Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042705.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 9:07 Sample : J1705-01 Misc : ALS Vial : 4 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.161 3.108 3.189 VV 195814 6205732 4.10% 0.967% 2 3.225 3.205 3.271 VV 583104 10913312 7.21% 1.700% 3 3.292 3.271 3.338 VV 319756 8463658 5.59% 1.319% 4 3.353 3.338 3.366 VV 255731 3359074 2.22% 0.523% 5 3.485 3.467 3.518 VV 221879 4491531 2.97% 0.700% 6 3.692 3.673 3.706 VV 179550 2162389 1.43% 0.337% 7 4.101 4.057 4.207 PV 12497467 147023020 97.14% 22.905% 8 4.394 4.374 4.411 VV 228949 3411655 2.25% 0.532% 9 4.427 4.411 4.447 VV 178161 2680718 1.77% 0.418% 10 4.494 4.476 4.517 VV 337442 4374092 2.89% 0.681% 11 4.542 4.517 4.549 VV 260919 3081741 2.04% 0.480% 12 4.563 4.549 4.583 VV 518978 6207196 4.10% 0.967% 13 5.169 5.141 5.198 PV 890900 9803140 6.48% 1.527% 14 5.247 5.238 5.283 VV 117327 1369311 0.90% 0.213% 15 5.686 5.659 5.709 VV 107924 1626785 1.07% 0.253% 16 5.835 5.795 5.873 PV 107013 2956935 1.95% 0.461% 17 6.053 6.018 6.068 VV 161231 2204821 1.46% 0.343% 18 6.078 6.068 6.096 VV 136582 1471598 0.97% 0.229% 19 6.117 6.096 6.161 VV 138984 2122067 1.40% 0.331% 20 6.268 6.229 6.304 VV 319990 4958975 3.28% 0.773% 21 6.530 6.492 6.554 VV 238093 4750336 3.14% 0.740% 22 6.625 6.591 6.662 PV 398727 6408135 4.23% 0.998% 23 6.682 6.662 6.716 VV 169980 3116877 2.06% 0.486% 24 6.743 6.716 6.764 VV 114375 2137192 1.41% 0.333% 25 6.785 6.764 6.811 VB 225399 2969246 1.96% 0.463% 26 6.902 6.867 6.928 PV 132350 1938098 1.28% 0.302% 27 7.035 6.989 7.061 PV 329664 4293392 2.84% 0.669% 28 7.076 7.061 7.093 VV 109844 1183104 0.78% 0.184% 29 7.117 7.093 7.137 VV 181689 2277026 1.50% 0.355% 30 7.163 7.137 7.181 VV 142695 1982303 1.31% 0.309% 31 7.311 7.229 7.336 VV 360955 6184100 4.09% 0.963% 32 7.388 7.361 7.422 VV 1016023 12644200 8.35% 1.970% 33 7.446 7.422 7.471 VV 347502 4473828 2.96% 0.697% 34 7.490 7.471 7.516 VV 118060 1758634 1.16% 0.274% 35 7.575 7.516 7.587 VV 149059 3635700 2.40% 0.566% 36 7.628 7.587 7.653 VV 482554 10752665 7.10% 1.675% 37 7.687 7.663 7.696 VV 178535 2231364 1.47% 0.348% 38 7.712 7.696 7.731 VV 249189 3596104 2.38% 0.560% 39 7.761 7.731 7.779 VV 144107 3221524 2.13% 0.502% 40 7.851 7.812 7.879 VV 177105 4645078 3.07% 0.724% 41 7.910 7.879 7.936 VV 1410941 18441831 12.18% 2.873% 42 7.956 7.936 7.978 VV 274455 4423091 2.92% 0.689% 43 8.111 8.058 8.131 VV 111695 4069709 2.69% 0.634% 44 8.186 8.131 8.222 VV 1919638 29945574 19.78% 4.665% 45 8.267 8.222 8.302 VV 1675489 30890880 20.41% 4.813% 46 8.328 8.302 8.341 VV 124976 2698330 1.78% 0.420% 47 8.467 8.341 8.487 VV 617837 16580386 10.95% 2.583% 48 8.493 8.487 8.504 VV 264183 2625197 1.73% 0.409% 49 8.518 8.504 8.546 VV 285433 4988430 3.30% 0.777% 50 8.566 8.546 8.582 VV 297220 4140818 2.74% 0.645% 51 8.598 8.582 8.643 VV 247963 5737723 3.79% 0.894% 52 8.836 8.762 8.876 VV 1064290 19859925 13.12% 3.094% 53 8.910 8.876 8.922 VV 103168 2430842 1.61% 0.379% 54 9.191 9.054 9.260 VV 1631728 30058728 19.86% 4.683% 55 9.291 9.260 9.299 VV 27493 533518 0.35% 0.083% 56 9.478 9.388 9.548 BV 8867293 151358022 100.00% 23.581% Sum of corrected areas: 641869663 Signal #2 : ECD2B.CH 1 2.748 2.713 2.804 PV 119072 2056701 0.90% 0.085% 2 3.040 3.023 3.083 VV 168727 3338149 1.46% 0.137% 3 3.240 3.173 3.316 PV 93186 4167168 1.82% 0.171% 4 3.344 3.316 3.426 VV 13694525 167483910 73.15% 6.893% 5 3.543 3.523 3.586 VV 239222 2795299 1.22% 0.115% 6 3.604 3.586 3.617 VV 146953 1642396 0.72% 0.068% 7 3.629 3.617 3.691 VV 191675 3332190 1.46% 0.137% 8 3.757 3.715 3.806 VV 410068 7595423 3.32% 0.313% 9 4.256 4.230 4.296 PV 991172 12289768 5.37% 0.506% 10 4.388 4.346 4.423 BV 167211 3022804 1.32% 0.124% 11 4.800 4.786 4.851 VV 134714 2947374 1.29% 0.121% 12 4.942 4.889 4.968 VV 118209 2109392 0.92% 0.087% 13 5.141 5.122 5.163 VV 245211 3414290 1.49% 0.141% 14 5.180 5.163 5.198 VV 137954 1722653 0.75% 0.071% 15 5.283 5.263 5.294 VV 195411 2588533 1.13% 0.107% 16 5.306 5.294 5.318 VV 242258 2951747 1.29% 0.121% 17 5.339 5.318 5.359 VV 266651 6050049 2.64% 0.249% 18 5.529 5.467 5.566 PV 444802 13131633 5.74% 0.540% 19 5.585 5.566 5.621 VV 312918 8674492 3.79% 0.357% 20 5.681 5.621 5.707 VV 461756 16427570 7.17% 0.676% 21 5.724 5.707 5.766 VV 284173 7417052 3.24% 0.305% 22 5.797 5.766 5.826 VV 531356 10681941 4.67% 0.440% 23 5.850 5.826 5.876 VV 295282 7849170 3.43% 0.323% 24 5.894 5.876 5.911 VV 356716 6385278 2.79% 0.263% 25 5.925 5.911 5.951 VV 316964 6705625 2.93% 0.276% 26 5.982 5.951 6.046 VV 878900 23329866 10.19% 0.960% 27 6.127 6.064 6.164 VV 703252 21154441 9.24% 0.871% 28 6.197 6.164 6.224 VV 469717 13265276 5.79% 0.546% 29 6.246 6.224 6.272 VV 454544 10320083 4.51% 0.425% 30 6.298 6.272 6.314 VV 705461 13209427 5.77% 0.544% 31 6.335 6.314 6.368 VV 1727250 29045203 12.69% 1.195% 32 6.388 6.368 6.426 VV 704700 15712578 6.86% 0.647% 33 6.481 6.426 6.504 VV 415666 16135884 7.05% 0.664% 34 6.528 6.504 6.554 VV 562884 14126832 6.17% 0.581% 35 6.581 6.554 6.613 VV 1193788 24255340 10.59% 0.998% 36 6.664 6.613 6.708 VV 667221 27186383 11.87% 1.119% 37 6.734 6.708 6.786 VV 440157 18569832 8.11% 0.764% 38 6.828 6.786 6.894 VV 2277174 49564729 21.65% 2.040% 39 6.927 6.904 6.951 VV 631229 13510757 5.90% 0.556% 40 6.964 6.951 6.991 VV 461474 9648531 4.21% 0.397% 41 7.100 7.041 7.138 PV 2909458 50703377 22.14% 2.087% 42 7.166 7.138 7.206 VV 3453305 54800252 23.93% 2.255% 43 7.209 7.206 7.229 VV 353918 4338369 1.89% 0.179% 44 7.275 7.229 7.288 VV 274455 8944947 3.91% 0.368% 45 7.359 7.288 7.408 VV 1013370 26342303 11.50% 1.084% 46 7.413 7.408 7.425 VV 192743 1852454 0.81% 0.076% 47 7.450 7.425 7.498 VV 526401 13848316 6.05% 0.570% 48 7.521 7.498 7.536 VV 336735 5374232 2.35% 0.221% 49 7.553 7.536 7.575 VV 339768 5255196 2.30% 0.216% 50 7.582 7.575 7.591 VV 125053 1135840 0.50% 0.047% 51 7.654 7.591 7.685 VV 1715102 27477477 12.00% 1.131% 52 7.691 7.685 7.714 VV 189286 2821596 1.23% 0.116% 53 7.753 7.714 7.774 VV 154429 4392000 1.92% 0.181% 54 7.815 7.774 7.832 VV 141416 3688208 1.61% 0.152% 55 7.851 7.832 7.870 VV 139168 2222517 0.97% 0.091% 56 7.917 7.870 7.952 PV 2976953 42687580 18.64% 1.757% 57 7.965 7.952 7.971 VV 206708 2278619 1.00% 0.094% 58 7.978 7.971 7.989 VV 190108 1947157 0.85% 0.080% 59 8.070 7.989 8.089 VV 235750 11246515 4.91% 0.463% 60 8.127 8.089 8.179 VV 16802665 228970307 100.00% 9.423% 61 8.230 8.179 8.244 VV 379349 13599689 5.94% 0.560% 62 8.498 8.244 8.516 VV 638811 83083747 36.29% 3.419% 63 8.585 8.516 8.607 VV 687771 35345635 15.44% 1.455% 64 8.662 8.607 8.688 VV 749769 33237659 14.52% 1.368% 65 8.758 8.688 8.776 VV 808395 40370664 17.63% 1.661% 66 8.809 8.776 8.818 VV 861165 19198210 8.38% 0.790% 67 8.837 8.818 8.854 VV 837685 17683039 7.72% 0.728% 68 8.896 8.854 8.918 VV 844604 30273382 13.22% 1.246% 69 9.023 8.918 9.033 VV 952579 61744837 26.97% 2.541% 70 9.070 9.033 9.103 VV 964469 38431699 16.78% 1.582% 71 9.297 9.103 9.318 VV 1048101 126378070 55.19% 5.201% 72 9.347 9.318 9.384 VV 1050247 40017777 17.48% 1.647% 73 9.741 9.384 9.750 VV 1081004 223935395 97.80% 9.216% 74 9.970 9.750 9.983 VV 982734 140353990 61.30% 5.776% 75 10.091 9.983 10.101 VV 879366 65118583 28.44% 2.680% 76 10.468 10.101 10.521 VV 760212 202036783 88.24% 8.315% 77 10.739 10.521 10.832 VV 537683 98717653 43.11% 4.063% 78 10.966 10.832 11.022 VV 327572 37720390 16.47% 1.552% 79 11.204 11.022 11.232 VV 119897 16530182 7.22% 0.680% Sum of corrected areas: 2429920415