Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042704.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 8:49 Sample : AR1660CCC500 Misc : ALS Vial : 3 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.161 3.101 3.197 PV 189089 2279044 0.47% 0.036% 2 3.223 3.197 3.263 VV 705491 7017210 1.44% 0.112% 3 3.380 3.322 3.391 PV 37874 572728 0.12% 0.009% 4 4.098 4.061 4.264 PV 30541613 363090205 74.72% 5.809% 5 4.295 4.264 4.356 VV 773864 13583189 2.80% 0.217% 6 4.384 4.356 4.429 VV 1322565 18882822 3.89% 0.302% 7 4.456 4.429 4.576 VV 5211500 70263464 14.46% 1.124% 8 4.600 4.576 4.646 VV 886205 10941141 2.25% 0.175% 9 4.779 4.751 4.795 PV 7726664 87745128 18.06% 1.404% 10 4.808 4.795 4.845 VV 4679067 56148924 11.56% 0.898% 11 4.864 4.845 4.881 VV 1038706 12126626 2.50% 0.194% 12 4.893 4.881 4.904 VV 443300 4923623 1.01% 0.079% 13 4.917 4.904 4.941 VV 608407 7713531 1.59% 0.123% 14 4.965 4.941 5.032 VV 7999736 96491364 19.86% 1.544% 15 5.073 5.047 5.102 VV 325767 5103361 1.05% 0.082% 16 5.128 5.102 5.143 VV 2455615 27342151 5.63% 0.437% 17 5.156 5.143 5.193 VV 1680015 25440258 5.24% 0.407% 18 5.223 5.193 5.232 VV 11851037 122777840 25.27% 1.964% 19 5.244 5.232 5.282 VV 14870604 207248050 42.65% 3.316% 20 5.305 5.282 5.370 VV 9296172 135988213 27.99% 2.176% 21 5.400 5.370 5.444 VV 8147700 109039590 22.44% 1.745% 22 5.462 5.444 5.469 VV 956080 9658259 1.99% 0.155% 23 5.489 5.469 5.512 VV 6451122 81144949 16.70% 1.298% 24 5.533 5.512 5.558 VV 5561946 93457401 19.23% 1.495% 25 5.568 5.558 5.647 VV 2979524 38462731 7.92% 0.615% 26 5.686 5.647 5.709 VV 7932397 102056863 21.00% 1.633% 27 5.724 5.709 5.748 VV 3520652 47793754 9.84% 0.765% 28 5.769 5.748 5.791 VV 2983923 36311546 7.47% 0.581% 29 5.821 5.791 5.863 VV 6811795 113001705 23.26% 1.808% 30 5.886 5.863 5.920 VV 2427544 32175110 6.62% 0.515% 31 5.941 5.920 5.973 VV 356340 5639149 1.16% 0.090% 32 6.001 5.973 6.022 VV 444367 5974436 1.23% 0.096% 33 6.051 6.022 6.068 VV 7856066 95916916 19.74% 1.535% 34 6.077 6.068 6.098 VV 3338542 39760659 8.18% 0.636% 35 6.115 6.098 6.176 VV 2528432 37222423 7.66% 0.596% 36 6.202 6.176 6.234 VV 971466 12027219 2.48% 0.192% 37 6.265 6.234 6.294 VV 7010788 88999183 18.32% 1.424% 38 6.305 6.294 6.384 VB 387291 6597917 1.36% 0.106% 39 6.466 6.443 6.489 PV 254716 3197867 0.66% 0.051% 40 6.538 6.506 6.549 BV 1325189 14796595 3.05% 0.237% 41 6.566 6.549 6.596 VV 3239456 39483283 8.13% 0.632% 42 6.622 6.596 6.652 VV 3844175 47055531 9.68% 0.753% 43 6.679 6.652 6.716 VV 9390721 147290773 30.31% 2.357% 44 6.731 6.716 6.754 VV 2495165 31447412 6.47% 0.503% 45 6.782 6.754 6.836 VV 17707930 214599813 44.16% 3.433% 46 6.900 6.866 6.932 PV 2538311 32064342 6.60% 0.513% 47 6.966 6.932 7.002 VV 3560750 44383650 9.13% 0.710% 48 7.034 7.002 7.057 VV 22793800 278811756 57.38% 4.461% 49 7.075 7.057 7.095 VV 6638413 81562102 16.79% 1.305% 50 7.115 7.095 7.137 VV 5555710 67677632 13.93% 1.083% 51 7.159 7.137 7.180 VV 9912697 122883086 25.29% 1.966% 52 7.190 7.180 7.229 VV 2223083 26324788 5.42% 0.421% 53 7.264 7.229 7.280 VV 2179548 32792234 6.75% 0.525% 54 7.310 7.280 7.333 VV 22368288 316859348 65.21% 5.069% 55 7.340 7.333 7.363 VV 3373030 44384924 9.13% 0.710% 56 7.387 7.363 7.417 VV 18046457 229105082 47.15% 3.665% 57 7.444 7.417 7.492 VV 9586582 118041873 24.29% 1.889% 58 7.573 7.492 7.584 PV 3545123 41654331 8.57% 0.666% 59 7.608 7.584 7.656 VV 15817657 227151892 46.75% 3.634% 60 7.684 7.656 7.719 VV 8390408 116114957 23.90% 1.858% 61 7.738 7.719 7.769 VV 4178093 52855524 10.88% 0.846% 62 7.793 7.769 7.812 VV 822757 9888149 2.03% 0.158% 63 7.838 7.812 7.872 VV 4671388 60896865 12.53% 0.974% 64 7.908 7.872 7.938 VV 40551618 485918802 100.00% 7.774% 65 7.955 7.938 8.009 VV 2283241 30756428 6.33% 0.492% 66 8.194 8.131 8.221 BV 16571185 290575090 59.80% 4.649% 67 8.248 8.221 8.256 VV 7618699 101916354 20.97% 1.631% 68 8.260 8.256 8.352 VB 7284952 86289268 17.76% 1.381% 69 8.465 8.416 8.497 BV 542797 7172971 1.48% 0.115% 70 8.543 8.509 8.554 PV 424996 5416086 1.11% 0.087% 71 8.560 8.554 8.574 VV 410063 4209172 0.87% 0.067% 72 8.600 8.574 8.661 VV 3873991 53168915 10.94% 0.851% 73 8.834 8.796 8.884 BV 8373273 125690478 25.87% 2.011% 74 8.913 8.884 8.951 VV 429829 6763890 1.39% 0.108% 75 9.190 9.139 9.244 BV 1967879 32725129 6.73% 0.524% 76 9.475 9.419 9.555 PV 21934435 387502825 79.75% 6.200% Sum of corrected areas: 6250347897 Signal #2 : ECD2B.CH 1 2.540 2.522 2.597 BB 197112 2683672 0.28% 0.023% 2 3.344 3.309 3.491 PV 38534022 486599028 50.59% 4.117% 3 3.547 3.491 3.604 VV 1242625 20180208 2.10% 0.171% 4 3.629 3.604 3.676 VV 1868326 24383384 2.54% 0.206% 5 3.700 3.676 3.767 VV 6557809 87740209 9.12% 0.742% 6 3.784 3.767 3.818 VV 205344 3955223 0.41% 0.033% 7 3.856 3.818 3.915 VV 998050 13871585 1.44% 0.117% 8 3.983 3.956 4.037 PV 10203714 190631894 19.82% 1.613% 9 4.058 4.037 4.077 VV 1310757 16748760 1.74% 0.142% 10 4.090 4.077 4.109 VV 545709 6757174 0.70% 0.057% 11 4.126 4.109 4.137 VV 631853 7059303 0.73% 0.060% 12 4.163 4.137 4.199 VV 9037029 131946357 13.72% 1.116% 13 4.210 4.199 4.234 VV 407812 5268886 0.55% 0.045% 14 4.275 4.234 4.289 VV 3196269 43715117 4.54% 0.370% 15 4.299 4.289 4.342 VV 2176277 27267715 2.83% 0.231% 16 4.389 4.342 4.426 VV 21849060 449385138 46.72% 3.802% 17 4.444 4.426 4.530 VV 11777180 200625402 20.86% 1.697% 18 4.557 4.530 4.581 VV 11143296 143994349 14.97% 1.218% 19 4.600 4.581 4.619 VV 9202013 118742437 12.35% 1.005% 20 4.639 4.619 4.657 VV 10394117 142617090 14.83% 1.207% 21 4.666 4.657 4.735 VV 4376384 56978600 5.92% 0.482% 22 4.803 4.774 4.826 BV 11343820 153297423 15.94% 1.297% 23 4.840 4.826 4.857 VV 5089240 63602167 6.61% 0.538% 24 4.872 4.857 4.901 VV 4269371 56815200 5.91% 0.481% 25 4.943 4.901 4.980 VV 9266145 168729159 17.54% 1.427% 26 5.012 4.980 5.049 VV 3419722 55028611 5.72% 0.466% 27 5.072 5.049 5.087 VV 611336 9740038 1.01% 0.082% 28 5.108 5.087 5.120 VV 2983340 35721292 3.71% 0.302% 29 5.140 5.120 5.165 VV 12772128 170247979 17.70% 1.440% 30 5.179 5.165 5.214 VV 3287502 52920990 5.50% 0.448% 31 5.228 5.214 5.257 VV 1541801 22434199 2.33% 0.190% 32 5.283 5.257 5.322 VV 9603902 127424257 13.25% 1.078% 33 5.347 5.322 5.353 VV 681788 9665671 1.00% 0.082% 34 5.367 5.353 5.437 VV 1023793 21511726 2.24% 0.182% 35 5.503 5.477 5.556 VV 361128 5489731 0.57% 0.046% 36 5.585 5.556 5.618 PV 1965659 25478335 2.65% 0.216% 37 5.648 5.618 5.658 VV 4787149 53411264 5.55% 0.452% 38 5.684 5.658 5.705 VV 16251919 252145224 26.21% 2.133% 39 5.723 5.705 5.767 VV 5859494 113228283 11.77% 0.958% 40 5.796 5.767 5.841 VV 28146104 367603685 38.22% 3.110% 41 5.855 5.841 5.874 VV 641704 8982293 0.93% 0.076% 42 5.897 5.874 5.905 VV 1866064 20666261 2.15% 0.175% 43 5.924 5.905 5.955 VV 6683255 93509083 9.72% 0.791% 44 5.983 5.955 6.096 VV 38716223 506249871 52.63% 4.283% 45 6.127 6.096 6.177 PV 31473505 430604661 44.77% 3.643% 46 6.201 6.177 6.223 VV 3731239 48285483 5.02% 0.408% 47 6.246 6.223 6.270 VV 9314441 122702434 12.76% 1.038% 48 6.299 6.270 6.317 VV 34174604 489235662 50.86% 4.139% 49 6.334 6.317 6.365 VV 33536326 473041040 49.18% 4.002% 50 6.386 6.365 6.462 VV 16252062 225018864 23.39% 1.904% 51 6.522 6.489 6.557 BV 5779380 84061688 8.74% 0.711% 52 6.585 6.557 6.612 VV 27139361 361228004 37.56% 3.056% 53 6.622 6.612 6.645 VV 3244755 42020831 4.37% 0.355% 54 6.679 6.645 6.707 VV 14436335 213120454 22.16% 1.803% 55 6.727 6.707 6.743 VV 7205636 97778734 10.17% 0.827% 56 6.756 6.743 6.790 VV 6046059 95455322 9.92% 0.808% 57 6.827 6.790 6.868 VV 69258069 961863705 100.00% 8.137% 58 6.880 6.868 6.905 VV 2328428 38391297 3.99% 0.325% 59 6.926 6.905 7.042 VV 3243615 83072881 8.64% 0.703% 60 7.099 7.042 7.135 PV 16700468 246983958 25.68% 2.089% 61 7.164 7.135 7.302 VV 42715763 689602667 71.69% 5.834% 62 7.311 7.302 7.331 VV 528342 9140032 0.95% 0.077% 63 7.357 7.331 7.397 VV 1408499 29146297 3.03% 0.247% 64 7.422 7.397 7.435 VV 1154023 17764437 1.85% 0.150% 65 7.448 7.435 7.486 VV 1107290 20764638 2.16% 0.176% 66 7.520 7.486 7.594 VV 7179164 111937777 11.64% 0.947% 67 7.606 7.594 7.622 VV 314144 4925291 0.51% 0.042% 68 7.653 7.622 7.686 VV 16167198 223171159 23.20% 1.888% 69 7.698 7.686 7.787 VV 1309128 35532001 3.69% 0.301% 70 7.801 7.787 7.806 VV 329018 3579917 0.37% 0.030% 71 7.855 7.806 7.867 VV 328881 11340252 1.18% 0.096% 72 7.916 7.867 8.001 VV 4204749 78833292 8.20% 0.667% 73 8.073 8.001 8.080 VV 426823 18817685 1.96% 0.159% 74 8.127 8.080 8.196 VV 47351784 658160037 68.43% 5.568% 75 8.200 8.196 8.215 VV 624871 6658641 0.69% 0.056% 76 8.225 8.215 8.234 VV 585865 6762525 0.70% 0.057% 77 8.257 8.234 8.273 VV 581970 13042791 1.36% 0.110% 78 8.313 8.273 8.317 VV 587001 14835311 1.54% 0.126% 79 8.374 8.317 8.380 VV 619863 22281752 2.32% 0.188% 80 8.401 8.380 8.406 VV 628243 9686395 1.01% 0.082% 81 8.526 8.406 8.532 VV 703869 50390122 5.24% 0.426% 82 8.649 8.532 8.657 VV 788873 55355135 5.75% 0.468% 83 8.728 8.657 8.732 VV 818485 35314343 3.67% 0.299% 84 8.831 8.732 8.836 VV 877462 51936535 5.40% 0.439% 85 8.984 8.836 8.989 VV 916592 80988311 8.42% 0.685% 86 9.064 8.989 9.071 VV 957830 46245778 4.81% 0.391% 87 9.113 9.071 9.118 VV 979236 27170529 2.82% 0.230% 88 9.138 9.118 9.144 VV 1005361 15227838 1.58% 0.129% 89 9.191 9.144 9.204 VV 980794 34830946 3.62% 0.295% 90 9.266 9.204 9.272 VV 1013316 39907172 4.15% 0.338% 91 9.336 9.272 9.342 VV 1002445 41896739 4.36% 0.354% 92 9.355 9.342 9.360 VV 1000609 10278287 1.07% 0.087% 93 9.378 9.360 9.394 VV 1018252 20681411 2.15% 0.175% 94 9.406 9.394 9.410 VV 1008890 9515402 0.99% 0.080% 95 9.416 9.410 9.426 VV 1016887 9246812 0.96% 0.078% 96 9.431 9.426 9.434 VV 991645 5196582 0.54% 0.044% 97 9.440 9.434 9.444 VV 1001446 5400445 0.56% 0.046% 98 9.449 9.444 9.454 VV 997735 6255433 0.65% 0.053% 99 9.501 9.454 9.506 VV 1003125 30939181 3.22% 0.262% 100 9.523 9.506 9.527 VV 987292 11877122 1.23% 0.100% 101 9.581 9.527 9.586 VV 995203 34786765 3.62% 0.294% 102 9.622 9.586 9.627 VV 998254 24723285 2.57% 0.209% 103 9.662 9.627 9.672 VV 1007851 26230573 2.73% 0.222% 104 9.678 9.672 9.689 VV 1002694 9961674 1.04% 0.084% 105 9.693 9.689 9.699 VV 1005774 5868700 0.61% 0.050% 106 9.716 9.699 9.732 VV 996005 19380198 2.01% 0.164% 107 9.750 9.732 9.757 VV 981564 14898525 1.55% 0.126% 108 9.842 9.757 9.849 VV 986253 52744292 5.48% 0.446% 109 9.854 9.849 9.863 VV 977990 8513378 0.89% 0.072% 110 9.869 9.863 9.885 VV 969455 12255061 1.27% 0.104% 111 9.900 9.885 9.911 VV 959088 14565217 1.51% 0.123% 112 9.941 9.911 9.957 VV 960257 26273231 2.73% 0.222% 113 9.987 9.957 9.992 VV 927350 19047585 1.98% 0.161% 114 10.000 9.992 10.005 VV 927677 7147800 0.74% 0.060% 115 10.015 10.005 10.038 VV 919953 17649048 1.83% 0.149% 116 10.043 10.038 10.051 VV 899225 7049011 0.73% 0.060% 117 10.091 10.062 10.112 VV 891291 25840899 2.69% 0.219% 118 10.163 10.112 10.176 VV 863788 32780058 3.41% 0.277% 119 10.188 10.176 10.199 VV 850676 12000084 1.25% 0.102% 120 10.500 10.199 10.516 VV 670945 139393468 14.49% 1.179% 121 10.742 10.516 10.765 VV 483971 78695909 8.18% 0.666% 122 10.986 10.765 10.999 VV 272656 46440280 4.83% 0.393% 123 11.114 10.999 11.131 VV 162252 14615534 1.52% 0.124% 124 11.188 11.131 11.231 VB 104229 4698309 0.49% 0.040% 125 11.588 11.459 11.596 VV 52533 2500252 0.26% 0.021% Sum of corrected areas: 11820615449