Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042712.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 10:53 Sample : PB106954BS Misc : ALS Vial : 10 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.221 3.196 3.246 VV 777858 7415873 4.42% 0.311% 2 3.580 3.473 3.599 VV 219031 5918130 3.53% 0.248% 3 3.629 3.599 3.657 VV 182372 5308381 3.17% 0.222% 4 3.662 3.657 3.669 VV 130499 796729 0.48% 0.033% 5 3.687 3.669 3.729 VV 110434 3157007 1.88% 0.132% 6 3.768 3.729 3.774 VV 63519 1553360 0.93% 0.065% 7 3.791 3.774 3.816 VV 52658 790488 0.47% 0.033% 8 4.096 4.051 4.256 BV 12944700 158882651 94.77% 6.653% 9 4.293 4.256 4.356 VV 333865 6032659 3.60% 0.253% 10 4.381 4.356 4.429 VV 547732 7721987 4.61% 0.323% 11 4.453 4.429 4.534 VV 2287544 29185609 17.41% 1.222% 12 4.558 4.534 4.576 VV 331761 3851797 2.30% 0.161% 13 4.597 4.576 4.652 VV 371679 4606202 2.75% 0.193% 14 4.776 4.747 4.792 PV 3608711 39154922 23.36% 1.640% 15 4.805 4.792 4.844 VV 1996483 24457932 14.59% 1.024% 16 4.861 4.844 4.878 VV 419746 4867098 2.90% 0.204% 17 4.915 4.904 4.936 VV 211977 2557688 1.53% 0.107% 18 4.962 4.936 5.014 VV 3397854 40729458 24.29% 1.706% 19 5.070 5.041 5.098 VV 138720 2168272 1.29% 0.091% 20 5.125 5.098 5.140 PV 973890 11270001 6.72% 0.472% 21 5.158 5.140 5.194 VV 844319 14229677 8.49% 0.596% 22 5.221 5.194 5.229 VV 5083857 52895473 31.55% 2.215% 23 5.241 5.229 5.279 VV 6533389 90289199 53.86% 3.781% 24 5.302 5.279 5.366 VV 3893321 57366780 34.22% 2.402% 25 5.396 5.366 5.441 VV 3465731 45788044 27.31% 1.917% 26 5.460 5.441 5.466 VV 369878 3949760 2.36% 0.165% 27 5.486 5.466 5.510 VV 2919522 35701512 21.30% 1.495% 28 5.529 5.510 5.556 VV 2360886 39527112 23.58% 1.655% 29 5.565 5.556 5.622 VV 1282810 15332258 9.15% 0.642% 30 5.682 5.644 5.707 PV 3167989 41807193 24.94% 1.751% 31 5.721 5.707 5.746 VV 1398729 18231422 10.87% 0.763% 32 5.765 5.746 5.789 VV 1067176 12740673 7.60% 0.534% 33 5.818 5.789 5.862 VV 2264071 34745436 20.73% 1.455% 34 5.883 5.862 5.923 VV 690562 8546810 5.10% 0.358% 35 6.049 6.022 6.094 VV 2652516 39416313 23.51% 1.651% 36 6.112 6.094 6.161 VB 467725 6698223 4.00% 0.280% 37 6.199 6.177 6.232 BV 439154 4831373 2.88% 0.202% 38 6.262 6.232 6.291 VV 3075894 36517005 21.78% 1.529% 39 6.300 6.291 6.349 VB 139332 2538470 1.51% 0.106% 40 6.464 6.434 6.486 PV 134973 1852131 1.10% 0.078% 41 6.535 6.486 6.547 VV 601681 7303692 4.36% 0.306% 42 6.563 6.547 6.594 VV 1214545 15396499 9.18% 0.645% 43 6.620 6.594 6.651 VV 2093253 27078814 16.15% 1.134% 44 6.677 6.651 6.713 VV 3517350 55325271 33.00% 2.317% 45 6.727 6.713 6.751 VV 977232 12223854 7.29% 0.512% 46 6.780 6.751 6.820 VV 6959497 82638410 49.29% 3.460% 47 6.898 6.867 6.930 PV 1107234 14166124 8.45% 0.593% 48 6.964 6.930 6.994 VV 1299608 16205159 9.67% 0.679% 49 7.031 6.994 7.054 VV 8665927 104985719 62.62% 4.396% 50 7.071 7.054 7.093 VV 2686920 32329368 19.28% 1.354% 51 7.112 7.093 7.133 VV 1775401 21038167 12.55% 0.881% 52 7.157 7.133 7.177 VV 3743914 46506288 27.74% 1.947% 53 7.187 7.177 7.224 VV 739590 8705144 5.19% 0.365% 54 7.261 7.224 7.278 PV 846026 12768829 7.62% 0.535% 55 7.307 7.278 7.330 VV 8794694 122473000 73.05% 5.129% 56 7.338 7.330 7.361 VV 1308911 16767610 10.00% 0.702% 57 7.384 7.361 7.416 VV 5860691 72528805 43.26% 3.037% 58 7.440 7.416 7.475 VV 3284679 39140865 23.35% 1.639% 59 7.516 7.494 7.521 BV 106745 911655 0.54% 0.038% 60 7.570 7.546 7.581 VV 1287686 15417772 9.20% 0.646% 61 7.605 7.581 7.656 VV 5526042 79601079 47.48% 3.333% 62 7.681 7.656 7.716 VV 2973316 40084558 23.91% 1.679% 63 7.734 7.716 7.759 VV 1541258 19677366 11.74% 0.824% 64 7.790 7.759 7.811 VV 323964 5032377 3.00% 0.211% 65 7.835 7.811 7.866 VV 1782906 24127588 14.39% 1.010% 66 7.906 7.866 7.936 VV 13494911 167648239 100.00% 7.020% 67 7.953 7.936 7.989 VV 757130 11054177 6.59% 0.463% 68 8.192 8.136 8.218 VV 5972552 102072330 60.88% 4.274% 69 8.245 8.218 8.334 VV 2399052 60483455 36.08% 2.533% 70 8.461 8.431 8.507 VV 261944 3828895 2.28% 0.160% 71 8.537 8.516 8.556 VV 133310 1784988 1.06% 0.075% 72 8.596 8.567 8.632 VV 1178653 16318091 9.73% 0.683% 73 8.830 8.792 8.874 VV 2699368 39231268 23.40% 1.643% 74 8.909 8.874 8.939 VV 156794 2802474 1.67% 0.117% 75 9.184 9.015 9.236 VV 793907 15923408 9.50% 0.667% 76 9.241 9.236 9.246 VV 22224 98775 0.06% 0.004% 77 9.471 9.422 9.522 PV 9042869 150728922 89.91% 6.312% 78 9.528 9.522 9.547 VV 39963 219129 0.13% 0.009% Sum of corrected areas: 2388059269 Signal #2 : ECD2B.CH 1 3.345 3.302 3.466 PV 15452797 195199549 59.02% 4.195% 2 3.548 3.466 3.592 VV 614361 15250932 4.61% 0.328% 3 3.597 3.592 3.606 VV 120099 862637 0.26% 0.019% 4 3.630 3.606 3.666 VV 820873 11377461 3.44% 0.245% 5 3.701 3.666 3.741 VV 2822662 36810667 11.13% 0.791% 6 3.759 3.741 3.816 VV 446798 8096064 2.45% 0.174% 7 3.857 3.816 3.882 VV 438470 5558907 1.68% 0.119% 8 3.984 3.952 4.038 PV 4450932 83192468 25.15% 1.788% 9 4.058 4.038 4.079 VV 541376 7180174 2.17% 0.154% 10 4.091 4.079 4.109 VV 240600 2806722 0.85% 0.060% 11 4.127 4.109 4.139 VV 295384 3289798 0.99% 0.071% 12 4.164 4.139 4.202 VV 3840563 56020396 16.94% 1.204% 13 4.211 4.202 4.229 VV 181161 2023841 0.61% 0.043% 14 4.276 4.229 4.290 VV 1413852 23364868 7.06% 0.502% 15 4.300 4.290 4.346 VV 919341 11724378 3.54% 0.252% 16 4.389 4.346 4.426 VV 9481562 193673109 58.56% 4.162% 17 4.445 4.426 4.531 VV 4942321 82674118 25.00% 1.777% 18 4.558 4.531 4.581 VV 4639088 57492901 17.38% 1.236% 19 4.600 4.581 4.619 VV 3831091 46871223 14.17% 1.007% 20 4.638 4.619 4.656 VV 4378181 58627194 17.73% 1.260% 21 4.666 4.656 4.759 VB 1826130 26407417 7.98% 0.568% 22 4.803 4.761 4.825 BV 4542357 60089115 18.17% 1.291% 23 4.839 4.825 4.857 VV 1948651 24105290 7.29% 0.518% 24 4.871 4.857 4.901 VV 1512780 19687964 5.95% 0.423% 25 4.943 4.901 4.982 VV 2993557 53735642 16.25% 1.155% 26 5.011 4.982 5.047 VV 909053 13560863 4.10% 0.291% 27 5.107 5.087 5.118 VV 523014 5870725 1.77% 0.126% 28 5.139 5.118 5.166 VV 3980245 51900051 15.69% 1.115% 29 5.178 5.166 5.210 VV 650036 9497234 2.87% 0.204% 30 5.229 5.210 5.257 VV 543350 7295982 2.21% 0.157% 31 5.283 5.257 5.319 VV 3991987 50458790 15.26% 1.084% 32 5.347 5.319 5.352 VV 204478 3276259 0.99% 0.070% 33 5.367 5.352 5.442 VB 303630 6054100 1.83% 0.130% 34 5.502 5.471 5.557 BV 170023 3215585 0.97% 0.069% 35 5.584 5.557 5.616 VV 885009 12128059 3.67% 0.261% 36 5.647 5.616 5.656 VV 1822510 20671090 6.25% 0.444% 37 5.682 5.656 5.704 VV 5896368 96420241 29.15% 2.072% 38 5.722 5.704 5.763 VV 2212138 44645253 13.50% 0.959% 39 5.795 5.763 5.839 VV 10545765 138912902 42.00% 2.985% 40 5.855 5.839 5.874 VV 400828 6838642 2.07% 0.147% 41 5.895 5.874 5.905 VV 1037237 12600161 3.81% 0.271% 42 5.923 5.905 5.953 VV 2676416 39883968 12.06% 0.857% 43 5.982 5.953 6.083 VV 14371121 207255184 62.66% 4.454% 44 6.127 6.095 6.176 VV 11771966 164254235 49.66% 3.530% 45 6.199 6.176 6.222 VV 1514966 23518867 7.11% 0.505% 46 6.244 6.222 6.269 VV 3623947 51132791 15.46% 1.099% 47 6.297 6.269 6.316 VV 13583094 197055706 59.58% 4.235% 48 6.333 6.316 6.364 VV 10645186 159971733 48.37% 3.438% 49 6.386 6.364 6.454 VV 5643939 93957229 28.41% 2.019% 50 6.522 6.454 6.556 VV 2024257 50704629 15.33% 1.090% 51 6.584 6.556 6.609 VV 8553383 122471851 37.03% 2.632% 52 6.621 6.609 6.645 VV 1717601 26212341 7.93% 0.563% 53 6.678 6.645 6.705 VV 5171039 82617926 24.98% 1.776% 54 6.726 6.705 6.742 VV 2899419 41562213 12.57% 0.893% 55 6.755 6.742 6.786 VV 2367801 40667278 12.30% 0.874% 56 6.826 6.786 6.866 VV 22989387 330753771 100.00% 7.108% 57 6.880 6.866 6.904 VV 1156441 21294362 6.44% 0.458% 58 6.925 6.904 6.979 VV 1298684 36106830 10.92% 0.776% 59 7.098 7.039 7.132 PV 5130981 86659074 26.20% 1.862% 60 7.163 7.132 7.277 VV 14551269 247010890 74.68% 5.308% 61 7.319 7.277 7.331 VV 405784 13024290 3.94% 0.280% 62 7.357 7.331 7.396 VV 769492 18381194 5.56% 0.395% 63 7.420 7.396 7.435 VV 602452 10707816 3.24% 0.230% 64 7.447 7.435 7.480 VV 451469 9043842 2.73% 0.194% 65 7.518 7.480 7.581 VV 2245534 40526724 12.25% 0.871% 66 7.601 7.581 7.606 VV 218615 3176424 0.96% 0.068% 67 7.652 7.606 7.684 VV 4989435 69779068 21.10% 1.500% 68 7.697 7.684 7.727 VV 450745 8488425 2.57% 0.182% 69 7.914 7.727 7.954 VV 1649419 42233409 12.77% 0.908% 70 8.125 7.954 8.199 VV 16760224 262457634 79.35% 5.640% 71 8.230 8.199 8.234 VV 373210 7666122 2.32% 0.165% 72 8.251 8.234 8.262 VV 378990 6289730 1.90% 0.135% 73 8.353 8.262 8.359 VV 422300 22641034 6.85% 0.487% 74 8.516 8.359 8.520 VV 500868 43801073 13.24% 0.941% 75 8.526 8.520 8.538 VV 503538 5008689 1.51% 0.108% 76 8.601 8.538 8.605 VV 532427 20034480 6.06% 0.431% 77 8.661 8.605 8.666 VV 548430 19198354 5.80% 0.413% 78 8.683 8.666 8.700 VV 521685 10178619 3.08% 0.219% 79 8.725 8.700 8.729 VV 594287 8444044 2.55% 0.181% 80 8.756 8.729 8.771 VV 562053 13392925 4.05% 0.288% 81 8.809 8.771 8.820 VV 598178 16373731 4.95% 0.352% 82 8.896 8.820 8.912 VV 662346 33141179 10.02% 0.712% 83 8.954 8.912 8.962 VV 612241 18171825 5.49% 0.391% 84 8.985 8.962 8.989 VV 592003 9180121 2.78% 0.197% 85 9.017 8.989 9.023 VV 611166 12006176 3.63% 0.258% 86 9.184 9.023 9.189 VV 648629 61515432 18.60% 1.322% 87 9.249 9.189 9.264 VV 654069 28142303 8.51% 0.605% 88 9.269 9.264 9.274 VV 636512 3667223 1.11% 0.079% 89 9.323 9.274 9.327 VV 612884 19473300 5.89% 0.418% 90 9.362 9.327 9.381 VV 610961 19269057 5.83% 0.414% 91 9.427 9.381 9.432 VV 588117 17674903 5.34% 0.380% 92 9.440 9.432 9.451 VV 569609 6225652 1.88% 0.134% 93 9.476 9.451 9.487 VV 548258 11889812 3.59% 0.256% 94 9.498 9.487 9.512 VV 547226 7890612 2.39% 0.170% 95 9.552 9.512 9.558 VV 555454 14486558 4.38% 0.311% 96 9.603 9.558 9.607 VV 515500 15264605 4.62% 0.328% 97 9.617 9.607 9.645 VV 530561 11199515 3.39% 0.241% 98 9.728 9.645 9.739 VV 470486 26436880 7.99% 0.568% 99 9.773 9.739 9.782 VV 455925 11204618 3.39% 0.241% 100 9.788 9.782 9.804 VV 444767 5550968 1.68% 0.119% 101 9.838 9.804 9.842 VV 403457 9011848 2.72% 0.194% 102 9.846 9.842 9.859 VV 409555 3961149 1.20% 0.085% 103 9.873 9.859 9.879 VV 402684 4593795 1.39% 0.099% 104 9.884 9.879 9.889 VV 404876 2245509 0.68% 0.048% 105 9.911 9.889 9.926 VV 388739 8352683 2.53% 0.180% 106 9.933 9.926 9.939 VV 360923 2754251 0.83% 0.059% 107 9.958 9.939 9.965 VV 372934 5483537 1.66% 0.118% 108 10.058 9.965 10.062 VV 286195 17709851 5.35% 0.381% 109 10.066 10.062 10.081 VV 280736 2835030 0.86% 0.061% 110 10.087 10.081 10.094 VV 255623 1938508 0.59% 0.042% 111 10.098 10.094 10.112 VV 251505 2443405 0.74% 0.053% 112 10.152 10.122 10.163 VV 203949 4699942 1.42% 0.101% 113 10.201 10.163 10.206 VV 167401 4294469 1.30% 0.092% 114 10.211 10.206 10.229 VV 167077 1994151 0.60% 0.043% 115 10.256 10.229 10.261 VV 127134 2324996 0.70% 0.050% 116 10.271 10.261 10.284 VV 122097 1496184 0.45% 0.032% 117 10.289 10.284 10.294 VV 112378 592318 0.18% 0.013% 118 10.364 10.344 10.381 VV 46250 597832 0.18% 0.013% Sum of corrected areas: 4653127471