Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO022118\ Data File : PO042527.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 20 Feb 2018 22:27 Sample : PO022118ICV500 Misc : ALS Vial : 15 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.162 3.131 3.206 VV 214811 3116160 0.49% 0.039% 2 3.224 3.206 3.248 PV 530727 5246586 0.83% 0.066% 3 3.558 3.509 3.571 VV 244263 5659189 0.90% 0.071% 4 3.607 3.571 3.648 VV 345725 11567469 1.83% 0.146% 5 3.669 3.648 3.687 VV 231279 4573672 0.72% 0.058% 6 3.703 3.687 3.728 VV 250518 5627584 0.89% 0.071% 7 3.735 3.728 3.763 VV 245868 4740375 0.75% 0.060% 8 3.793 3.763 3.826 VV 271131 8892895 1.41% 0.112% 9 3.884 3.839 3.900 VV 287915 9330386 1.48% 0.118% 10 4.101 4.056 4.213 VV 40335611 455352729 72.13% 5.752% 11 4.298 4.267 4.351 VV 1155343 19661840 3.11% 0.248% 12 4.386 4.360 4.422 VV 1873229 25367482 4.02% 0.320% 13 4.458 4.422 4.522 VV 7719045 94454182 14.96% 1.193% 14 4.604 4.574 4.649 VV 1156212 15270617 2.42% 0.193% 15 4.783 4.718 4.799 VV 10985274 119896273 18.99% 1.515% 16 4.812 4.799 4.849 VV 6284202 71817897 11.38% 0.907% 17 4.868 4.849 4.885 VV 1294212 15100161 2.39% 0.191% 18 4.897 4.885 4.907 VV 524312 5182464 0.82% 0.065% 19 4.919 4.907 4.943 VV 776668 8419984 1.33% 0.106% 20 4.968 4.943 5.005 PV 10803571 119989050 19.01% 1.516% 21 5.079 5.052 5.107 VV 405260 6653052 1.05% 0.084% 22 5.132 5.107 5.147 VV 3164812 35069199 5.56% 0.443% 23 5.160 5.147 5.197 VV 2204883 33183434 5.26% 0.419% 24 5.227 5.197 5.236 VV 16357787 170666327 27.04% 2.156% 25 5.248 5.236 5.285 VV 20734862 269122226 42.63% 3.400% 26 5.308 5.285 5.373 VV 12527307 166283646 26.34% 2.101% 27 5.404 5.373 5.445 VV 11068847 137929280 21.85% 1.742% 28 5.468 5.445 5.473 VV 1125758 11308332 1.79% 0.143% 29 5.493 5.473 5.516 VV 8198885 100818496 15.97% 1.274% 30 5.537 5.516 5.563 VV 7223162 114605352 18.15% 1.448% 31 5.573 5.563 5.620 VV 3847441 48839403 7.74% 0.617% 32 5.690 5.620 5.714 VV 10209284 142696613 22.60% 1.803% 33 5.729 5.714 5.753 VV 4629925 59936264 9.49% 0.757% 34 5.774 5.753 5.796 VV 3699770 42493785 6.73% 0.537% 35 5.827 5.796 5.869 PV 9113827 136878327 21.68% 1.729% 36 5.891 5.869 5.918 VV 3019964 36734593 5.82% 0.464% 37 5.925 5.918 5.928 VV 188818 1084641 0.17% 0.014% 38 5.945 5.928 5.968 VV 477955 7263456 1.15% 0.092% 39 6.006 5.968 6.029 VV 616201 10900297 1.73% 0.138% 40 6.057 6.029 6.072 VV 9566684 119091920 18.87% 1.504% 41 6.081 6.072 6.101 VV 4434112 50553782 8.01% 0.639% 42 6.119 6.101 6.184 VV 3104632 45755422 7.25% 0.578% 43 6.207 6.184 6.239 VV 1148724 14587312 2.31% 0.184% 44 6.270 6.239 6.297 PV 8818214 104960777 16.63% 1.326% 45 6.311 6.297 6.353 VV 451121 8619723 1.37% 0.109% 46 6.471 6.436 6.519 VV 319017 5215685 0.83% 0.066% 47 6.543 6.519 6.554 VV 1577580 17444115 2.76% 0.220% 48 6.571 6.554 6.601 VV 3627677 45572067 7.22% 0.576% 49 6.626 6.601 6.657 VV 4387818 52971871 8.39% 0.669% 50 6.685 6.657 6.722 VV 11272481 173383640 27.47% 2.190% 51 6.736 6.722 6.760 VV 3011973 36293117 5.75% 0.458% 52 6.788 6.760 6.833 VV 21500066 255461666 40.47% 3.227% 53 6.906 6.876 6.936 PV 2977743 37946242 6.01% 0.479% 54 6.972 6.936 7.003 VV 4151357 52261124 8.28% 0.660% 55 7.040 7.003 7.063 VV 28227207 337258935 53.43% 4.260% 56 7.080 7.063 7.100 VV 7874583 91897429 14.56% 1.161% 57 7.120 7.100 7.142 VV 6081608 75841796 12.01% 0.958% 58 7.165 7.142 7.185 VV 12175482 145960900 23.12% 1.844% 59 7.195 7.185 7.234 VV 2442463 29611374 4.69% 0.374% 60 7.271 7.234 7.286 VV 2498137 38238381 6.06% 0.483% 61 7.315 7.286 7.338 VV 28326398 383772898 60.79% 4.848% 62 7.346 7.338 7.368 VV 4037191 51307724 8.13% 0.648% 63 7.393 7.368 7.423 VV 22370836 274303703 43.45% 3.465% 64 7.449 7.423 7.496 VV 11533075 139616047 22.12% 1.764% 65 7.579 7.515 7.590 PV 4260430 51124681 8.10% 0.646% 66 7.613 7.590 7.662 VV 19785481 276007785 43.72% 3.487% 67 7.690 7.662 7.724 VV 10361752 140201890 22.21% 1.771% 68 7.742 7.724 7.776 VV 5106193 65120168 10.32% 0.823% 69 7.799 7.776 7.818 VV 1058962 13480007 2.14% 0.170% 70 7.844 7.818 7.875 VV 6006289 78603406 12.45% 0.993% 71 7.914 7.875 7.943 VV 51605107 631268810 100.00% 7.974% 72 7.961 7.943 8.018 VV 2946719 41114391 6.51% 0.519% 73 8.199 8.126 8.226 VV 23121664 387622401 61.40% 4.897% 74 8.255 8.226 8.263 VV 9229538 135527065 21.47% 1.712% 75 8.268 8.263 8.333 VV 8902154 111995271 17.74% 1.415% 76 8.472 8.365 8.503 VV 871308 20064667 3.18% 0.253% 77 8.508 8.503 8.513 VV 138026 722849 0.11% 0.009% 78 8.551 8.513 8.580 VV 826592 20720853 3.28% 0.262% 79 8.605 8.580 8.650 VV 5294580 76547417 12.13% 0.967% 80 8.841 8.758 8.885 VV 12068337 183274648 29.03% 2.315% 81 8.919 8.885 8.953 VV 738819 14339575 2.27% 0.181% 82 8.961 8.953 8.969 VV 150791 1267983 0.20% 0.016% 83 8.996 8.969 9.004 VV 143470 2721528 0.43% 0.034% 84 9.036 9.004 9.041 VV 128103 2513474 0.40% 0.032% 85 9.052 9.041 9.059 VV 129431 1280063 0.20% 0.016% 86 9.111 9.059 9.123 VV 117894 4352921 0.69% 0.055% 87 9.196 9.123 9.237 VV 2949612 51535383 8.16% 0.651% 88 9.258 9.237 9.285 VV 115979 2834466 0.45% 0.036% 89 9.291 9.285 9.321 VV 96528 1599957 0.25% 0.020% 90 9.369 9.321 9.386 VV 92324 2636878 0.42% 0.033% 91 9.485 9.386 9.569 VV 27098402 467059634 73.99% 5.900% 92 9.575 9.569 9.579 VV 52200 240807 0.04% 0.003% 93 9.593 9.579 9.598 VV 53869 406500 0.06% 0.005% 94 9.607 9.598 9.614 VV 30610 251398 0.04% 0.003% 95 9.634 9.614 9.640 VV 34224 212916 0.03% 0.003% Sum of corrected areas: 7916311158 Signal #2 : ECD2B.CH 1 2.540 2.506 2.586 BV 217886 3104469 0.24% 0.020% 2 2.678 2.660 2.701 VV 215146 3923783 0.30% 0.025% 3 2.866 2.838 2.903 PV 270230 7876865 0.61% 0.050% 4 2.910 2.903 2.934 VV 239548 4084863 0.32% 0.026% 5 2.951 2.934 2.975 VV 284789 6002982 0.46% 0.038% 6 2.997 2.975 3.028 VV 320384 7621589 0.59% 0.049% 7 3.348 3.316 3.474 VV 52717609 680411386 52.67% 4.337% 8 3.494 3.474 3.499 VV 217425 3095695 0.24% 0.020% 9 3.503 3.499 3.511 VV 210752 1395213 0.11% 0.009% 10 3.552 3.527 3.611 VV 1977413 31499909 2.44% 0.201% 11 3.634 3.611 3.676 VV 2795750 38299514 2.96% 0.244% 12 3.705 3.676 3.755 VV 10415952 131922493 10.21% 0.841% 13 3.793 3.755 3.821 VV 304603 8731116 0.68% 0.056% 14 3.862 3.821 3.936 VV 1543082 29991262 2.32% 0.191% 15 3.989 3.963 4.043 VV 14816933 282974687 21.91% 1.804% 16 4.064 4.043 4.083 VV 1943022 27249260 2.11% 0.174% 17 4.097 4.083 4.114 VV 989142 13047159 1.01% 0.083% 18 4.131 4.114 4.144 VV 1408032 16933866 1.31% 0.108% 19 4.170 4.144 4.206 VV 13281774 196305416 15.20% 1.251% 20 4.216 4.206 4.244 VV 807920 13280147 1.03% 0.085% 21 4.281 4.244 4.296 VV 4948561 72565240 5.62% 0.463% 22 4.306 4.296 4.344 VV 3338811 45553309 3.53% 0.290% 23 4.395 4.344 4.431 VV 33428065 665710088 51.53% 4.243% 24 4.451 4.431 4.534 VV 16694202 273576730 21.18% 1.744% 25 4.564 4.534 4.588 PV 15889495 200965767 15.56% 1.281% 26 4.607 4.588 4.626 VV 12607981 159124939 12.32% 1.014% 27 4.645 4.626 4.664 VV 14451364 195989017 15.17% 1.249% 28 4.673 4.664 4.771 VV 5868613 91861018 7.11% 0.586% 29 4.810 4.771 4.832 VV 15800253 213998583 16.57% 1.364% 30 4.847 4.832 4.864 VV 6802752 86506988 6.70% 0.551% 31 4.879 4.864 4.908 VV 5759973 78772632 6.10% 0.502% 32 4.950 4.908 4.986 VV 13879347 245118884 18.97% 1.562% 33 5.019 4.986 5.052 VV 4479344 74445837 5.76% 0.475% 34 5.079 5.052 5.094 VV 940937 16483006 1.28% 0.105% 35 5.114 5.094 5.127 VV 4156460 50263570 3.89% 0.320% 36 5.147 5.127 5.171 VV 16809125 215788053 16.70% 1.376% 37 5.186 5.171 5.208 VV 4284567 56865220 4.40% 0.362% 38 5.215 5.208 5.221 VV 1034718 7679452 0.59% 0.049% 39 5.236 5.221 5.264 VV 1823809 26961922 2.09% 0.172% 40 5.291 5.264 5.327 VV 12374630 158259398 12.25% 1.009% 41 5.353 5.327 5.361 VV 878861 12919651 1.00% 0.082% 42 5.375 5.361 5.431 VV 1265265 24418183 1.89% 0.156% 43 5.463 5.444 5.490 VV 192228 3574433 0.28% 0.023% 44 5.511 5.490 5.549 VV 489348 6956971 0.54% 0.044% 45 5.592 5.566 5.627 VV 2416504 29833417 2.31% 0.190% 46 5.656 5.627 5.665 VV 5619551 62680137 4.85% 0.400% 47 5.691 5.665 5.713 VV 20119975 311434087 24.11% 1.985% 48 5.732 5.713 5.775 VV 6859805 129011809 9.99% 0.822% 49 5.804 5.775 5.847 VV 35512310 443913433 34.36% 2.830% 50 5.864 5.847 5.882 VV 641067 8750125 0.68% 0.056% 51 5.903 5.882 5.913 VV 2505653 27815681 2.15% 0.177% 52 5.932 5.913 5.962 VV 7492757 98528590 7.63% 0.628% 53 5.990 5.962 6.067 VV 48557669 618212133 47.86% 3.941% 54 6.136 6.096 6.184 BV 41046047 529773675 41.01% 3.377% 55 6.209 6.184 6.231 VV 4302697 56067791 4.34% 0.357% 56 6.254 6.231 6.278 VV 11467531 150274547 11.63% 0.958% 57 6.306 6.278 6.325 VV 45132844 636598235 49.28% 4.058% 58 6.343 6.325 6.374 VV 41621536 580864776 44.96% 3.703% 59 6.396 6.374 6.465 VV 20482599 273761075 21.19% 1.745% 60 6.531 6.502 6.565 VV 7218008 105600301 8.17% 0.673% 61 6.594 6.565 6.620 VV 33683382 447455906 34.64% 2.852% 62 6.631 6.620 6.654 VV 3856019 48421770 3.75% 0.309% 63 6.688 6.654 6.715 VV 18045785 256062460 19.82% 1.632% 64 6.736 6.715 6.751 VV 8837481 113876059 8.82% 0.726% 65 6.765 6.751 6.796 VV 7472932 110337546 8.54% 0.703% 66 6.837 6.796 6.876 VV 94439822 1291824507 100.00% 8.234% 67 6.890 6.876 6.913 VV 2159502 30219678 2.34% 0.193% 68 6.936 6.913 6.976 VV 3283432 47888195 3.71% 0.305% 69 7.108 7.054 7.142 PV 21730020 295983392 22.91% 1.887% 70 7.173 7.142 7.263 VV 60699535 878450753 68.00% 5.600% 71 7.268 7.263 7.287 VV 187823 2183138 0.17% 0.014% 72 7.324 7.287 7.339 VV 136787 3778851 0.29% 0.024% 73 7.368 7.339 7.401 VV 1475811 20381375 1.58% 0.130% 74 7.428 7.401 7.443 VV 1302021 15870283 1.23% 0.101% 75 7.457 7.443 7.496 VV 1109459 14860334 1.15% 0.095% 76 7.528 7.496 7.577 PV 9630966 125237391 9.69% 0.798% 77 7.583 7.577 7.586 VV 73613 350620 0.03% 0.002% 78 7.591 7.586 7.604 VV 70035 605160 0.05% 0.004% 79 7.662 7.604 7.693 VV 24310748 309292627 23.94% 1.972% 80 7.706 7.693 7.745 VV 1290080 19453959 1.51% 0.124% 81 7.757 7.745 7.763 VV 152605 1463341 0.11% 0.009% 82 7.766 7.763 7.788 VV 130244 1563369 0.12% 0.010% 83 7.823 7.788 7.827 VV 129127 2248318 0.17% 0.014% 84 7.860 7.827 7.864 VV 161570 2858977 0.22% 0.018% 85 7.924 7.864 7.969 VV 5684863 81443807 6.30% 0.519% 86 8.048 7.969 8.052 VV 300006 12163088 0.94% 0.078% 87 8.078 8.052 8.083 VV 338111 5682653 0.44% 0.036% 88 8.136 8.083 8.208 VV 57634258 778548401 60.27% 4.963% 89 8.263 8.208 8.268 VV 503409 16915928 1.31% 0.108% 90 8.325 8.268 8.331 VV 546626 18601938 1.44% 0.119% 91 8.657 8.331 8.661 VV 933630 144031283 11.15% 0.918% 92 8.768 8.661 8.789 VV 1110225 77021772 5.96% 0.491% 93 9.063 8.789 9.068 VV 1322296 199224351 15.42% 1.270% 94 9.095 9.068 9.099 VV 1341400 24809449 1.92% 0.158% 95 9.131 9.099 9.138 VV 1349882 30326479 2.35% 0.193% 96 9.144 9.138 9.149 VV 1359697 8872684 0.69% 0.057% 97 9.154 9.149 9.166 VV 1357294 13756962 1.06% 0.088% 98 9.172 9.166 9.189 VV 1402130 19199576 1.49% 0.122% 99 9.213 9.189 9.217 VV 1389899 23567645 1.82% 0.150% 100 9.230 9.217 9.241 VV 1418969 19740898 1.53% 0.126% 101 9.253 9.241 9.263 VV 1433725 18351059 1.42% 0.117% 102 9.266 9.263 9.269 VV 1420913 5538034 0.43% 0.035% 103 9.279 9.269 9.296 VV 1479481 23456264 1.82% 0.150% 104 9.314 9.296 9.319 VV 1467629 20057485 1.55% 0.128% 105 9.401 9.319 9.412 VV 1488633 81463174 6.31% 0.519% 106 9.423 9.412 9.441 VV 1509417 24782892 1.92% 0.158% 107 9.447 9.441 9.451 VV 1510362 9336994 0.72% 0.060% 108 9.458 9.451 9.468 VV 1485050 15255039 1.18% 0.097% 109 9.474 9.468 9.479 VV 1469648 9345137 0.72% 0.060% 110 9.526 9.479 9.538 VV 1538033 52401293 4.06% 0.334% 111 9.602 9.538 9.608 VV 1573553 63717242 4.93% 0.406% 112 9.652 9.608 9.661 VV 1552317 48075415 3.72% 0.306% 113 9.670 9.661 9.675 VV 1515851 13266823 1.03% 0.085% 114 9.694 9.675 9.706 VV 1536650 27455874 2.13% 0.175% 115 9.820 9.706 9.828 VV 1529073 110383941 8.54% 0.704% 116 9.865 9.828 9.874 VV 1527438 42429500 3.28% 0.270% 117 9.886 9.874 9.893 VV 1524988 16583708 1.28% 0.106% 118 9.923 9.893 9.927 VV 1518198 31300173 2.42% 0.200% 119 9.977 9.927 9.982 VV 1509537 49192293 3.81% 0.314% 120 9.990 9.982 10.010 VV 1501172 24433095 1.89% 0.156% 121 10.016 10.010 10.021 VV 1499282 9505096 0.74% 0.061% 122 10.088 10.021 10.110 VV 1474370 78380095 6.07% 0.500% 123 10.113 10.110 10.124 VV 1470765 12707326 0.98% 0.081% 124 10.167 10.124 10.180 VV 1490148 48103862 3.72% 0.307% 125 10.281 10.180 10.309 VV 1422664 107938688 8.36% 0.688% 126 10.315 10.309 10.324 VV 1386570 12606702 0.98% 0.080% 127 10.333 10.324 10.344 VV 1371409 15812288 1.22% 0.101% 128 10.353 10.344 10.357 VV 1356093 10944572 0.85% 0.070% 129 10.373 10.357 10.389 VV 1361825 25372757 1.96% 0.162% 130 10.394 10.389 10.406 VV 1333558 13249269 1.03% 0.084% 131 10.412 10.406 10.416 VV 1310621 7894777 0.61% 0.050% 132 10.425 10.416 10.434 VV 1316600 13565717 1.05% 0.086% 133 10.439 10.434 10.453 VV 1309468 14736204 1.14% 0.094% 134 10.455 10.453 10.463 VV 1295990 8077719 0.63% 0.051% 135 10.478 10.463 10.483 VV 1304545 15317924 1.19% 0.098% 136 10.491 10.483 10.509 VV 1295226 19557052 1.51% 0.125% 137 10.522 10.509 10.534 VV 1251046 18312255 1.42% 0.117% 138 10.615 10.534 10.634 VV 1209307 72065931 5.58% 0.459% 139 10.638 10.634 10.646 VV 1192790 8103907 0.63% 0.052% 140 10.662 10.646 10.726 VV 1165729 51576740 3.99% 0.329% 141 10.800 10.726 10.825 VV 1048174 59851457 4.63% 0.382% 142 10.901 10.825 10.914 VV 976938 49546731 3.84% 0.316% 143 11.016 10.914 11.027 VV 879721 59741750 4.62% 0.381% 144 11.143 11.027 11.152 VV 765276 58149750 4.50% 0.371% 145 11.160 11.152 11.166 VV 752782 6289170 0.49% 0.040% 146 11.173 11.166 11.185 VV 739194 8220810 0.64% 0.052% 147 11.191 11.185 11.213 VV 697589 11032604 0.85% 0.070% 148 11.351 11.213 11.382 VV 539849 57593286 4.46% 0.367% 149 11.472 11.382 11.485 VV 401621 25656699 1.99% 0.164% 150 11.502 11.485 11.515 VV 338836 5807860 0.45% 0.037% 151 11.532 11.515 11.555 VV 313028 7021999 0.54% 0.045% 152 11.619 11.555 11.629 VV 222435 10140447 0.78% 0.065% 153 11.675 11.629 11.705 VV 177457 6292476 0.49% 0.040% 154 11.714 11.705 11.779 VB 103831 2162705 0.17% 0.014% Sum of corrected areas: 15687967361