Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042711.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 10:38 (#1); 01 Mar 2018 10:37 (#2) Sample : PB106954BL Misc : ALS Vial : 9 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.221 3.192 3.253 VV 844184 8250916 5.51% 1.537% 2 3.518 3.479 3.526 PV 38906 461125 0.31% 0.086% 3 3.591 3.526 3.616 VV 153478 4493746 3.00% 0.837% 4 3.641 3.616 3.662 VV 123638 2733943 1.83% 0.509% 5 3.669 3.662 3.682 VV 67717 661859 0.44% 0.123% 6 3.696 3.682 3.702 VV 38020 405243 0.27% 0.075% 7 4.096 4.064 4.220 BV 12387672 144656225 96.61% 26.946% 8 4.387 4.334 4.431 BV 185043 2348083 1.57% 0.437% 9 5.164 5.120 5.202 PV 688096 7539526 5.04% 1.404% 10 5.490 5.439 5.509 PV 200051 2098876 1.40% 0.391% 11 6.357 6.284 6.375 VV 190779 6666087 4.45% 1.242% 12 6.401 6.375 6.444 VV 196427 6635045 4.43% 1.236% 13 6.620 6.590 6.679 VV 903349 17333141 11.58% 3.229% 14 7.020 6.960 7.042 PV 179185 6793683 4.54% 1.266% 15 7.070 7.042 7.095 VV 165455 4516299 3.02% 0.841% 16 7.159 7.095 7.168 VV 176413 6435737 4.30% 1.199% 17 7.174 7.168 7.180 VV 188209 1231368 0.82% 0.229% 18 7.191 7.180 7.196 VV 182359 1625585 1.09% 0.303% 19 7.306 7.216 7.339 VV 190504 12224397 8.16% 2.277% 20 7.421 7.375 7.435 PV 109800 2666951 1.78% 0.497% 21 7.453 7.435 7.479 VV 231504 4500152 3.01% 0.838% 22 7.519 7.479 7.551 VV 260569 7964532 5.32% 1.484% 23 7.571 7.551 7.593 VV 392537 6562828 4.38% 1.223% 24 7.603 7.593 7.609 VV 167333 1520143 1.02% 0.283% 25 7.625 7.609 7.635 VV 142791 2165694 1.45% 0.403% 26 7.650 7.635 7.657 VV 137926 1695729 1.13% 0.316% 27 7.686 7.657 7.694 VV 142358 2918602 1.95% 0.544% 28 7.719 7.694 7.753 VV 266532 6590917 4.40% 1.228% 29 7.784 7.753 7.821 VV 223507 7616105 5.09% 1.419% 30 7.844 7.821 7.857 VV 141442 2889081 1.93% 0.538% 31 7.958 7.857 7.973 VV 153351 9794645 6.54% 1.825% 32 8.034 7.973 8.075 VV 145678 7371807 4.92% 1.373% 33 8.094 8.075 8.104 VV 92955 1610173 1.08% 0.300% 34 8.194 8.104 8.214 VV 75025 4092934 2.73% 0.762% 35 8.295 8.214 8.337 VB 65836 3120749 2.08% 0.581% 36 8.465 8.360 8.547 BV 118436 6762470 4.52% 1.260% 37 8.674 8.547 8.718 PV 137222 10914447 7.29% 2.033% 38 8.746 8.718 8.755 VV 129466 2670714 1.78% 0.497% 39 8.832 8.755 8.854 VV 125828 7016026 4.69% 1.307% 40 8.921 8.854 8.965 VV 191394 9606737 6.42% 1.790% 41 9.182 8.965 9.248 VV 220499 23998330 16.03% 4.470% 42 9.264 9.248 9.315 VV 122132 4071797 2.72% 0.758% 43 9.471 9.398 9.535 PV 8279779 149732056 100.00% 27.892% 44 9.549 9.535 9.557 VV 105004 1287258 0.86% 0.240% 45 9.570 9.557 9.625 VV 120586 4235504 2.83% 0.789% 46 10.099 9.985 10.120 PV 53901 2277255 1.52% 0.424% 47 10.172 10.120 10.222 VV 71765 2917317 1.95% 0.543% 48 10.264 10.222 10.295 VV 42495 1145916 0.77% 0.213% Sum of corrected areas: 536827752 Signal #2 : ECD2B.CH 1 3.345 3.242 3.469 PV 15631926 194596988 88.91% 22.100% 2 3.509 3.490 3.520 VV 94551 1327142 0.61% 0.151% 3 3.630 3.609 3.664 VV 244305 3227175 1.47% 0.367% 4 4.255 4.203 4.329 PV 793058 11399687 5.21% 1.295% 5 4.386 4.355 4.444 VV 99125 2406565 1.10% 0.273% 6 4.681 4.647 4.725 VV 290478 4479698 2.05% 0.509% 7 4.801 4.761 4.824 PV 89073 1810202 0.83% 0.206% 8 5.144 5.119 5.160 PV 43104 366808 0.17% 0.042% 9 5.545 5.486 5.567 PV 121776 4222110 1.93% 0.479% 10 5.663 5.615 5.680 VV 141067 4211755 1.92% 0.478% 11 5.797 5.749 5.837 PV 101704 3415383 1.56% 0.388% 12 5.914 5.864 5.926 VV 110209 2814422 1.29% 0.320% 13 5.978 5.950 6.060 VV 1286165 21865337 9.99% 2.483% 14 6.196 6.150 6.224 PV 63866 1341356 0.61% 0.152% 15 6.302 6.262 6.308 PV 66000 958201 0.44% 0.109% 16 6.399 6.308 6.428 VV 185218 6262629 2.86% 0.711% 17 6.439 6.428 6.452 VV 42462 432248 0.20% 0.049% 18 6.502 6.475 6.524 VV 51323 928734 0.42% 0.105% 19 6.646 6.569 6.653 BV 206108 5295871 2.42% 0.601% 20 6.667 6.653 6.737 VV 223656 8843414 4.04% 1.004% 21 6.831 6.753 6.841 VV 339751 13122564 6.00% 1.490% 22 6.859 6.841 6.876 VV 343264 6936918 3.17% 0.788% 23 6.900 6.876 6.922 VV 363282 9615270 4.39% 1.092% 24 6.989 6.943 6.993 VV 473779 12760555 5.83% 1.449% 25 7.017 6.993 7.042 VV 531271 11082909 5.06% 1.259% 26 7.126 7.042 7.136 PV 425749 20633650 9.43% 2.343% 27 7.226 7.136 7.254 VV 482271 29055647 13.27% 3.300% 28 7.259 7.254 7.264 VV 333101 1912885 0.87% 0.217% 29 7.303 7.264 7.329 VV 255255 9569376 4.37% 1.087% 30 7.402 7.329 7.433 VV 259947 12473473 5.70% 1.417% 31 7.499 7.433 7.506 VV 178233 6102383 2.79% 0.693% 32 7.522 7.506 7.555 VB 151229 2906723 1.33% 0.330% 33 7.656 7.560 7.665 BV 83827 1094062 0.50% 0.124% 34 7.680 7.665 7.718 VB 86962 1623978 0.74% 0.184% 35 7.915 7.833 7.932 PV 147741 2787131 1.27% 0.317% 36 7.958 7.932 7.963 VV 52674 777081 0.36% 0.088% 37 7.967 7.963 7.972 VV 33252 110421 0.05% 0.013% 38 8.125 7.972 8.175 PV 15982522 218877506 100.00% 24.858% 39 8.184 8.175 8.200 VV 217089 2892555 1.32% 0.329% 40 8.394 8.200 8.409 VV 270091 26178343 11.96% 2.973% 41 8.413 8.409 8.425 VV 249488 2311552 1.06% 0.263% 42 8.431 8.425 8.440 VV 226101 1932155 0.88% 0.219% 43 8.447 8.440 8.452 VV 239160 1512420 0.69% 0.172% 44 8.541 8.452 8.564 VV 283712 15754079 7.20% 1.789% 45 8.630 8.564 8.644 VV 259256 11676663 5.33% 1.326% 46 8.673 8.644 8.701 VV 220506 6101926 2.79% 0.693% 47 8.744 8.701 8.748 VV 237613 4880115 2.23% 0.554% 48 8.755 8.748 8.772 VV 251404 2731129 1.25% 0.310% 49 8.808 8.772 8.830 VV 283771 7871925 3.60% 0.894% 50 8.866 8.830 8.870 VV 296614 6396490 2.92% 0.726% 51 8.897 8.870 8.920 VV 351251 8873856 4.05% 1.008% 52 8.953 8.920 8.960 VV 271937 6057197 2.77% 0.688% 53 9.256 8.960 9.265 VV 470232 66177717 30.24% 7.516% 54 9.318 9.265 9.342 VV 383557 17712138 8.09% 2.012% 55 9.347 9.342 9.358 VV 343607 3057347 1.40% 0.347% 56 9.365 9.358 9.382 VV 311404 3803443 1.74% 0.432% 57 9.386 9.382 9.394 VV 223876 1416131 0.65% 0.161% 58 9.409 9.394 9.413 VV 226421 2440303 1.11% 0.277% 59 9.419 9.413 9.427 VV 224754 1671498 0.76% 0.190% 60 9.437 9.427 9.444 VV 196047 1840913 0.84% 0.209% 61 9.479 9.444 9.492 VV 140032 3826743 1.75% 0.435% 62 9.508 9.492 9.514 VV 99897 1266091 0.58% 0.144% 63 9.520 9.514 9.535 VV 110821 973390 0.44% 0.111% 64 9.545 9.535 9.563 VV 80395 769325 0.35% 0.087% 65 9.763 9.688 9.776 VV 72545 2137130 0.98% 0.243% 66 9.869 9.776 9.874 VV 84944 2329720 1.06% 0.265% 67 9.885 9.874 9.890 VV 91620 657995 0.30% 0.075% 68 9.900 9.890 9.904 VV 103271 583251 0.27% 0.066% 69 9.948 9.904 9.954 VV 115191 2558628 1.17% 0.291% 70 10.037 9.954 10.048 VV 135938 5722175 2.61% 0.650% 71 10.054 10.048 10.063 VV 100577 792248 0.36% 0.090% 72 10.097 10.063 10.107 VV 100540 2074040 0.95% 0.236% 73 10.134 10.107 10.139 VV 115680 1664090 0.76% 0.189% 74 10.221 10.139 10.230 VV 108947 4848274 2.22% 0.551% 75 10.237 10.230 10.244 VV 106183 750469 0.34% 0.085% 76 10.250 10.244 10.255 VV 123176 736271 0.34% 0.084% 77 10.279 10.255 10.290 VV 125724 2297565 1.05% 0.261% 78 10.295 10.290 10.312 VV 121996 1290332 0.59% 0.147% 79 10.479 10.420 10.483 PV 21296 309106 0.14% 0.035% Sum of corrected areas: 880524995