Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042713.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 11:10 Sample : J1630-01MS Misc : ALS Vial : 11 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.062 3.038 3.097 PV 603146 6054572 2.18% 0.083% 2 3.163 3.137 3.186 VV 93449 1677094 0.60% 0.023% 3 3.225 3.186 3.258 PV 866003 13888915 5.00% 0.190% 4 3.303 3.258 3.367 VV 365334 16648051 5.99% 0.228% 5 3.400 3.367 3.484 VV 263974 13200620 4.75% 0.181% 6 3.500 3.484 3.562 VV 194818 5173837 1.86% 0.071% 7 3.618 3.580 3.623 PV 41168 586258 0.21% 0.008% 8 4.100 4.061 4.127 PV 17538361 193723019 69.74% 2.656% 9 4.137 4.127 4.175 VV 709819 9354942 3.37% 0.128% 10 4.298 4.256 4.359 BV 485658 9474223 3.41% 0.130% 11 4.386 4.359 4.431 PV 893828 15644992 5.63% 0.215% 12 4.458 4.431 4.509 VV 3490229 50713778 18.26% 0.695% 13 4.540 4.509 4.552 VV 382377 8313222 2.99% 0.114% 14 4.561 4.552 4.581 VV 406009 6640468 2.39% 0.091% 15 4.602 4.581 4.624 VV 975401 16562984 5.96% 0.227% 16 4.729 4.709 4.754 VV 565978 13952334 5.02% 0.191% 17 4.781 4.754 4.797 VV 5555320 68253016 24.57% 0.936% 18 4.810 4.797 4.845 VV 3479800 50936997 18.34% 0.698% 19 4.865 4.845 4.881 VV 1249599 19948299 7.18% 0.274% 20 4.895 4.881 4.908 VV 919663 13378896 4.82% 0.183% 21 4.918 4.908 4.943 VV 888125 17713336 6.38% 0.243% 22 4.967 4.943 5.003 VV 5334851 78591580 28.29% 1.078% 23 5.077 5.027 5.103 VV 1023218 40505195 14.58% 0.555% 24 5.130 5.103 5.145 VV 2286551 38973507 14.03% 0.534% 25 5.164 5.145 5.204 VV 2219446 51895498 18.68% 0.712% 26 5.226 5.204 5.235 VV 7868879 86391540 31.10% 1.185% 27 5.247 5.235 5.283 VV 9619295 147417185 53.07% 2.021% 28 5.307 5.283 5.347 VV 6619132 117477579 42.29% 1.611% 29 5.401 5.374 5.444 VV 6098257 113642579 40.91% 1.558% 30 5.464 5.444 5.471 VV 1802925 25743353 9.27% 0.353% 31 5.491 5.471 5.514 VV 5187827 82528487 29.71% 1.132% 32 5.534 5.514 5.550 VV 4788301 73527376 26.47% 1.008% 33 5.570 5.550 5.634 VV 8664170 175884309 63.32% 2.412% 34 5.687 5.634 5.710 VV 6204081 128550492 46.28% 1.763% 35 5.726 5.710 5.751 VV 3626091 65221668 23.48% 0.894% 36 5.770 5.751 5.792 VV 3109201 58087090 20.91% 0.797% 37 5.823 5.792 5.861 VV 5041249 120018007 43.21% 1.646% 38 5.888 5.861 5.916 VV 2722149 70732030 25.46% 0.970% 39 5.939 5.916 6.004 VV 1971009 94973952 34.19% 1.302% 40 6.022 6.004 6.036 VV 1780234 25375563 9.14% 0.348% 41 6.055 6.036 6.071 VV 6185879 79494093 28.62% 1.090% 42 6.076 6.071 6.099 VV 3491577 52000236 18.72% 0.713% 43 6.116 6.099 6.148 VV 3126793 73248778 26.37% 1.004% 44 6.204 6.148 6.229 VV 2767596 110029558 39.61% 1.509% 45 6.266 6.229 6.294 VV 6640183 141482674 50.94% 1.940% 46 6.308 6.294 6.332 VV 2581965 56593829 20.37% 0.776% 47 6.344 6.332 6.361 VV 2357745 40728309 14.66% 0.558% 48 6.398 6.361 6.406 VV 2437195 64500328 23.22% 0.884% 49 6.410 6.406 6.428 VV 2446907 31596167 11.38% 0.433% 50 6.538 6.489 6.551 VV 3517421 100826209 36.30% 1.383% 51 6.567 6.551 6.599 VV 4280779 96590057 34.77% 1.324% 52 6.624 6.599 6.657 VV 9982845 186669875 67.20% 2.560% 53 6.681 6.657 6.697 VV 7479465 126025903 45.37% 1.728% 54 6.702 6.697 6.718 VV 4626039 52160827 18.78% 0.715% 55 6.732 6.718 6.757 VV 4205739 83281217 29.98% 1.142% 56 6.784 6.757 6.831 VV 11657781 237476206 85.50% 3.256% 57 6.843 6.831 6.870 VV 3098251 45784837 16.48% 0.628% 58 6.902 6.870 6.934 PV 4480955 100859727 36.31% 1.383% 59 6.968 6.934 6.999 VV 4564820 134411371 48.39% 1.843% 60 7.036 6.999 7.059 VV 14116471 240936531 86.74% 3.304% 61 7.076 7.059 7.097 VV 6390638 106706039 38.42% 1.463% 62 7.116 7.097 7.138 VV 5139519 95050956 34.22% 1.303% 63 7.161 7.138 7.182 VV 7860729 133564640 48.09% 1.831% 64 7.192 7.182 7.241 VV 3570560 99809508 35.93% 1.369% 65 7.267 7.241 7.282 VV 3496353 69925948 25.17% 0.959% 66 7.310 7.282 7.332 VV 12671796 210822885 75.90% 2.891% 67 7.342 7.332 7.365 VV 4195293 70039866 25.22% 0.960% 68 7.389 7.365 7.418 VV 9768956 164851303 59.35% 2.260% 69 7.444 7.418 7.486 VV 6338262 138109584 49.72% 1.894% 70 7.574 7.486 7.584 VV 3561800 140517046 50.59% 1.927% 71 7.609 7.584 7.657 VV 9300110 191112588 68.80% 2.621% 72 7.686 7.657 7.719 VV 5937264 121417113 43.71% 1.665% 73 7.739 7.719 7.751 VV 3947949 62126867 22.37% 0.852% 74 7.787 7.751 7.823 VV 6207873 217211426 78.20% 2.978% 75 7.837 7.823 7.880 VV 5160287 115394261 41.54% 1.582% 76 7.909 7.880 7.939 VV 19248836 277763203 100.00% 3.809% 77 7.957 7.939 7.999 VV 2554219 69132066 24.89% 0.948% 78 8.195 8.129 8.222 VV 9167003 203608136 73.30% 2.792% 79 8.247 8.222 8.258 VV 4180499 70994408 25.56% 0.973% 80 8.266 8.258 8.306 VV 3890437 63658429 22.92% 0.873% 81 8.466 8.442 8.501 VV 1150316 34344871 12.36% 0.471% 82 8.538 8.501 8.556 VV 891682 26005513 9.36% 0.357% 83 8.601 8.556 8.636 VV 2175951 51862181 18.67% 0.711% 84 8.746 8.692 8.789 VV 561581 27036804 9.73% 0.371% 85 8.835 8.789 8.882 VV 3649722 66890353 24.08% 0.917% 86 8.916 8.882 8.974 VV 363370 12560282 4.52% 0.172% 87 9.033 8.974 9.043 VV 38115 2362733 0.85% 0.032% 88 9.191 9.139 9.218 PV 1018458 15565350 5.60% 0.213% 89 9.237 9.218 9.260 VV 127998 1974993 0.71% 0.027% 90 9.478 9.404 9.527 BV 9429805 163799234 58.97% 2.246% 91 9.613 9.554 9.635 VV 609084 16517827 5.95% 0.226% 92 9.665 9.635 9.795 VV 562492 34239568 12.33% 0.470% 93 9.862 9.795 9.902 PV 488369 12160282 4.38% 0.167% 94 9.917 9.902 9.996 VB 132571 3495339 1.26% 0.048% Sum of corrected areas: 7292705181 Signal #2 : ECD2B.CH 1 2.534 2.506 2.586 BV 561992 7784848 1.37% 0.045% 2 2.632 2.610 2.659 VV 248118 4195741 0.74% 0.024% 3 2.677 2.659 2.710 VV 162592 2878114 0.51% 0.017% 4 2.831 2.791 2.839 PV 69710 1213276 0.21% 0.007% 5 2.843 2.839 2.851 VV 36052 167327 0.03% 0.001% 6 3.009 2.982 3.037 VV 194476 3688035 0.65% 0.021% 7 3.344 3.309 3.418 VV 22613091 304024848 53.69% 1.767% 8 3.445 3.418 3.466 VV 808848 20822587 3.68% 0.121% 9 3.504 3.466 3.527 VV 1553948 41681167 7.36% 0.242% 10 3.547 3.527 3.588 VV 1803910 49287066 8.70% 0.286% 11 3.629 3.606 3.665 VV 2371834 58800816 10.38% 0.342% 12 3.700 3.665 3.736 VV 5649372 113288073 20.01% 0.658% 13 3.742 3.736 3.752 VV 1731994 17229535 3.04% 0.100% 14 3.757 3.752 3.764 VV 1749550 12278570 2.17% 0.071% 15 3.827 3.787 3.840 VV 1830698 53450502 9.44% 0.311% 16 3.857 3.840 3.876 VV 2428262 42416018 7.49% 0.247% 17 3.904 3.876 3.913 VV 1879613 39643366 7.00% 0.230% 18 3.948 3.913 3.954 VV 2059595 49406144 8.72% 0.287% 19 3.983 3.954 4.056 VV 8640132 253675227 44.80% 1.474% 20 4.096 4.079 4.109 VV 2581414 42508146 7.51% 0.247% 21 4.124 4.109 4.139 VV 2875692 48753399 8.61% 0.283% 22 4.164 4.139 4.199 VV 7844270 168352575 29.73% 0.978% 23 4.209 4.199 4.231 VV 2999967 55615839 9.82% 0.323% 24 4.276 4.231 4.290 VV 4958544 137390250 24.26% 0.799% 25 4.300 4.290 4.346 VV 4316152 118356250 20.90% 0.688% 26 4.389 4.346 4.426 VV 17151971 430005345 75.93% 2.499% 27 4.444 4.426 4.500 VV 10370599 264691644 46.74% 1.538% 28 4.558 4.531 4.582 VV 10471347 191808743 33.87% 1.115% 29 4.601 4.582 4.619 VV 9247998 150546626 26.58% 0.875% 30 4.639 4.619 4.657 VV 10177354 174172415 30.76% 1.012% 31 4.667 4.657 4.720 VV 6612402 185524602 32.76% 1.078% 32 4.805 4.763 4.825 PV 7326249 124599276 22.00% 0.724% 33 4.839 4.825 4.856 VV 5366724 83112735 14.68% 0.483% 34 4.873 4.856 4.882 VV 5368427 71201665 12.57% 0.414% 35 4.898 4.882 4.915 VV 8000704 127302394 22.48% 0.740% 36 4.943 4.915 4.980 VV 8277321 231959509 40.96% 1.348% 37 5.013 4.980 5.051 VV 5450670 194941859 34.42% 1.133% 38 5.073 5.051 5.087 VV 4347205 94436857 16.68% 0.549% 39 5.107 5.087 5.121 VV 5055087 92982064 16.42% 0.540% 40 5.141 5.121 5.147 VV 9927098 117621116 20.77% 0.684% 41 5.164 5.147 5.215 VV 18998007 412657297 72.87% 2.398% 42 5.229 5.215 5.258 VV 5328904 127232018 22.47% 0.739% 43 5.284 5.258 5.318 VV 9500750 209798430 37.05% 1.219% 44 5.368 5.318 5.381 VV 4660018 162212537 28.64% 0.943% 45 5.386 5.381 5.417 VV 4552314 94388881 16.67% 0.549% 46 5.427 5.417 5.442 VV 4256749 65887525 11.63% 0.383% 47 5.457 5.442 5.488 VV 4237324 79221754 13.99% 0.460% 48 5.587 5.488 5.611 PV 4449126 216219147 38.18% 1.257% 49 5.648 5.611 5.657 VV 6118666 131448222 23.21% 0.764% 50 5.683 5.657 5.705 VV 10691513 222646992 39.32% 1.294% 51 5.721 5.705 5.767 VV 6423449 193368479 34.15% 1.124% 52 5.796 5.767 5.839 VV 17257824 339838192 60.01% 1.975% 53 5.856 5.839 5.873 VV 4086641 80222085 14.17% 0.466% 54 5.896 5.873 5.906 VV 5161962 91800238 16.21% 0.534% 55 5.924 5.906 5.953 VV 7091677 149909401 26.47% 0.871% 56 5.982 5.953 6.032 VV 28271585 500301139 88.35% 2.908% 57 6.046 6.032 6.070 VV 3496596 67092842 11.85% 0.390% 58 6.128 6.070 6.174 VV 17928520 392899782 69.38% 2.284% 59 6.200 6.174 6.221 VV 4930294 111217658 19.64% 0.646% 60 6.246 6.221 6.271 VV 7538079 155424737 27.45% 0.903% 61 6.299 6.271 6.318 VV 21007249 343650675 60.68% 1.997% 62 6.334 6.318 6.367 VV 17111839 294589267 52.02% 1.712% 63 6.388 6.367 6.438 VV 10030950 226266031 39.96% 1.315% 64 6.523 6.438 6.559 VV 5378923 261036493 46.10% 1.517% 65 6.586 6.559 6.611 VV 14144283 241233609 42.60% 1.402% 66 6.623 6.611 6.647 VV 4730188 85886224 15.17% 0.499% 67 6.680 6.647 6.708 VV 9120400 194588030 34.36% 1.131% 68 6.728 6.708 6.743 VV 5687759 94334145 16.66% 0.548% 69 6.757 6.743 6.789 VV 5364466 116461875 20.57% 0.677% 70 6.829 6.789 6.871 VV 31501867 535569736 94.57% 3.113% 71 6.883 6.871 6.906 VV 3434669 67855239 11.98% 0.394% 72 6.927 6.906 6.981 VV 3635996 132660139 23.43% 0.771% 73 7.017 6.981 7.042 VV 2706439 89495789 15.80% 0.520% 74 7.101 7.042 7.131 VV 9177688 231562613 40.89% 1.346% 75 7.164 7.131 7.287 VV 21936016 566291482 100.00% 3.291% 76 7.318 7.287 7.336 VV 2406291 68699518 12.13% 0.399% 77 7.359 7.336 7.397 VV 2850942 89702885 15.84% 0.521% 78 7.421 7.397 7.438 VV 2789151 60895941 10.75% 0.354% 79 7.448 7.438 7.473 VV 2529231 51164413 9.03% 0.297% 80 7.520 7.473 7.566 VV 4893791 160318213 28.31% 0.932% 81 7.569 7.566 7.594 VV 2242319 37156359 6.56% 0.216% 82 7.654 7.594 7.684 VV 8233981 197738744 34.92% 1.149% 83 7.697 7.684 7.729 VV 2540198 62537087 11.04% 0.363% 84 7.767 7.729 7.782 VV 2219155 70286273 12.41% 0.409% 85 7.800 7.782 7.815 VV 2230671 43633946 7.71% 0.254% 86 7.822 7.815 7.829 VV 2205681 17807672 3.14% 0.103% 87 7.846 7.829 7.864 VV 2189314 45236266 7.99% 0.263% 88 7.916 7.864 7.947 VV 3927423 131151829 23.16% 0.762% 89 8.011 7.947 8.022 VV 2715069 107861943 19.05% 0.627% 90 8.058 8.022 8.069 VV 2895191 77913471 13.76% 0.453% 91 8.082 8.069 8.097 VV 2936447 49235727 8.69% 0.286% 92 8.127 8.097 8.177 VV 21214993 357650792 63.16% 2.079% 93 8.182 8.177 8.187 VV 2418162 14435184 2.55% 0.084% 94 8.253 8.187 8.274 VV 2435400 124891889 22.05% 0.726% 95 8.346 8.274 8.372 VV 2469381 140526346 24.82% 0.817% 96 8.397 8.372 8.402 VV 2499298 44027911 7.77% 0.256% 97 8.474 8.402 8.497 VV 2518950 141196700 24.93% 0.821% 98 8.529 8.497 8.551 VV 2535935 79706289 14.08% 0.463% 99 8.648 8.551 8.670 VV 2593415 179020310 31.61% 1.040% 100 8.706 8.670 8.722 VV 2583907 79538800 14.05% 0.462% 101 8.814 8.722 8.833 VV 2846492 179585180 31.71% 1.044% 102 8.837 8.833 8.854 VV 2778058 35675673 6.30% 0.207% 103 8.874 8.854 8.893 VV 2766526 64385911 11.37% 0.374% 104 8.923 8.893 8.927 VV 2720842 55494279 9.80% 0.323% 105 8.939 8.927 8.946 VV 2738261 30045425 5.31% 0.175% 106 9.075 8.946 9.084 VV 2812330 228597926 40.37% 1.329% 107 9.099 9.084 9.107 VV 2779746 38460150 6.79% 0.224% 108 9.179 9.107 9.187 VV 2804489 133261369 23.53% 0.775% 109 9.221 9.187 9.234 VV 2786408 77449371 13.68% 0.450% 110 9.240 9.234 9.247 VV 2770768 22801567 4.03% 0.133% 111 9.299 9.247 9.304 VV 2787656 94428521 16.67% 0.549% 112 9.309 9.304 9.313 VV 2783255 15534895 2.74% 0.090% 113 9.338 9.313 9.363 VV 2746102 81706988 14.43% 0.475% 114 9.415 9.363 9.452 VV 2694958 140858323 24.87% 0.819% 115 9.589 9.452 9.609 VV 2643246 242813944 42.88% 1.411% 116 9.623 9.609 9.627 VV 2609976 28767028 5.08% 0.167% 117 9.694 9.627 9.711 VV 2592495 129366906 22.84% 0.752% 118 9.717 9.711 9.759 VV 2521105 53919035 9.52% 0.313% 119 9.884 9.759 9.919 VV 2236884 180614340 31.89% 1.050% 120 10.019 9.919 10.035 VV 2248827 149812651 26.46% 0.871% 121 10.046 10.035 10.067 VV 2222058 41902821 7.40% 0.244% 122 10.071 10.067 10.079 VV 2143304 14461612 2.55% 0.084% 123 10.154 10.079 10.165 VV 2187875 112005034 19.78% 0.651% 124 10.201 10.165 10.210 VV 2180852 58012697 10.24% 0.337% 125 10.215 10.210 10.241 VV 2156841 38904494 6.87% 0.226% 126 10.252 10.241 10.258 VV 2135627 22356738 3.95% 0.130% 127 10.279 10.258 10.284 VV 2149206 33248335 5.87% 0.193% 128 10.288 10.284 10.335 VV 2146993 62013312 10.95% 0.360% 129 10.371 10.335 10.424 VV 2018198 102832163 18.16% 0.598% 130 10.486 10.424 10.493 VV 1951289 77610057 13.70% 0.451% 131 10.540 10.493 10.556 VV 1912581 71112473 12.56% 0.413% 132 10.559 10.556 10.563 VV 1871754 7520656 1.33% 0.044% 133 10.568 10.563 10.576 VV 1873715 15151006 2.68% 0.088% 134 10.589 10.576 10.604 VV 1870422 30876785 5.45% 0.179% 135 10.629 10.604 10.672 VV 1841409 69521046 12.28% 0.404% 136 10.734 10.672 10.745 VV 1677294 69528470 12.28% 0.404% 137 10.755 10.745 10.760 VV 1651021 14756234 2.61% 0.086% 138 10.781 10.760 10.829 VV 1654034 47538916 8.39% 0.276% 139 10.919 10.829 10.956 PV 1372277 76073569 13.43% 0.442% 140 10.991 10.956 11.034 VV 1310423 55479286 9.80% 0.322% 141 11.101 11.034 11.143 VV 1149995 69486364 12.27% 0.404% 142 11.208 11.143 11.214 VV 1019443 43586745 7.70% 0.253% 143 11.223 11.214 11.239 VV 1024386 14912505 2.63% 0.087% 144 11.254 11.239 11.270 VV 966415 17434382 3.08% 0.101% 145 11.275 11.270 11.289 VV 936949 10428253 1.84% 0.061% 146 11.301 11.289 11.305 VV 886154 8500802 1.50% 0.049% 147 11.311 11.305 11.323 VV 885523 9226935 1.63% 0.054% 148 11.332 11.323 11.339 VV 844756 7756952 1.37% 0.045% 149 11.345 11.339 11.359 VV 817378 9628823 1.70% 0.056% 150 11.386 11.359 11.391 VV 757384 14235448 2.51% 0.083% 151 11.426 11.391 11.433 VV 707333 18136288 3.20% 0.105% 152 11.452 11.433 11.497 VV 696900 23656321 4.18% 0.137% 153 11.558 11.497 11.571 VV 487095 22288140 3.94% 0.130% 154 11.699 11.571 11.707 VV 256975 25626064 4.53% 0.149% 155 11.731 11.707 11.754 VV 216191 4942132 0.87% 0.029% 156 11.766 11.754 11.800 VV 121322 2021198 0.36% 0.012% Sum of corrected areas: 17205770316