Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042706.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 9:22 Sample : J1705-03 Misc : ALS Vial : 5 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.222 3.201 3.254 PV 938098 9971132 10.56% 2.178% 2 3.590 3.523 3.620 PV 175561 5165723 5.47% 1.128% 3 3.638 3.620 3.658 VV 141222 2521674 2.67% 0.551% 4 3.676 3.658 3.699 VV 262921 4577327 4.85% 1.000% 5 3.714 3.699 3.754 VV 256578 4359816 4.62% 0.952% 6 3.821 3.797 3.847 VV 61433 1161105 1.23% 0.254% 7 4.096 4.056 4.163 PV 8522845 94433324 100.00% 20.625% 8 4.389 4.333 4.424 BV 121511 1541754 1.63% 0.337% 9 4.536 4.493 4.547 BV 624768 6399523 6.78% 1.398% 10 4.557 4.547 4.616 VV 620492 8066733 8.54% 1.762% 11 4.901 4.875 4.920 VV 440624 5953621 6.30% 1.300% 12 4.993 4.920 5.018 VV 1508868 33673404 35.66% 7.355% 13 5.035 5.018 5.061 VV 695234 10124095 10.72% 2.211% 14 5.083 5.061 5.114 VV 242971 5005358 5.30% 1.093% 15 5.165 5.143 5.196 VV 737533 8416881 8.91% 1.838% 16 5.246 5.229 5.286 VV 141393 2519788 2.67% 0.550% 17 5.529 5.507 5.557 PV 94934 1238280 1.31% 0.270% 18 5.826 5.790 5.863 PV 132371 2891005 3.06% 0.631% 19 6.050 6.028 6.063 VV 198172 2310598 2.45% 0.505% 20 6.075 6.063 6.094 VV 177308 2545388 2.70% 0.556% 21 6.117 6.094 6.151 VV 300859 6968079 7.38% 1.522% 22 6.199 6.151 6.237 VV 556968 17342213 18.36% 3.788% 23 6.262 6.237 6.300 VV 563223 10352824 10.96% 2.261% 24 6.316 6.300 6.343 PV 166793 2708017 2.87% 0.591% 25 6.393 6.343 6.418 VV 214106 6065251 6.42% 1.325% 26 6.424 6.418 6.430 VV 143310 983478 1.04% 0.215% 27 6.461 6.430 6.484 VV 172573 4701802 4.98% 1.027% 28 6.525 6.484 6.554 VV 557830 11220131 11.88% 2.451% 29 6.558 6.554 6.589 VV 208295 2729892 2.89% 0.596% 30 6.623 6.589 6.652 PV 507142 8978503 9.51% 1.961% 31 6.679 6.652 6.714 VV 233411 5584346 5.91% 1.220% 32 6.736 6.714 6.760 VV 145238 3208580 3.40% 0.701% 33 6.780 6.760 6.814 VV 397739 5901940 6.25% 1.289% 34 6.898 6.863 6.919 VV 197551 3127725 3.31% 0.683% 35 6.962 6.919 6.996 VV 115974 2710650 2.87% 0.592% 36 7.029 6.996 7.052 VV 478232 6698691 7.09% 1.463% 37 7.072 7.052 7.091 VV 162698 1888110 2.00% 0.412% 38 7.111 7.091 7.135 VV 133518 1771616 1.88% 0.387% 39 7.161 7.135 7.203 PV 185732 3131730 3.32% 0.684% 40 7.263 7.203 7.281 PV 65167 1444537 1.53% 0.316% 41 7.307 7.281 7.329 VV 484232 7164147 7.59% 1.565% 42 7.339 7.329 7.351 VV 146924 1685976 1.79% 0.368% 43 7.384 7.351 7.416 VV 389556 6366285 6.74% 1.390% 44 7.440 7.416 7.475 VV 171658 2532645 2.68% 0.553% 45 7.606 7.505 7.651 PV 255857 5585933 5.92% 1.220% 46 7.657 7.651 7.663 PV 18521 56258 0.06% 0.012% 47 7.682 7.663 7.701 VV 144213 1547253 1.64% 0.338% 48 7.735 7.701 7.748 VV 60997 887273 0.94% 0.194% 49 7.795 7.764 7.809 VV 35176 612825 0.65% 0.134% 50 7.835 7.809 7.859 VB 89694 1161668 1.23% 0.254% 51 7.905 7.871 7.936 BV 574637 6785908 7.19% 1.482% 52 8.188 8.153 8.217 PV 291235 5573444 5.90% 1.217% 53 8.258 8.217 8.288 VV 177172 4614786 4.89% 1.008% 54 8.462 8.288 8.489 VV 124178 6919222 7.33% 1.511% 55 8.494 8.489 8.498 VV 85986 380346 0.40% 0.083% 56 8.504 8.498 8.544 VB 80356 1399935 1.48% 0.306% 57 8.594 8.546 8.618 BV 112024 2680254 2.84% 0.585% 58 8.833 8.753 8.860 VV 181738 5234639 5.54% 1.143% 59 8.912 8.860 8.918 VV 75283 1962612 2.08% 0.429% 60 8.962 8.918 8.999 VV 332348 6728738 7.13% 1.470% 61 9.187 9.149 9.221 VV 158044 2740748 2.90% 0.599% 62 9.471 9.414 9.533 BV 3607526 62862264 66.57% 13.730% 63 9.582 9.533 9.624 PV 89237 1976504 2.09% 0.432% Sum of corrected areas: 457854302 Signal #2 : ECD2B.CH 1 2.738 2.711 2.771 PV 257792 4660768 3.61% 0.294% 2 2.834 2.816 2.871 VV 225409 5073839 3.93% 0.320% 3 3.015 2.999 3.029 VV 262686 3238029 2.51% 0.204% 4 3.041 3.029 3.105 VV 282523 6312766 4.89% 0.398% 5 3.345 3.316 3.446 VV 10466137 129192825 100.00% 8.143% 6 3.631 3.588 3.638 VV 306905 3979762 3.08% 0.251% 7 3.665 3.638 3.675 VV 1067385 15308071 11.85% 0.965% 8 3.698 3.675 3.720 VV 2831984 45831796 35.48% 2.889% 9 3.737 3.720 3.814 VV 1769326 38888392 30.10% 2.451% 10 4.257 4.216 4.299 BV 734065 5532316 4.28% 0.349% 11 4.308 4.299 4.327 VV 61487 672818 0.52% 0.042% 12 4.332 4.327 4.341 VV 33883 206726 0.16% 0.013% 13 4.346 4.341 4.352 VV 31505 141064 0.11% 0.009% 14 4.389 4.352 4.428 VV 161786 2999896 2.32% 0.189% 15 4.452 4.428 4.458 PV 29424 228959 0.18% 0.014% 16 4.560 4.505 4.584 VV 156321 3044908 2.36% 0.192% 17 4.601 4.584 4.619 VV 228947 4038074 3.13% 0.255% 18 4.682 4.619 4.766 VV 1098975 49214835 38.09% 3.102% 19 4.944 4.919 4.965 VV 368650 8271898 6.40% 0.521% 20 5.140 5.123 5.166 VV 704482 13705370 10.61% 0.864% 21 5.180 5.166 5.196 VV 501833 8489531 6.57% 0.535% 22 5.284 5.256 5.293 VV 643672 11630937 9.00% 0.733% 23 5.306 5.293 5.320 VV 757785 11410616 8.83% 0.719% 24 5.334 5.320 5.374 VV 718284 21280207 16.47% 1.341% 25 5.388 5.374 5.464 VV 669218 28180804 21.81% 1.776% 26 5.528 5.464 5.561 PV 1091710 33476046 25.91% 2.110% 27 5.584 5.561 5.607 VV 638802 15557875 12.04% 0.981% 28 5.684 5.607 5.703 VV 906066 38604200 29.88% 2.433% 29 5.718 5.703 5.766 VV 756743 19988979 15.47% 1.260% 30 5.795 5.766 5.828 VV 867622 18073604 13.99% 1.139% 31 5.850 5.828 5.877 VV 402417 11075980 8.57% 0.698% 32 5.894 5.877 5.910 VV 485973 8128253 6.29% 0.512% 33 5.927 5.910 5.952 VV 421899 8934128 6.92% 0.563% 34 5.982 5.952 6.039 VV 950715 23316928 18.05% 1.470% 35 6.055 6.039 6.088 VV 449211 8804506 6.82% 0.555% 36 6.126 6.088 6.165 VV 687534 14728009 11.40% 0.928% 37 6.196 6.165 6.223 VV 380824 8092044 6.26% 0.510% 38 6.246 6.223 6.269 VV 274056 4916458 3.81% 0.310% 39 6.298 6.269 6.317 VV 725182 11666484 9.03% 0.735% 40 6.334 6.317 6.368 VV 553942 8787682 6.80% 0.554% 41 6.387 6.368 6.429 VV 262440 4097928 3.17% 0.258% 42 6.523 6.499 6.558 VV 140846 3184555 2.46% 0.201% 43 6.584 6.558 6.606 VV 454355 7316817 5.66% 0.461% 44 6.625 6.606 6.649 VV 233019 4665014 3.61% 0.294% 45 6.679 6.649 6.706 VV 368640 8087264 6.26% 0.510% 46 6.726 6.706 6.741 VV 296904 4977721 3.85% 0.314% 47 6.827 6.776 6.883 VV 1157250 27027450 20.92% 1.704% 48 7.020 6.985 7.042 VV 399349 10439069 8.08% 0.658% 49 7.100 7.042 7.125 PV 655664 17378779 13.45% 1.095% 50 7.131 7.125 7.143 VV 324444 3356348 2.60% 0.212% 51 7.164 7.143 7.201 VV 931519 18143277 14.04% 1.144% 52 7.214 7.201 7.234 VV 255182 4424392 3.42% 0.279% 53 7.266 7.234 7.279 VV 224655 5492636 4.25% 0.346% 54 7.359 7.279 7.393 VV 288829 13463376 10.42% 0.849% 55 7.414 7.393 7.425 VV 140687 2529247 1.96% 0.159% 56 7.446 7.425 7.459 VV 161058 2497585 1.93% 0.157% 57 7.477 7.459 7.483 VV 103973 1297979 1.00% 0.082% 58 7.524 7.483 7.546 VV 171922 4361146 3.38% 0.275% 59 7.560 7.546 7.568 VV 85762 944932 0.73% 0.060% 60 7.641 7.568 7.678 VV 790608 14529464 11.25% 0.916% 61 7.685 7.678 7.690 VV 79535 492535 0.38% 0.031% 62 7.782 7.690 7.789 VV 73074 3564918 2.76% 0.225% 63 7.798 7.789 7.804 VV 66658 512030 0.40% 0.032% 64 7.808 7.804 7.813 VV 74883 283087 0.22% 0.018% 65 7.838 7.813 7.846 VV 64717 1109648 0.86% 0.070% 66 7.856 7.846 7.863 VV 68538 438091 0.34% 0.028% 67 7.868 7.863 7.872 VV 39440 181516 0.14% 0.011% 68 7.886 7.872 7.890 VV 56318 409070 0.32% 0.026% 69 7.917 7.890 7.937 VV 322237 4913164 3.80% 0.310% 70 7.943 7.937 7.947 VV 89727 473009 0.37% 0.030% 71 8.071 7.947 8.084 VV 123547 7950889 6.15% 0.501% 72 8.126 8.084 8.169 VV 7203667 101616249 78.65% 6.405% 73 8.400 8.169 8.407 VV 381889 41796420 32.35% 2.635% 74 8.438 8.407 8.453 VV 394431 10225844 7.92% 0.645% 75 8.632 8.453 8.636 VV 514024 47473622 36.75% 2.992% 76 8.776 8.636 8.788 VV 529561 46247705 35.80% 2.915% 77 8.823 8.788 8.837 VV 579446 16080939 12.45% 1.014% 78 8.842 8.837 8.856 VV 560758 6267352 4.85% 0.395% 79 8.870 8.856 8.901 VV 554042 14001272 10.84% 0.883% 80 8.964 8.901 8.970 VV 592070 22267346 17.24% 1.404% 81 8.981 8.970 8.986 VV 598527 5551091 4.30% 0.350% 82 9.047 8.986 9.052 VV 622441 23805118 18.43% 1.500% 83 9.174 9.052 9.181 VV 661600 48769034 37.75% 3.074% 84 9.285 9.181 9.300 VV 640969 45088682 34.90% 2.842% 85 9.359 9.300 9.371 VV 643554 26499307 20.51% 1.670% 86 9.376 9.371 9.386 VV 630405 5433291 4.21% 0.342% 87 9.424 9.386 9.435 VV 622512 17748621 13.74% 1.119% 88 9.440 9.435 9.444 VV 593088 3222851 2.49% 0.203% 89 9.480 9.444 9.510 VV 656313 24113757 18.66% 1.520% 90 9.517 9.510 9.523 VV 582850 4556490 3.53% 0.287% 91 9.593 9.523 9.597 VV 577788 24827781 19.22% 1.565% 92 9.719 9.597 9.752 VV 664352 54083086 41.86% 3.409% 93 9.756 9.752 9.771 VV 559810 6335207 4.90% 0.399% 94 9.818 9.771 9.826 VV 538911 17215061 13.33% 1.085% 95 9.831 9.826 9.837 VV 507290 3166691 2.45% 0.200% 96 9.844 9.837 9.851 VV 499290 4135734 3.20% 0.261% 97 9.944 9.851 9.949 VV 499068 28082315 21.74% 1.770% 98 9.955 9.949 9.968 VV 492609 5227720 4.05% 0.330% 99 9.973 9.968 9.985 VV 455820 4651829 3.60% 0.293% 100 10.003 9.985 10.007 VV 438101 5568837 4.31% 0.351% 101 10.039 10.007 10.052 VV 427478 11263660 8.72% 0.710% 102 10.057 10.052 10.064 VV 404370 2793409 2.16% 0.176% 103 10.070 10.064 10.078 VV 388561 2988299 2.31% 0.188% 104 10.173 10.089 10.178 VV 381303 19151749 14.82% 1.207% 105 10.187 10.178 10.206 VV 349855 5387577 4.17% 0.340% 106 10.222 10.206 10.254 VV 330201 8825853 6.83% 0.556% 107 10.306 10.254 10.313 VV 264723 8802227 6.81% 0.555% 108 10.345 10.313 10.353 VV 201901 4778765 3.70% 0.301% 109 10.392 10.353 10.396 VV 173177 4476738 3.47% 0.282% 110 10.454 10.396 10.484 VV 208603 8153960 6.31% 0.514% 111 10.489 10.484 10.507 VV 104522 966439 0.75% 0.061% 112 10.541 10.507 10.548 VV 65840 1051658 0.81% 0.066% 113 10.552 10.548 10.557 VV 39940 128641 0.10% 0.008% 114 10.717 10.667 10.728 VV 133861 2412208 1.87% 0.152% 115 10.732 10.728 10.771 VV 98196 1190074 0.92% 0.075% 116 10.848 10.791 10.853 PV 69012 1743941 1.35% 0.110% 117 10.858 10.853 10.861 VV 52060 242289 0.19% 0.015% 118 10.869 10.861 10.890 VV 64493 591968 0.46% 0.037% 119 11.196 11.139 11.228 PV 103702 2844768 2.20% 0.179% 120 11.264 11.228 11.270 PV 32927 410790 0.32% 0.026% Sum of corrected areas: 1586493579