Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042707.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 9:37 Sample : J1705-12 Misc : ALS Vial : 6 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.230 3.180 3.278 PV 1343777 17583749 11.79% 4.170% 2 3.490 3.406 3.499 VV 127121 2863301 1.92% 0.679% 3 3.540 3.499 3.562 VV 101604 3054350 2.05% 0.724% 4 3.592 3.562 3.597 VV 34573 422888 0.28% 0.100% 5 4.097 4.051 4.202 BV 11824061 134314328 90.05% 31.852% 6 4.390 4.357 4.434 BV 176337 2467624 1.65% 0.585% 7 5.166 5.140 5.205 VV 1395393 16376479 10.98% 3.884% 8 5.223 5.205 5.230 VV 213534 2107147 1.41% 0.500% 9 5.244 5.230 5.282 VV 406477 6461342 4.33% 1.532% 10 5.300 5.282 5.337 VV 168400 2744341 1.84% 0.651% 11 5.398 5.376 5.425 VV 195061 2466033 1.65% 0.585% 12 5.532 5.507 5.554 PV 127692 1946859 1.31% 0.462% 13 5.684 5.624 5.710 PV 202607 2778317 1.86% 0.659% 14 5.822 5.794 5.869 VV 193534 3257584 2.18% 0.773% 15 5.989 5.961 6.021 VV 149695 2291688 1.54% 0.543% 16 6.050 6.021 6.063 VV 156490 2275299 1.53% 0.540% 17 6.077 6.063 6.092 VV 253431 3104301 2.08% 0.736% 18 6.113 6.092 6.187 VV 286191 4744825 3.18% 1.125% 19 6.267 6.226 6.286 PV 231557 2996708 2.01% 0.711% 20 6.314 6.286 6.339 VV 172900 3667867 2.46% 0.870% 21 6.394 6.339 6.449 VV 231724 7607578 5.10% 1.804% 22 6.532 6.499 6.538 VV 146130 2082037 1.40% 0.494% 23 6.623 6.595 6.660 VV 283043 3926744 2.63% 0.931% 24 6.900 6.870 6.930 PV 117475 2207873 1.48% 0.524% 25 7.030 6.981 7.054 VV 91388 1953725 1.31% 0.463% 26 7.106 7.088 7.124 PV 67720 701481 0.47% 0.166% 27 7.311 7.284 7.326 BV 101395 1371039 0.92% 0.325% 28 7.606 7.540 7.611 PV 89363 1663773 1.12% 0.395% 29 7.614 7.611 7.640 VV 71389 725416 0.49% 0.172% 30 7.688 7.640 7.701 VV 59589 1195205 0.80% 0.283% 31 7.794 7.701 7.811 VV 109548 3619525 2.43% 0.858% 32 7.814 7.811 7.831 VV 63980 644835 0.43% 0.153% 33 7.841 7.831 7.859 VV 51086 641562 0.43% 0.152% 34 7.908 7.859 7.931 VV 119170 2237412 1.50% 0.531% 35 7.957 7.931 7.972 VV 81472 1649311 1.11% 0.391% 36 7.981 7.972 7.994 VV 57955 534304 0.36% 0.127% 37 8.038 7.994 8.054 VV 62382 1634696 1.10% 0.388% 38 8.080 8.054 8.110 VV 54421 1249005 0.84% 0.296% 39 8.143 8.110 8.150 VV 29094 364754 0.24% 0.086% 40 8.190 8.150 8.214 VV 86100 1600325 1.07% 0.380% 41 8.247 8.214 8.282 VB 48619 939850 0.63% 0.223% 42 8.467 8.413 8.507 VV 113070 3658572 2.45% 0.868% 43 8.597 8.547 8.602 PV 79631 1923454 1.29% 0.456% 44 8.694 8.602 8.699 VV 23206 2001098 1.34% 0.475% 45 8.926 8.857 8.960 VV 83098 3172007 2.13% 0.752% 46 9.188 8.960 9.241 VV 119332 5296204 3.55% 1.256% 47 9.473 9.241 9.541 VV 8979761 149161006 100.00% 35.372% Sum of corrected areas: 421687819 Signal #2 : ECD2B.CH 1 2.737 2.709 2.794 PV 1219852 16403048 6.22% 1.189% 2 3.344 3.312 3.441 BV 14611699 177705816 67.33% 12.885% 3 3.628 3.586 3.659 BV 189060 2135598 0.81% 0.155% 4 4.158 4.116 4.187 BV 100170 1047581 0.40% 0.076% 5 4.255 4.229 4.297 VV 1628014 20900533 7.92% 1.515% 6 4.388 4.347 4.445 PV 608325 11514865 4.36% 0.835% 7 4.557 4.532 4.584 PV 262012 3005144 1.14% 0.218% 8 4.602 4.584 4.622 PV 153328 1825563 0.69% 0.132% 9 4.638 4.622 4.658 VV 116640 1197003 0.45% 0.087% 10 4.801 4.765 4.825 PV 291483 4551828 1.72% 0.330% 11 4.840 4.825 4.856 VV 150630 2012373 0.76% 0.146% 12 4.872 4.856 4.902 VV 134925 2321144 0.88% 0.168% 13 4.941 4.902 4.977 VV 394448 7636744 2.89% 0.554% 14 5.012 4.987 5.041 VV 171758 3314697 1.26% 0.240% 15 5.107 5.073 5.122 VV 234971 3821584 1.45% 0.277% 16 5.141 5.122 5.161 VV 410441 5967175 2.26% 0.433% 17 5.179 5.161 5.224 VV 372273 6652227 2.52% 0.482% 18 5.346 5.304 5.372 VV 366822 8401036 3.18% 0.609% 19 5.389 5.372 5.424 VV 306244 5023277 1.90% 0.364% 20 5.529 5.487 5.562 PV 147798 3669304 1.39% 0.266% 21 5.586 5.562 5.615 VV 116623 2426100 0.92% 0.176% 22 5.638 5.615 5.649 VV 97919 1482960 0.56% 0.108% 23 5.670 5.649 5.697 VV 155807 2555144 0.97% 0.185% 24 5.798 5.755 5.832 PB 99337 1923426 0.73% 0.139% 25 5.894 5.876 5.941 BV 119400 2157632 0.82% 0.156% 26 5.980 5.941 6.062 VV 364192 7356400 2.79% 0.533% 27 6.125 6.094 6.158 VV 102490 1912769 0.72% 0.139% 28 6.196 6.168 6.222 VV 182929 3366076 1.28% 0.244% 29 6.299 6.261 6.316 VV 138444 2533191 0.96% 0.184% 30 6.336 6.316 6.359 VV 115117 1946141 0.74% 0.141% 31 6.583 6.547 6.608 PV 83798 1285054 0.49% 0.093% 32 6.827 6.792 6.881 VV 338897 13309134 5.04% 0.965% 33 7.107 7.040 7.125 PV 458353 17858007 6.77% 1.295% 34 7.163 7.125 7.191 VV 497798 17104267 6.48% 1.240% 35 7.195 7.191 7.198 VV 391165 1774593 0.67% 0.129% 36 7.233 7.198 7.246 VV 381752 10648749 4.03% 0.772% 37 7.327 7.246 7.334 VV 310438 17113802 6.48% 1.241% 38 7.360 7.334 7.394 VV 369627 10632064 4.03% 0.771% 39 7.452 7.394 7.459 VV 258810 9179696 3.48% 0.666% 40 7.463 7.459 7.473 VV 240366 1939804 0.73% 0.141% 41 7.566 7.473 7.570 VV 189378 11599059 4.39% 0.841% 42 7.609 7.570 7.613 VV 177766 4361837 1.65% 0.316% 43 7.655 7.613 7.667 VV 207524 5647765 2.14% 0.410% 44 7.677 7.667 7.683 VV 173170 1579609 0.60% 0.115% 45 7.820 7.683 7.834 VV 181490 15357049 5.82% 1.114% 46 7.915 7.834 7.944 VV 325829 13299046 5.04% 0.964% 47 7.991 7.944 7.995 VV 219300 6211726 2.35% 0.450% 48 8.125 7.995 8.191 VV 17691255 263925131 100.00% 19.137% 49 8.194 8.191 8.199 VV 382630 1953232 0.74% 0.142% 50 8.349 8.199 8.357 VV 443318 36974653 14.01% 2.681% 51 8.373 8.357 8.378 VV 457529 5605569 2.12% 0.406% 52 8.630 8.378 8.637 VV 566278 74987398 28.41% 5.437% 53 8.716 8.637 8.720 VV 549926 26886231 10.19% 1.950% 54 8.832 8.720 8.839 VV 608091 41394435 15.68% 3.002% 55 8.850 8.839 8.856 VV 609243 6005637 2.28% 0.435% 56 8.860 8.856 8.867 VV 596938 4099213 1.55% 0.297% 57 8.961 8.867 8.966 VV 640370 35560494 13.47% 2.578% 58 9.093 8.966 9.102 VV 660735 52248558 19.80% 3.789% 59 9.122 9.102 9.127 VV 660735 9591787 3.63% 0.696% 60 9.148 9.127 9.161 VV 685838 13526744 5.13% 0.981% 61 9.213 9.161 9.219 VV 674502 22420475 8.50% 1.626% 62 9.226 9.219 9.237 VV 668498 7207440 2.73% 0.523% 63 9.274 9.237 9.279 VV 652686 16216302 6.14% 1.176% 64 9.353 9.279 9.382 VV 663717 39229078 14.86% 2.845% 65 9.428 9.382 9.433 VV 608165 18807150 7.13% 1.364% 66 9.457 9.433 9.463 VV 610834 10680758 4.05% 0.774% 67 9.470 9.463 9.475 VV 603552 4196893 1.59% 0.304% 68 9.513 9.475 9.534 VV 575603 19725058 7.47% 1.430% 69 9.555 9.534 9.576 VV 582487 14009217 5.31% 1.016% 70 9.631 9.576 9.636 VV 545218 19416969 7.36% 1.408% 71 9.682 9.636 9.688 VV 546375 16869209 6.39% 1.223% 72 9.769 9.688 9.774 VV 514414 26161572 9.91% 1.897% 73 9.847 9.774 9.861 VV 464993 24010872 9.10% 1.741% 74 9.948 9.861 9.957 VV 411842 24146618 9.15% 1.751% 75 10.031 9.957 10.037 VV 359531 17966318 6.81% 1.303% 76 10.057 10.037 10.062 VV 364499 5128285 1.94% 0.372% 77 10.069 10.062 10.086 VV 344258 4619715 1.75% 0.335% 78 10.093 10.086 10.099 VV 301701 2365552 0.90% 0.172% 79 10.132 10.099 10.137 VV 293131 6204581 2.35% 0.450% 80 10.234 10.137 10.242 VV 235880 15755801 5.97% 1.142% 81 10.246 10.242 10.253 VV 223409 1227143 0.46% 0.089% 82 10.296 10.253 10.304 VV 175073 5190150 1.97% 0.376% 83 10.325 10.304 10.361 VV 163482 4395171 1.67% 0.319% 84 10.364 10.361 10.369 VV 117089 487506 0.18% 0.035% 85 10.380 10.369 10.417 VV 97389 1795770 0.68% 0.130% 86 10.451 10.429 10.456 VV 39091 364160 0.14% 0.026% 87 10.464 10.456 10.469 VV 50964 202427 0.08% 0.015% 88 10.905 10.886 10.922 VV 69229 682490 0.26% 0.049% 89 11.173 11.095 11.184 VV 53502 827957 0.31% 0.060% 90 11.201 11.184 11.212 PV 41855 380752 0.14% 0.028% Sum of corrected areas: 1379118109