Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042703.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 7:57 Sample : I.BLK Misc : ALS Vial : 2 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.220 3.202 3.264 BB 274404 2516120 1.72% 0.696% 2 3.589 3.535 3.626 PV 102095 2620528 1.79% 0.725% 3 3.655 3.626 3.669 VV 53243 1087398 0.74% 0.301% 4 4.095 4.053 4.210 PV 11301231 131125951 89.44% 36.283% 5 4.387 4.357 4.418 PV 161319 2070822 1.41% 0.573% 6 5.164 5.109 5.193 PV 809908 9479520 6.47% 2.623% 7 5.244 5.193 5.277 VV 120284 2624175 1.79% 0.726% 8 5.680 5.655 5.709 VV 123733 1689913 1.15% 0.468% 9 5.821 5.786 5.859 PV 101399 1631566 1.11% 0.451% 10 6.073 6.043 6.095 PV 179482 3502306 2.39% 0.969% 11 6.109 6.095 6.160 VB 179246 3094219 2.11% 0.856% 12 6.264 6.212 6.286 BV 119612 1068106 0.73% 0.296% 13 6.621 6.589 6.664 BV 376312 4882648 3.33% 1.351% 14 6.899 6.865 6.928 PV 158587 4167145 2.84% 1.153% 15 6.986 6.928 6.991 VV 97250 3717396 2.54% 1.029% 16 6.995 6.991 7.009 VV 92891 914550 0.62% 0.253% 17 7.026 7.009 7.050 VV 105111 2006536 1.37% 0.555% 18 7.104 7.050 7.135 VV 176456 4348514 2.97% 1.203% 19 7.161 7.135 7.200 VV 97656 2121997 1.45% 0.587% 20 7.271 7.200 7.284 VV 22451 920676 0.63% 0.255% 21 7.309 7.284 7.322 VV 52872 704852 0.48% 0.195% 22 7.604 7.455 7.620 BV 34727 1360808 0.93% 0.377% 23 8.084 7.922 8.094 VV 46691 2343445 1.60% 0.648% 24 8.186 8.094 8.208 VV 80752 3392897 2.31% 0.939% 25 8.214 8.208 8.217 VV 72507 314341 0.21% 0.087% 26 8.241 8.217 8.254 VV 86857 1675779 1.14% 0.464% 27 8.260 8.254 8.274 VV 86102 899332 0.61% 0.249% 28 8.459 8.274 8.487 VV 149799 10786520 7.36% 2.985% 29 8.515 8.487 8.544 VV 96325 2410871 1.64% 0.667% 30 8.572 8.544 8.578 PV 77920 1180213 0.80% 0.327% 31 8.608 8.578 8.620 VV 64351 1344224 0.92% 0.372% 32 8.634 8.620 8.640 VV 50588 453540 0.31% 0.125% 33 8.687 8.640 8.692 VV 16413 710033 0.48% 0.196% 34 9.184 9.155 9.224 VV 94567 1617282 1.10% 0.448% 35 9.468 9.395 9.531 PV 8508659 146612611 100.00% 40.568% Sum of corrected areas: 361396834 Signal #2 : ECD2B.CH 1 2.540 2.519 2.609 BV 116126 1735001 0.74% 0.161% 2 3.345 3.300 3.449 BV 13927207 172204314 73.34% 16.024% 3 3.630 3.605 3.665 BV 207523 2591800 1.10% 0.241% 4 4.256 4.204 4.299 PV 913912 11571014 4.93% 1.077% 5 4.388 4.359 4.414 VV 196035 3000985 1.28% 0.279% 6 4.560 4.535 4.579 BV 124408 1601000 0.68% 0.149% 7 4.604 4.579 4.624 VV 121091 1575684 0.67% 0.147% 8 4.639 4.624 4.660 VV 92574 930888 0.40% 0.087% 9 4.804 4.765 4.827 PV 407347 9728226 4.14% 0.905% 10 4.840 4.827 4.858 VV 312770 5259489 2.24% 0.489% 11 4.874 4.858 4.899 VV 318631 6846160 2.92% 0.637% 12 4.904 4.899 4.908 VV 247003 1337013 0.57% 0.124% 13 4.944 4.908 4.979 VV 362574 11857984 5.05% 1.103% 14 5.015 4.979 5.044 VV 297530 9891838 4.21% 0.920% 15 5.109 5.085 5.122 VV 303230 5879204 2.50% 0.547% 16 5.142 5.122 5.162 VV 394639 7476871 3.18% 0.696% 17 5.180 5.162 5.217 VV 390944 9639044 4.11% 0.897% 18 5.350 5.300 5.377 VV 354577 11961320 5.09% 1.113% 19 5.390 5.377 5.409 VV 303359 5205595 2.22% 0.484% 20 5.522 5.489 5.542 PV 216635 5250550 2.24% 0.489% 21 5.585 5.542 5.612 VV 227989 8441467 3.60% 0.785% 22 5.634 5.612 5.654 VV 199957 4571285 1.95% 0.425% 23 5.670 5.654 5.697 VV 212738 4416533 1.88% 0.411% 24 5.757 5.697 5.763 VV 111314 4694599 2.00% 0.437% 25 5.801 5.763 5.836 VV 153243 5005650 2.13% 0.466% 26 5.848 5.836 5.856 VV 92160 889518 0.38% 0.083% 27 5.902 5.856 5.917 VV 99919 2700504 1.15% 0.251% 28 5.982 5.955 6.030 VV 473907 7434193 3.17% 0.692% 29 6.195 6.151 6.236 VV 221971 4056333 1.73% 0.377% 30 6.300 6.272 6.322 PV 65630 816347 0.35% 0.076% 31 6.997 6.959 7.007 VV 485765 12814214 5.46% 1.192% 32 7.108 7.042 7.114 PV 414924 14174991 6.04% 1.319% 33 7.139 7.114 7.144 VV 392562 7056855 3.01% 0.657% 34 7.167 7.144 7.179 VV 412044 8188335 3.49% 0.762% 35 7.233 7.179 7.247 VV 363522 14598852 6.22% 1.358% 36 7.258 7.247 7.265 VV 324184 3450584 1.47% 0.321% 37 7.357 7.265 7.389 VV 343838 20284530 8.64% 1.887% 38 7.450 7.389 7.469 VV 210364 8856816 3.77% 0.824% 39 7.608 7.469 7.617 VV 79650 8660480 3.69% 0.806% 40 7.661 7.617 7.666 VV 76375 1849961 0.79% 0.172% 41 7.674 7.666 7.679 VV 80477 501251 0.21% 0.047% 42 7.705 7.679 7.710 VV 80588 1142573 0.49% 0.106% 43 7.771 7.710 7.780 VV 50649 1767927 0.75% 0.165% 44 7.887 7.780 7.890 VV 32564 1568161 0.67% 0.146% 45 7.917 7.890 7.939 VV 164073 2342308 1.00% 0.218% 46 8.012 7.939 8.017 VV 23561 790695 0.34% 0.074% 47 8.127 8.017 8.185 PV 17256535 234789466 100.00% 21.847% 48 8.204 8.185 8.208 VV 127882 1748864 0.74% 0.163% 49 8.317 8.208 8.322 VV 154873 8796569 3.75% 0.819% 50 8.379 8.322 8.384 VV 196789 6259286 2.67% 0.582% 51 8.802 8.384 8.817 VV 460544 83824946 35.70% 7.800% 52 8.871 8.817 8.875 VV 444561 14949777 6.37% 1.391% 53 9.001 8.875 9.006 VV 483844 36264733 15.45% 3.374% 54 9.026 9.006 9.030 VV 489024 6918713 2.95% 0.644% 55 9.078 9.030 9.086 VV 487729 16317104 6.95% 1.518% 56 9.241 9.086 9.247 VV 508314 46265100 19.70% 4.305% 57 9.317 9.247 9.329 VV 478828 23161296 9.86% 2.155% 58 9.372 9.329 9.379 VV 459318 13448229 5.73% 1.251% 59 9.419 9.379 9.435 VV 441132 14726264 6.27% 1.370% 60 9.561 9.435 9.573 VV 388839 32727211 13.94% 3.045% 61 9.580 9.573 9.589 VV 390073 3592757 1.53% 0.334% 62 9.659 9.589 9.667 VV 375684 17403483 7.41% 1.619% 63 9.686 9.667 9.692 VV 382555 5327941 2.27% 0.496% 64 9.711 9.692 9.717 VV 342014 5164634 2.20% 0.481% 65 9.761 9.717 9.768 VV 344085 9984978 4.25% 0.929% 66 9.862 9.768 9.867 VV 293762 18418201 7.84% 1.714% 67 9.882 9.867 9.887 VV 294796 3373404 1.44% 0.314% 68 9.966 9.887 9.973 VV 242702 12963603 5.52% 1.206% 69 10.001 9.973 10.005 VV 208144 3999579 1.70% 0.372% 70 10.030 10.005 10.045 VV 200385 4430419 1.89% 0.412% 71 10.079 10.045 10.084 VV 190559 3874735 1.65% 0.361% 72 10.098 10.084 10.105 VV 161312 1883194 0.80% 0.175% 73 10.122 10.105 10.139 VV 141997 2646416 1.13% 0.246% 74 10.152 10.139 10.166 VV 118389 1559043 0.66% 0.145% 75 10.174 10.166 10.188 VV 112312 1131689 0.48% 0.105% 76 10.200 10.188 10.218 VV 95586 1195909 0.51% 0.111% 77 10.223 10.218 10.237 VV 68983 533707 0.23% 0.050% 78 10.261 10.237 10.265 VV 46057 391317 0.17% 0.036% Sum of corrected areas: 1074691512