691 0.71% 0.194% 21 5.492 5.474 5.511 VV 302358 5793768 0.36% 0.098% 22 5.537 5.511 5.561 VV 340462 8647712 0.53% 0.146% 23 5.583 5.561 5.608 VV 364310 8928698 0.55% 0.150% 24 5.684 5.608 5.757 VV 892484 40851283 2.52% 0.688% 25 5.830 5.796 5.859 PV 293483 7402962 0.46% 0.125% 26 5.889 5.859 5.911 VV 228390 6406013 0.39% 0.108% 27 5.930 5.911 5.947 VV 184977 3748561 0.23% 0.063% 28 6.002 5.947 6.029 VV 192057 7838581 0.48% 0.132% 29 6.081 6.029 6.104 VV 479843 12853087 0.79% 0.217% 30 6.119 6.104 6.168 VV 323463 5135791 0.32% 0.087% 31 6.273 6.243 6.290 PV 274696 3701505 0.23% 0.062% 32 6.310 6.290 6.346 VV 229822 4842228 0.30% 0.082% 33 6.504 6.459 6.528 VV 129759 4274957 0.26% 0.072% 34 6.541 6.528 6.574 VV 131098 2652096 0.16% 0.045% 35 6.626 6.600 6.644 VV 262920 4217369 0.26% 0.071% 36 6.684 6.654 6.719 VV 172421 4659520 0.29% 0.079% 37 6.748 6.719 6.766 VV 176103 3922255 0.24% 0.066% 38 6.905 6.873 6.929 VV 265338 5546647 0.34% 0.093% 39 7.039 7.024 7.069 VV 251483 4821110 0.30% 0.081% 40 7.121 7.097 7.143 PV 701242 9342763 0.58% 0.157% 41 7.173 7.143 7.219 VV 310977 8196774 0.51% 0.138% 42 7.268 7.219 7.279 VV 126037 3963942 0.24% 0.067% 43 7.306 7.279 7.336 VV 409160 7484623 0.46% 0.126% 44 7.393 7.336 7.427 VV 10152281 129483825 7.98% 2.182% 45 7.449 7.427 7.479 VV 750365 10694012 0.66% 0.180% 46 7.484 7.479 7.489 VV 100007 588379 0.04% 0.010% 47 7.498 7.489 7.503 VV 107965 761407 0.05% 0.013% 48 7.578 7.549 7.596 VV 494709 7406784 0.46% 0.125% 49 7.633 7.596 7.674 VV 13038978 168564631 10.39% 2.840% 50 7.716 7.674 7.757 VV 3682374 50491374 3.11% 0.851% 51 7.797 7.757 7.818 VV 308392 6737376 0.42% 0.114% 52 7.842 7.818 7.867 VV 196035 4489995 0.28% 0.076% 53 7.914 7.867 7.939 VV 5738540 73476986 4.53% 1.238% 54 7.960 7.939 7.988 VV 3156344 39782746 2.45% 0.670% 55 8.011 7.988 8.019 VV 205257 3636301 0.22% 0.061% 56 8.061 8.019 8.086 VV 213536 7756858 0.48% 0.131% 57 8.190 8.086 8.228 VV 54845668 714972192 44.08% 12.046% 58 8.272 8.228 8.347 VV 43051578 636784756 39.26% 10.728% 59 8.356 8.347 8.377 VV 219330 3645049 0.22% 0.061% 60 8.403 8.377 8.415 VV 206637 4414226 0.27% 0.074% 61 8.472 8.415 8.533 VV 39373057 547651528 33.76% 9.227% 62 8.570 8.533 8.596 VV 10370933 147729908 9.11% 2.489% 63 8.605 8.596 8.649 VV 1030991 16497137 1.02% 0.278% 64 8.841 8.750 8.889 VV 16318825 255738136 15.77% 4.309% 65 8.920 8.889 8.941 VV 261158 6832844 0.42% 0.115% 66 8.996 8.941 9.013 VV 224630 8495420 0.52% 0.143% 67 9.075 9.013 9.079 VV 163325 6399186 0.39% 0.108% 68 9.092 9.079 9.108 VV 163181 2586026 0.16% 0.044% 69 9.138 9.108 9.144 VV 151219 3016452 0.19% 0.051% 70 9.198 9.144 9.304 VV 106339830 1621963761 100.00% 27.327% 71 9.309 9.304 9.339 VV 143064 2427335 0.15% 0.041% 72 9.346 9.339 9.351 VV 114395 721846 0.04% 0.012% 73 9.364 9.351 9.377 VV 105921 1410142 0.09% 0.024% 74 9.484 9.377 9.564 VV 44220548 740149823 45.63% 12.470% 75 9.570 9.564 9.600 VB 44262 548159 0.03% 0.009% 76 10.171 10.099 10.181 PV 45121 1147239 0.07% 0.019% Sum of corrected areas: 5935479319 Signal #2 : ECD2B.CH 1 2.539 2.506 2.568 BV 167303 1468130 0.05% 0.011% 2 3.348 3.311 3.489 VV 49594582 629294526 21.58% 4.866% 3 3.633 3.601 3.678 VV 759785 12757737 0.44% 0.099% 4 3.795 3.748 3.825 PV 212742 4565874 0.16% 0.035% 5 3.835 3.825 3.841 VV 118598 858296 0.03% 0.007% 6 3.884 3.841 3.891 VV 117580 3047917 0.10% 0.024% 7 3.899 3.891 3.928 VV 106645 1668426 0.06% 0.013% 8 3.992 3.963 3.998 VV 91656 1295667 0.04% 0.010% 9 4.008 3.998 4.045 VB 82760 1109224 0.04% 0.009% 10 4.171 4.150 4.185 VV 172345 2765843 0.09% 0.021% 11 4.264 4.209 4.303 VV 1523302 28928153 0.99% 0.224% 12 4.395 4.341 4.436 VV 611274 24312899 0.83% 0.188% 13 4.451 4.436 4.533 VV 498903 21026595 0.72% 0.163% 14 4.568 4.533 4.586 PV 372849 7757070 0.27% 0.060% 15 4.610 4.586 4.626 VV 392896 7630471 0.26% 0.059% 16 4.644 4.626 4.666 VV 307049 5980723 0.21% 0.046% 17 4.672 4.666 4.697 VB 142853 1675902 0.06% 0.013% 18 4.810 4.774 4.838 BV 275721 5255335 0.18% 0.041% 19 4.848 4.838 4.864 VV 177898 2318710 0.08% 0.018% 20 4.879 4.864 4.894 VV 188184 2757533 0.09% 0.021% 21 4.959 4.894 5.048 VV 710830 28112713 0.96% 0.217% 22 5.114 5.086 5.129 VV 271648 4736768 0.16% 0.037% 23 5.148 5.129 5.165 VV 481713 6512993 0.22% 0.050% 24 5.186 5.165 5.210 VV 403268 6310274 0.22% 0.049% 25 5.292 5.274 5.308 VV 234594 3840407 0.13% 0.030% 26 5.354 5.308 5.379 VV 421073 10884996 0.37% 0.084% 27 5.395 5.379 5.416 VV 356663 6343296 0.22% 0.049% 28 5.471 5.416 5.486 VV 336713 10498808 0.36% 0.081% 29 5.492 5.486 5.498 VV 286221 1921415 0.07% 0.015% 30 5.515 5.498 5.529 VV 313262 5389822 0.18% 0.042% 31 5.596 5.572 5.617 VV 372434 8126601 0.28% 0.063% 32 5.638 5.617 5.662 VV 364995 8655837 0.30% 0.067% 33 5.679 5.662 5.726 VV 486001 13826259 0.47% 0.107% 34 5.800 5.763 5.840 VV 408279 15274633 0.52% 0.118% 35 5.860 5.840 5.872 VV 340084 6152381 0.21% 0.048% 36 5.902 5.872 5.944 VV 473526 11867164 0.41% 0.092% 37 5.989 5.944 6.030 PV 620704 15592918 0.53% 0.121% 38 6.043 6.030 6.051 VV 277965 3371450 0.12% 0.026% 39 6.058 6.051 6.066 VV 266144 2309293 0.08% 0.018% 40 6.082 6.066 6.093 VV 274175 4056126 0.14% 0.031% 41 6.097 6.093 6.102 VV 238139 1344114 0.05% 0.010% 42 6.136 6.102 6.178 VV 1202606 22358458 0.77% 0.173% 43 6.206 6.178 6.231 VV 515116 10475145 0.36% 0.081% 44 6.253 6.231 6.286 VV 645694 11826133 0.41% 0.091% 45 6.342 6.286 6.379 VV 18003195 237766394 8.15% 1.838% 46 6.395 6.379 6.431 VV 1278629 19725560 0.68% 0.153% 47 6.457 6.431 6.461 VV 173011 2732913 0.09% 0.021% 48 6.530 6.500 6.557 VV 775474 11042482 0.38% 0.085% 49 6.585 6.557 6.644 VV 23420781 302466720 10.37% 2.339% 50 6.672 6.644 6.719 VV 6239975 82990981 2.85% 0.642% 51 6.751 6.719 6.793 VV 367261 6970575 0.24% 0.054% 52 6.836 6.793 6.903 VV 10070141 130181116 4.46% 1.007% 53 6.935 6.903 6.973 VV 5079482 66112959 2.27% 0.511% 54 6.979 6.973 6.997 VV 107489 1262569 0.04% 0.010% 55 7.034 6.997 7.056 VV 127752 3062582 0.11% 0.024% 56 7.108 7.056 7.146 PV 104677594 1362121809 46.70% 10.532% 57 7.174 7.146 7.284 VV 93373445 1224388560 41.98% 9.467% 58 7.314 7.284 7.332 VV 182360 5199928 0.18% 0.040% 59 7.367 7.332 7.427 VV 80607080 1032273364 35.39% 7.981% 60 7.457 7.427 7.504 VV 19743016 257858280 8.84% 1.994% 61 7.529 7.504 7.559 VV 1545189 22778268 0.78% 0.176% 62 7.571 7.559 7.578 VV 139403 1291272 0.04% 0.010% 63 7.582 7.578 7.587 VV 132487 560385 0.02% 0.004% 64 7.610 7.587 7.617 VV 105459 1488558 0.05% 0.012% 65 7.661 7.617 7.738 VV 33174856 440120263 15.09% 3.403% 66 7.770 7.738 7.793 VV 232097 6511837 0.22% 0.050% 67 7.828 7.793 7.846 VV 361585 8954510 0.31% 0.069% 68 7.924 7.846 8.028 VV 223018988 2916706239 100.00% 22.552% 69 8.040 8.028 8.055 VV 625632 9775235 0.34% 0.076% 70 8.136 8.055 8.222 VV 93048881 1277085807 43.79% 9.874% 71 8.405 8.222 8.409 VV 734997 70477744 2.42% 0.545% 72 8.490 8.409 8.495 VV 795058 38889383 1.33% 0.301% 73 8.642 8.495 8.652 VV 1051404 85490652 2.93% 0.661% 74 8.735 8.652 8.742 VV 1141920 57046391 1.96% 0.441% 75 8.812 8.742 8.819 VV 1231965 53824126 1.85% 0.416% 76 8.853 8.819 8.858 VV 1244371 28324737 0.97% 0.219% 77 8.925 8.858 8.929 VV 1278214 53461881 1.83% 0.413% 78 8.993 8.929 8.998 VV 1349211 53667463 1.84% 0.415% 79 9.019 8.998 9.026 VV 1344646 22613953 0.78% 0.175% 80 9.063 9.026 9.067 VV 1410935 33529537 1.15% 0.259% 81 9.088 9.067 9.094 VV 1421353 22405862 0.77% 0.173% 82 9.106 9.094 9.114 VV 1432309 17228388 0.59% 0.133% 83 9.128 9.114 9.134 VV 1441350 17114473 0.59% 0.132% 84 9.167 9.134 9.179 VV 1493249 39397141 1.35% 0.305% 85 9.195 9.179 9.204 VV 1501429 22256989 0.76% 0.172% 86 9.213 9.204 9.231 VV 1509074 23645340 0.81% 0.183% 87 9.248 9.231 9.253 VV 1523543 19716822 0.68% 0.152% 88 9.256 9.253 9.261 VV 1516039 7112180 0.24% 0.055% 89 9.314 9.261 9.335 VV 1550239 67585166 2.32% 0.523% 90 9.370 9.335 9.378 VV 1564840 39143271 1.34% 0.303% 91 9.395 9.378 9.409 VV 1563991 28897114 0.99% 0.223% 92 9.450 9.409 9.456 VV 1586349 44166869 1.51% 0.341% 93 9.470 9.456 9.475 VV 1573164 17180184 0.59% 0.133% 94 9.486 9.475 9.491 VV 1570474 15151373 0.52% 0.117% 95 9.546 9.491 9.551 VV 1643536 57894529 1.98% 0.448% 96 9.640 9.551 9.648 VV 1649740 94145024 3.23% 0.728% 97 9.653 9.648 9.663 VV 1629369 14662610 0.50% 0.113% 98 9.666 9.663 9.669 VV 1632279 6118788 0.21% 0.047% 99 9.676 9.669 9.684 VV 1642433 14538276 0.50% 0.112% 100 9.702 9.684 9.719 VV 1648725 34084981 1.17% 0.264% 101 9.735 9.719 9.754 VV 1659604 33893317 1.16% 0.262% 102 9.805 9.754 9.809 VV 1638995 52459259 1.80% 0.406% 103 9.832 9.809 9.838 VV 1646168 28791339 0.99% 0.223% 104 9.891 9.838 9.901 VV 1653169 60315750 2.07% 0.466% 105 9.905 9.901 9.909 VV 1633653 8150061 0.28% 0.063% 106 9.943 9.909 9.949 VV 1622980 38697059 1.33% 0.299% 107 9.967 9.949 9.972 VV 1614745 22010072 0.75% 0.170% 108 9.977 9.972 9.980 VV 1623607 7687394 0.26% 0.059% 109 9.987 9.980 9.993 VV 1630604 11970132 0.41% 0.093% 110 10.059 9.993 10.070 VV 1612759 74033419 2.54% 0.572% 111 10.077 10.070 10.091 VV 1613078 19831944 0.68% 0.153% 112 10.104 10.091 10.112 VV 1584749 20146857 0.69% 0.156% 113 10.135 10.112 10.139 VV 1589860 25147387 0.86% 0.194% 114 10.146 10.139 10.152 VV 1582318 11469594 0.39% 0.089% 115 10.183 10.152 10.193 VV 1577573 38542170 1.32% 0.298% 116 10.200 10.193 10.204 VV 1554905 10054329 0.34% 0.078% 117 10.226 10.204 10.231 VV 1533739 25144948 0.86% 0.194% 118 10.248 10.231 10.254 VV 1528367 20623731 0.71% 0.159% 119 10.263 10.254 10.268 VV 1537701 12507155 0.43% 0.097% 120 10.293 10.268 10.303 VV 1530814 31578878 1.08% 0.244% 121 10.335 10.303 10.353 VV 1540907 45365642 1.56% 0.351% 122 10.372 10.353 10.378 VV 1501160 22342037 0.77% 0.173% 123 10.390 10.378 10.401 VV 1517329 20687767 0.71% 0.160% 124 10.406 10.401 10.423 VV 1498652 19389897 0.66% 0.150% 125 10.483 10.423 10.501 VV 1460833 67755548 2.32% 0.524% 126 10.504 10.501 10.513 VV 1433841 10402589 0.36% 0.080% 127 10.528 10.513 10.533 VV 1398020 16197964 0.56% 0.125% 128 10.552 10.533 10.560 VV 1389316 21914483 0.75% 0.169% 129 10.570 10.560 10.576 VV 1357714 13264185 0.45% 0.103% 130 10.663 10.576 10.668 VV 1297143 72578515 2.49% 0.561% 131 10.672 10.668 10.714 VV 1275960 33820623 1.16% 0.261% 132 10.728 10.714 10.733 VV 1226431 13766102 0.47% 0.106% 133 10.764 10.733 10.769 VV 1228457 26167155 0.90% 0.202% 134 10.801 10.769 10.806 VV 1193557 25984188 0.89% 0.201% 135 10.822 10.806 10.857 VV 1176738 35099008 1.20% 0.271% 136 10.898 10.857 10.906 VV 1136044 32586449 1.12% 0.252% 137 10.951 10.906 10.963 VV 1121926 37151929 1.27% 0.287% 138 11.194 10.963 11.202 VV 893784 138747654 4.76% 1.073% 139 11.298 11.202 11.306 VV 773745 50005293 1.71% 0.387% 140 11.339 11.306 11.351 VV 744671 19567408 0.67% 0.151% 141 11.401 11.351 11.415 VV 681080 25946506 0.89% 0.201% 142 11.514 11.415 11.546 VV 564475 44056594 1.51% 0.341% 143 11.581 11.546 11.601 VV 496548 15366400 0.53% 0.119% 144 11.615 11.601 11.646 VV 429426 10733296 0.37% 0.083% 145 11.714 11.646 11.749 VV 331641 20296253 0.70% 0.157% 146 11.786 11.749 11.796 VV 249432 6605447 0.23% 0.051% 147 11.983 11.796 11.991 VBA 59106 17125346 0.59% 0.132% Sum of corrected areas: 12933442524