Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042710.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 10:22 (#1); 01 Mar 2018 10:23 (#2) Sample : J1705-03RE Misc : ALS Vial : 5 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.113 3.081 3.132 BV 115966 1352429 0.98% 0.067% 2 3.220 3.188 3.251 PV 890101 9475279 6.85% 0.471% 3 3.391 3.361 3.414 VV 264881 3522117 2.54% 0.175% 4 3.587 3.469 3.620 VV 222678 10284448 7.43% 0.512% 5 3.637 3.620 3.654 VV 219708 3595092 2.60% 0.179% 6 3.674 3.654 3.696 VV 293413 5415631 3.91% 0.269% 7 3.711 3.696 3.757 VV 252925 4347509 3.14% 0.216% 8 4.095 4.053 4.154 PV 8319256 91630542 66.21% 4.559% 9 4.388 4.367 4.422 BV 127257 1592272 1.15% 0.079% 10 4.536 4.511 4.546 PV 641204 6622889 4.79% 0.329% 11 4.556 4.546 4.614 VV 628549 7869566 5.69% 0.392% 12 4.900 4.868 4.918 VV 433047 6482298 4.68% 0.322% 13 4.992 4.918 5.017 VV 1448446 33293138 24.06% 1.656% 14 5.033 5.017 5.057 VV 638600 9147819 6.61% 0.455% 15 5.163 5.141 5.199 VV 723221 8344037 6.03% 0.415% 16 5.395 5.347 5.414 PV 72614 1355679 0.98% 0.067% 17 5.681 5.626 5.697 PV 83905 1582466 1.14% 0.079% 18 5.727 5.697 5.737 VV 84633 1329698 0.96% 0.066% 19 5.766 5.737 5.788 VV 102067 2168376 1.57% 0.108% 20 5.835 5.788 5.868 VV 129998 3349962 2.42% 0.167% 21 6.047 6.026 6.062 VV 178696 2382209 1.72% 0.119% 22 6.125 6.099 6.143 PV 233919 4381213 3.17% 0.218% 23 6.199 6.143 6.236 VV 480816 16968223 12.26% 0.844% 24 6.262 6.236 6.298 VV 511174 11536093 8.34% 0.574% 25 6.318 6.298 6.325 VV 265052 3287506 2.38% 0.164% 26 6.389 6.325 6.414 VV 433219 18059553 13.05% 0.898% 27 6.419 6.414 6.434 VV 316561 3771804 2.73% 0.188% 28 6.437 6.434 6.445 VV 292898 1856029 1.34% 0.092% 29 6.460 6.445 6.494 VV 299064 8035283 5.81% 0.400% 30 6.524 6.494 6.547 VV 522602 11211229 8.10% 0.558% 31 6.626 6.547 6.644 VV 2370732 72983031 52.73% 3.631% 32 6.666 6.644 6.762 VV 2478471 115005918 83.09% 5.722% 33 6.779 6.762 6.832 VV 860003 25095521 18.13% 1.249% 34 6.899 6.832 6.957 VV 648822 35995532 26.01% 1.791% 35 7.024 6.957 7.050 PV 868683 27632910 19.97% 1.375% 36 7.073 7.050 7.091 VV 576285 12043397 8.70% 0.599% 37 7.118 7.091 7.141 VV 705849 19119081 13.81% 0.951% 38 7.154 7.141 7.216 VV 670208 24717794 17.86% 1.230% 39 7.306 7.216 7.370 VV 1133015 58082054 41.97% 2.890% 40 7.409 7.370 7.431 VV 530753 16533271 11.95% 0.823% 41 7.442 7.431 7.453 VV 501968 6256686 4.52% 0.311% 42 7.457 7.453 7.462 VV 451422 2370465 1.71% 0.118% 43 7.549 7.462 7.557 VV 815389 35602530 25.72% 1.771% 44 7.571 7.557 7.582 VV 793727 11472125 8.29% 0.571% 45 7.605 7.582 7.623 VV 935055 20799077 15.03% 1.035% 46 7.634 7.623 7.640 VV 806872 7875764 5.69% 0.392% 47 7.681 7.640 7.729 VV 1257887 51838497 37.45% 2.579% 48 7.736 7.729 7.741 VV 742010 5172719 3.74% 0.257% 49 7.785 7.741 7.805 VV 1047693 35402965 25.58% 1.761% 50 7.842 7.805 7.886 VV 1787053 64153728 46.35% 3.192% 51 7.905 7.886 7.955 VV 1381347 42487344 30.70% 2.114% 52 8.025 7.955 8.055 VV 1974900 85702884 61.92% 4.264% 53 8.080 8.055 8.137 VV 1678735 68537773 49.52% 3.410% 54 8.182 8.137 8.216 VV 1999955 72085383 52.08% 3.586% 55 8.220 8.216 8.226 VV 1454812 9417205 6.80% 0.469% 56 8.232 8.226 8.242 VV 1437499 13439853 9.71% 0.669% 57 8.261 8.242 8.301 VV 1516980 50725862 36.65% 2.524% 58 8.348 8.301 8.389 VV 1434061 68070128 49.18% 3.387% 59 8.411 8.389 8.439 VV 1205969 34886984 25.21% 1.736% 60 8.586 8.497 8.688 VV 1652214 138403330 100.00% 6.886% 61 8.771 8.688 8.778 VV 1345296 56550838 40.86% 2.813% 62 8.783 8.778 8.809 VV 1334484 23996030 17.34% 1.194% 63 8.814 8.809 8.848 VV 1201395 26874796 19.42% 1.337% 64 8.856 8.848 8.922 VV 1059766 38229404 27.62% 1.902% 65 8.960 8.922 9.091 VV 1083079 78012211 56.37% 3.881% 66 9.188 9.114 9.281 VV 770966 50540870 36.52% 2.514% 67 9.471 9.373 9.527 VV 4039336 85937364 62.09% 4.275% 68 9.576 9.544 9.621 VV 148079 3664885 2.65% 0.182% 69 10.706 10.646 10.714 BV 50641 999848 0.72% 0.050% 70 10.779 10.714 10.784 VV 45215 1871901 1.35% 0.093% 71 10.795 10.784 10.801 VV 29221 215846 0.16% 0.011% 72 10.942 10.801 11.081 PV 1852260 112820789 81.52% 5.613% 73 11.097 11.081 11.151 VB 151028 4157275 3.00% 0.207% Sum of corrected areas: 2010032252 Signal #2 : ECD2B.CH 1 2.670 2.634 2.712 PV 149042 3129613 0.86% 0.105% 2 2.738 2.712 2.786 PV 261331 4630650 1.27% 0.156% 3 2.837 2.810 2.870 VV 180311 3230225 0.88% 0.109% 4 3.013 2.998 3.028 PV 199516 2214118 0.61% 0.075% 5 3.041 3.028 3.105 VV 254931 6135986 1.68% 0.207% 6 3.143 3.105 3.186 PB 86803 2548453 0.70% 0.086% 7 3.345 3.319 3.444 PV 10761650 129957708 35.52% 4.380% 8 3.630 3.565 3.639 PV 299910 4477504 1.22% 0.151% 9 3.665 3.639 3.675 VV 1092126 15432780 4.22% 0.520% 10 3.698 3.675 3.719 VV 2825688 44640597 12.20% 1.505% 11 3.737 3.719 3.808 VV 1706317 37940623 10.37% 1.279% 12 4.255 4.234 4.282 PV 1130936 16945608 4.63% 0.571% 13 4.288 4.282 4.322 VV 364126 7716989 2.11% 0.260% 14 4.325 4.322 4.342 VV 272095 2888283 0.79% 0.097% 15 4.388 4.342 4.411 VV 259476 8212054 2.24% 0.277% 16 4.424 4.411 4.439 VV 88068 1170120 0.32% 0.039% 17 4.444 4.439 4.457 VV 47294 306190 0.08% 0.010% 18 4.560 4.527 4.574 BV 131372 1770349 0.48% 0.060% 19 4.603 4.574 4.619 VV 226111 4300846 1.18% 0.145% 20 4.682 4.619 4.763 VV 1012698 43206282 11.81% 1.456% 21 4.779 4.763 4.791 VV 197075 2506882 0.69% 0.084% 22 4.945 4.921 4.972 VV 187444 3402064 0.93% 0.115% 23 5.014 4.972 5.032 PV 121407 2754957 0.75% 0.093% 24 5.059 5.032 5.091 VV 132505 3524487 0.96% 0.119% 25 5.102 5.091 5.117 VV 115960 1489536 0.41% 0.050% 26 5.138 5.117 5.167 VV 327255 4929785 1.35% 0.166% 27 5.283 5.252 5.292 VV 184949 2199639 0.60% 0.074% 28 5.305 5.292 5.316 VV 233089 2584786 0.71% 0.087% 29 5.331 5.316 5.379 VV 217229 4410164 1.21% 0.149% 30 5.528 5.449 5.564 BV 720706 15873189 4.34% 0.535% 31 5.583 5.564 5.606 VV 428812 9468425 2.59% 0.319% 32 5.684 5.606 5.704 VV 823675 33461809 9.14% 1.128% 33 5.714 5.704 5.761 VV 715232 14264832 3.90% 0.481% 34 5.795 5.761 5.832 PV 859066 20321679 5.55% 0.685% 35 5.842 5.832 5.876 VV 466760 11569523 3.16% 0.390% 36 5.892 5.876 5.910 VV 563492 10083143 2.76% 0.340% 37 5.922 5.910 5.950 VV 490438 9835319 2.69% 0.331% 38 5.981 5.950 6.031 VV 1038592 28327682 7.74% 0.955% 39 6.054 6.031 6.107 VV 758850 19037582 5.20% 0.642% 40 6.126 6.107 6.153 VV 436563 5878812 1.61% 0.198% 41 6.198 6.153 6.223 PV 395847 8907260 2.43% 0.300% 42 6.245 6.223 6.265 VV 450272 9345792 2.55% 0.315% 43 6.297 6.265 6.316 VV 972302 19535673 5.34% 0.658% 44 6.332 6.316 6.362 VV 770439 15422818 4.22% 0.520% 45 6.386 6.362 6.424 VV 536175 15339812 4.19% 0.517% 46 6.452 6.424 6.460 VV 366198 7606624 2.08% 0.256% 47 6.485 6.460 6.490 VV 391694 6578378 1.80% 0.222% 48 6.523 6.490 6.556 VV 445228 15254945 4.17% 0.514% 49 6.584 6.556 6.607 VV 630687 13621307 3.72% 0.459% 50 6.623 6.607 6.636 VV 425544 6718237 1.84% 0.226% 51 6.678 6.636 6.705 VV 528242 17308381 4.73% 0.583% 52 6.730 6.705 6.783 VV 442551 17267554 4.72% 0.582% 53 6.827 6.783 6.864 VV 1035271 23327993 6.38% 0.786% 54 6.958 6.893 6.974 VV 327489 13831954 3.78% 0.466% 55 7.020 6.974 7.041 VV 335552 10820256 2.96% 0.365% 56 7.100 7.041 7.142 PV 539077 16028534 4.38% 0.540% 57 7.163 7.142 7.195 VV 770088 14056778 3.84% 0.474% 58 7.209 7.195 7.226 VV 243619 4097165 1.12% 0.138% 59 7.247 7.226 7.254 VV 213460 3274077 0.89% 0.110% 60 7.269 7.254 7.286 VV 201805 3513843 0.96% 0.118% 61 7.299 7.286 7.304 VV 166079 1739852 0.48% 0.059% 62 7.358 7.304 7.377 VV 240384 7365232 2.01% 0.248% 63 7.401 7.377 7.436 VV 201434 5760806 1.57% 0.194% 64 7.521 7.436 7.576 VV 250886 13915148 3.80% 0.469% 65 7.587 7.576 7.595 VV 131637 1379264 0.38% 0.046% 66 7.640 7.595 7.676 VV 757471 16599980 4.54% 0.559% 67 7.714 7.676 7.720 VV 231685 5721090 1.56% 0.193% 68 7.755 7.720 7.781 VV 242830 8098150 2.21% 0.273% 69 7.821 7.781 7.837 VV 206511 6401483 1.75% 0.216% 70 7.860 7.837 7.874 VV 205950 4215567 1.15% 0.142% 71 7.915 7.874 7.939 VV 411263 9817162 2.68% 0.331% 72 8.125 7.939 8.171 VV 6963127 133772596 36.56% 4.509% 73 8.226 8.171 8.233 VV 513863 18571240 5.08% 0.626% 74 8.328 8.233 8.336 VV 675699 36356084 9.94% 1.225% 75 8.515 8.336 8.524 VV 920097 88452915 24.17% 2.981% 76 8.552 8.524 8.567 VV 889976 22803035 6.23% 0.769% 77 8.669 8.567 8.678 VV 1075651 61149815 16.71% 2.061% 78 8.689 8.678 8.697 VV 1059048 11471733 3.14% 0.387% 79 8.717 8.697 8.722 VV 1075850 16127037 4.41% 0.544% 80 8.726 8.722 8.742 VV 1057203 12306970 3.36% 0.415% 81 8.774 8.742 8.789 VV 989787 27200652 7.43% 0.917% 82 8.878 8.789 8.897 VV 1066164 66533813 18.18% 2.243% 83 8.955 8.897 8.959 VV 1094468 38862401 10.62% 1.310% 84 8.966 8.959 8.972 VV 1073396 8475938 2.32% 0.286% 85 8.981 8.972 8.985 VV 1054487 8134865 2.22% 0.274% 86 9.082 8.985 9.092 VV 1229791 71949595 19.66% 2.425% 87 9.206 9.092 9.211 VV 1309454 86882025 23.74% 2.928% 88 9.291 9.211 9.302 VV 1375616 73501791 20.09% 2.477% 89 9.370 9.302 9.390 VV 1416656 72696353 19.87% 2.450% 90 9.481 9.390 9.541 VV 1486794 128393451 35.09% 4.327% 91 9.718 9.541 9.797 VV 1465506 206031738 56.31% 6.944% 92 9.826 9.797 9.839 VV 1247436 30793354 8.42% 1.038% 93 10.275 9.839 10.356 VV 1160252 365903073 100.00% 12.333% 94 10.383 10.356 10.409 VV 1007094 31404986 8.58% 1.058% 95 10.458 10.409 10.496 VV 1010036 49757416 13.60% 1.677% 96 10.556 10.496 10.571 VV 947520 40799605 11.15% 1.375% 97 10.639 10.571 10.671 VV 894791 52667855 14.39% 1.775% 98 10.721 10.671 10.751 VV 902027 40741127 11.13% 1.373% 99 10.842 10.751 10.862 VV 909558 56465589 15.43% 1.903% 100 10.875 10.862 10.902 VV 848234 19411303 5.31% 0.654% 101 10.987 10.902 10.996 VV 722302 40956489 11.19% 1.380% 102 11.042 10.996 11.096 VV 728856 39951637 10.92% 1.347% 103 11.104 11.096 11.133 VV 608118 12231953 3.34% 0.412% 104 11.189 11.133 11.222 VV 611233 29121076 7.96% 0.982% 105 11.349 11.222 11.390 VV 495533 50235517 13.73% 1.693% 106 11.399 11.390 11.405 VV 411128 3505267 0.96% 0.118% 107 11.441 11.405 11.548 VV 394741 27318059 7.47% 0.921% 108 11.561 11.548 11.635 VV 253337 9882863 2.70% 0.333% 109 11.704 11.635 11.738 VV 111501 5382293 1.47% 0.181% 110 11.776 11.738 11.786 VV 46556 1083863 0.30% 0.037% Sum of corrected areas: 2966937759