Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042714.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 11:25 Sample : J1630-01MSD Misc : ALS Vial : 12 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.058 3.039 3.102 BV 544217 5608884 2.54% 0.108% 2 3.221 3.183 3.252 PV 522377 5881050 2.66% 0.114% 3 3.591 3.552 3.614 PV 165630 3454168 1.56% 0.067% 4 3.635 3.614 3.661 VV 132928 2740589 1.24% 0.053% 5 3.666 3.661 3.670 VV 58251 296449 0.13% 0.006% 6 3.682 3.670 3.701 VV 81371 825642 0.37% 0.016% 7 4.096 4.054 4.124 PV 16693242 184169816 83.32% 3.555% 8 4.132 4.124 4.187 VV 536029 7395655 3.35% 0.143% 9 4.292 4.254 4.351 BV 450618 8452412 3.82% 0.163% 10 4.382 4.351 4.429 PV 796501 11925874 5.40% 0.230% 11 4.453 4.429 4.520 VV 3201091 40706162 18.42% 0.786% 12 4.598 4.576 4.641 VV 514060 6638249 3.00% 0.128% 13 4.777 4.749 4.792 VV 4881596 54974097 24.87% 1.061% 14 4.805 4.792 4.842 VV 2871053 36833331 16.66% 0.711% 15 4.861 4.842 4.877 VV 747178 9841138 4.45% 0.190% 16 4.891 4.877 4.904 VV 467466 6038586 2.73% 0.117% 17 4.915 4.904 4.938 VV 485140 8731647 3.95% 0.169% 18 4.962 4.938 5.019 VV 4848236 66515592 30.09% 1.284% 19 5.071 5.039 5.100 VV 574878 17323868 7.84% 0.334% 20 5.125 5.100 5.141 VV 1825064 27248724 12.33% 0.526% 21 5.156 5.141 5.198 VV 1583097 34562033 15.64% 0.667% 22 5.222 5.198 5.230 VV 7294546 78700296 35.61% 1.519% 23 5.242 5.230 5.279 VV 9298899 136296316 61.66% 2.631% 24 5.303 5.279 5.341 VV 6073826 98271992 44.46% 1.897% 25 5.397 5.370 5.442 VV 5541366 94742829 42.86% 1.829% 26 5.460 5.442 5.466 VV 1364423 17303239 7.83% 0.334% 27 5.486 5.466 5.510 VV 4727217 69382422 31.39% 1.339% 28 5.530 5.510 5.551 VV 4238665 71030648 32.14% 1.371% 29 5.566 5.551 5.630 VV 4585622 97428595 44.08% 1.881% 30 5.683 5.630 5.707 VV 5573401 107466547 48.62% 2.075% 31 5.722 5.707 5.745 VV 3119023 50823941 22.99% 0.981% 32 5.766 5.745 5.789 VV 2617946 49104609 22.22% 0.948% 33 5.820 5.789 5.857 VV 4469070 100193819 45.33% 1.934% 34 5.884 5.857 5.912 VV 2276644 56044951 25.36% 1.082% 35 6.018 6.000 6.033 VV 1430516 22945698 10.38% 0.443% 36 6.051 6.033 6.095 VV 5370698 114869610 51.97% 2.218% 37 6.111 6.095 6.147 VV 2632195 63461113 28.71% 1.225% 38 6.200 6.147 6.231 VV 2320538 92975815 42.06% 1.795% 39 6.262 6.231 6.289 VV 5901693 114217053 51.67% 2.205% 40 6.302 6.289 6.332 VV 2106068 51324616 23.22% 0.991% 41 6.340 6.332 6.414 VV 1864055 85652879 38.75% 1.653% 42 6.462 6.414 6.489 VV 1878572 76632488 34.67% 1.479% 43 6.535 6.489 6.547 VV 2354457 61912903 28.01% 1.195% 44 6.564 6.547 6.593 VV 3413559 71542661 32.37% 1.381% 45 6.620 6.593 6.652 VV 7769468 143982617 65.14% 2.780% 46 6.677 6.652 6.715 VV 6728842 156926490 71.00% 3.029% 47 6.728 6.715 6.753 VV 3602586 68856601 31.15% 1.329% 48 6.781 6.753 6.826 VV 11167743 208463085 94.31% 4.024% 49 6.839 6.826 6.867 VV 2522136 42867415 19.39% 0.828% 50 6.898 6.867 6.929 PV 3851714 83751586 37.89% 1.617% 51 6.964 6.929 6.991 VV 3804597 99501480 45.02% 1.921% 52 7.031 6.991 7.055 VV 13259673 209618475 94.84% 4.047% 53 7.073 7.055 7.093 VV 5201075 80504520 36.42% 1.554% 54 7.113 7.093 7.134 VV 3884047 64387795 29.13% 1.243% 55 7.157 7.134 7.178 VV 6594436 97724802 44.21% 1.887% 56 7.188 7.178 7.239 VV 2171027 49971389 22.61% 0.965% 57 7.264 7.239 7.279 VV 1907723 32177434 14.56% 0.621% 58 7.307 7.279 7.329 VV 11648377 168022287 76.02% 3.244% 59 7.338 7.329 7.361 VV 2301544 32652726 14.77% 0.630% 60 7.386 7.361 7.415 VV 7970089 105372040 47.67% 2.034% 61 7.441 7.415 7.475 VB 4312192 54453669 24.64% 1.051% 62 7.571 7.504 7.581 BV 1537532 17895554 8.10% 0.345% 63 7.605 7.581 7.655 VV 7102225 103865989 46.99% 2.005% 64 7.683 7.655 7.716 PV 3823292 51828554 23.45% 1.001% 65 7.735 7.716 7.749 VV 2033486 26867553 12.16% 0.519% 66 7.783 7.749 7.819 VV 3430801 106628289 48.24% 2.058% 67 7.835 7.819 7.875 VV 3076670 49968307 22.61% 0.965% 68 7.905 7.875 7.936 VV 17656785 221032758 100.00% 4.267% 69 7.953 7.936 7.991 VV 954063 12587676 5.69% 0.243% 70 8.034 7.991 8.044 PV 101431 1852394 0.84% 0.036% 71 8.191 8.135 8.218 VV 8049315 133375523 60.34% 2.575% 72 8.243 8.218 8.255 VV 3061674 46966491 21.25% 0.907% 73 8.262 8.255 8.304 VV 2734735 29728852 13.45% 0.574% 74 8.463 8.382 8.502 BV 405938 10145029 4.59% 0.196% 75 8.538 8.502 8.554 VV 352592 7065991 3.20% 0.136% 76 8.562 8.554 8.569 VV 258116 2206733 1.00% 0.043% 77 8.597 8.569 8.641 VV 1754406 30932206 13.99% 0.597% 78 8.731 8.688 8.787 VV 333022 13395180 6.06% 0.259% 79 8.831 8.787 8.869 PV 3493624 53530584 24.22% 1.033% 80 8.910 8.869 8.942 VV 375130 10454123 4.73% 0.202% 81 8.974 8.942 9.017 VB 122793 4279274 1.94% 0.083% 82 9.186 9.032 9.216 BV 999978 15325290 6.93% 0.296% 83 9.231 9.216 9.261 VB 85339 1359170 0.61% 0.026% 84 9.471 9.296 9.547 BV 9876444 172231101 77.92% 3.325% 85 9.607 9.547 9.629 VV 209254 6000305 2.71% 0.116% 86 9.659 9.629 9.679 VV 185759 5071251 2.29% 0.098% 87 9.697 9.679 9.791 VB 173058 6499794 2.94% 0.125% 88 9.851 9.797 10.011 BB 496456 17322800 7.84% 0.334% Sum of corrected areas: 5180140188 Signal #2 : ECD2B.CH 1 2.536 2.512 2.589 BV 538198 7044532 1.38% 0.048% 2 2.635 2.589 2.662 PV 106141 1794341 0.35% 0.012% 3 3.345 3.306 3.419 VV 21093819 285279541 55.77% 1.930% 4 3.504 3.482 3.529 VV 1222203 29143590 5.70% 0.197% 5 3.548 3.529 3.582 VV 1614703 39177278 7.66% 0.265% 6 3.630 3.582 3.669 VV 2165107 70863770 13.85% 0.479% 7 3.701 3.669 3.747 VV 5220015 110755829 21.65% 0.749% 8 3.758 3.747 3.786 VV 1565782 34829161 6.81% 0.236% 9 3.824 3.786 3.840 VV 1673371 49491110 9.68% 0.335% 10 3.857 3.840 3.876 VV 2213141 39184265 7.66% 0.265% 11 3.983 3.876 4.049 VV 8120204 307940275 60.20% 2.083% 12 4.061 4.049 4.080 VV 2333271 41350834 8.08% 0.280% 13 4.094 4.080 4.109 VV 2424055 41324049 8.08% 0.280% 14 4.126 4.109 4.139 VV 2662015 44001141 8.60% 0.298% 15 4.165 4.139 4.199 VV 7407172 157008031 30.70% 1.062% 16 4.209 4.199 4.233 VV 2731182 53975270 10.55% 0.365% 17 4.276 4.233 4.290 VV 4641869 119786429 23.42% 0.810% 18 4.300 4.290 4.346 VV 3989333 108446649 21.20% 0.734% 19 4.389 4.346 4.426 VV 16355923 409676443 80.09% 2.772% 20 4.445 4.426 4.529 VV 9871280 305976831 59.82% 2.070% 21 4.558 4.529 4.581 VV 9866910 184385840 36.05% 1.248% 22 4.600 4.581 4.619 VV 8879592 144783137 28.31% 0.980% 23 4.639 4.619 4.657 VV 9591238 163047526 31.88% 1.103% 24 4.666 4.657 4.721 VV 6227287 174565428 34.13% 1.181% 25 4.804 4.763 4.825 PV 8572315 150445826 29.41% 1.018% 26 4.838 4.825 4.856 VV 5798465 87835714 17.17% 0.594% 27 4.872 4.856 4.887 VV 5557488 90250967 17.64% 0.611% 28 4.897 4.887 4.909 VV 4939211 60488108 11.83% 0.409% 29 4.943 4.909 4.979 VV 8057594 233425700 45.64% 1.579% 30 5.012 4.979 5.047 VV 5134100 176399969 34.49% 1.193% 31 5.072 5.047 5.087 VV 3999380 94492806 18.47% 0.639% 32 5.106 5.087 5.119 VV 4690854 83213621 16.27% 0.563% 33 5.140 5.119 5.148 VV 9547937 126837120 24.80% 0.858% 34 5.163 5.148 5.213 VV 12480269 287641201 56.23% 1.946% 35 5.229 5.213 5.259 VV 4784041 120667150 23.59% 0.816% 36 5.283 5.259 5.317 VV 9064405 193558760 37.84% 1.310% 37 5.347 5.317 5.355 VV 4210893 88563351 17.31% 0.599% 38 5.367 5.355 5.382 VV 4256916 67395881 13.18% 0.456% 39 5.386 5.382 5.439 VV 4157336 134578065 26.31% 0.911% 40 5.450 5.439 5.488 VV 3823119 81314169 15.90% 0.550% 41 5.586 5.488 5.614 PV 4463076 229258921 44.82% 1.551% 42 5.647 5.614 5.656 VV 5795560 115215326 22.52% 0.780% 43 5.682 5.656 5.704 VV 10651286 219127631 42.84% 1.483% 44 5.721 5.704 5.764 VV 6215725 176405357 34.49% 1.194% 45 5.795 5.764 5.839 VV 16963158 330541249 64.62% 2.236% 46 5.854 5.839 5.872 VV 3684823 70397293 13.76% 0.476% 47 5.894 5.872 5.905 VV 4752478 82664256 16.16% 0.559% 48 5.923 5.905 5.952 VV 6660555 138696958 27.12% 0.938% 49 5.981 5.952 6.032 VV 25657090 451636942 88.30% 3.056% 50 6.044 6.032 6.068 VV 3072346 59340353 11.60% 0.401% 51 6.126 6.068 6.174 VV 18230788 379501810 74.19% 2.568% 52 6.199 6.174 6.221 VV 4676882 104976319 20.52% 0.710% 53 6.245 6.221 6.270 VV 7272019 140056823 27.38% 0.948% 54 6.298 6.270 6.317 VV 20416258 331871216 64.88% 2.245% 55 6.333 6.317 6.365 VV 16513381 280293891 54.80% 1.896% 56 6.386 6.365 6.445 VV 9679086 223081157 43.61% 1.509% 57 6.522 6.488 6.556 VV 4911717 142238559 27.81% 0.962% 58 6.584 6.556 6.610 VV 13795615 228251143 44.62% 1.544% 59 6.621 6.610 6.646 VV 4189578 75430917 14.75% 0.510% 60 6.678 6.646 6.706 VV 8536266 174773690 34.17% 1.182% 61 6.726 6.706 6.742 VV 5325065 87397963 17.09% 0.591% 62 6.755 6.742 6.787 VV 4859638 100671439 19.68% 0.681% 63 6.827 6.787 6.868 VV 31194988 511502985 100.00% 3.461% 64 6.880 6.868 6.905 VV 2945153 58464809 11.43% 0.396% 65 6.925 6.905 6.984 VV 3061072 114613676 22.41% 0.775% 66 7.014 6.984 7.041 VV 2192493 67244007 13.15% 0.455% 67 7.099 7.041 7.132 VV 8549130 209472122 40.95% 1.417% 68 7.162 7.132 7.283 VV 21168303 497128474 97.19% 3.363% 69 7.318 7.283 7.326 VV 1849707 45735012 8.94% 0.309% 70 7.327 7.326 7.333 VV 1821708 7571603 1.48% 0.051% 71 7.356 7.333 7.392 VV 2284706 67095621 13.12% 0.454% 72 7.419 7.392 7.437 VV 2162995 50203973 9.81% 0.340% 73 7.446 7.437 7.475 VV 1901118 41627887 8.14% 0.282% 74 7.518 7.475 7.571 VV 4374065 128976829 25.22% 0.873% 75 7.597 7.571 7.604 VV 1631983 32372724 6.33% 0.219% 76 7.652 7.604 7.684 VV 7872334 156981414 30.69% 1.062% 77 7.695 7.684 7.725 VV 1956886 43676139 8.54% 0.296% 78 7.769 7.725 7.773 VV 1603695 45910821 8.98% 0.311% 79 7.779 7.773 7.784 VV 1583519 9792969 1.91% 0.066% 80 7.806 7.784 7.812 VV 1583743 26895049 5.26% 0.182% 81 7.841 7.812 7.859 VV 1567700 42915567 8.39% 0.290% 82 7.915 7.859 7.949 VV 3366660 106599589 20.84% 0.721% 83 8.019 7.949 8.029 VV 1775792 80213864 15.68% 0.543% 84 8.058 8.029 8.065 VV 1834961 38932436 7.61% 0.263% 85 8.126 8.065 8.186 VV 21412071 382736742 74.83% 2.590% 86 8.255 8.186 8.274 VV 1802730 93602971 18.30% 0.633% 87 8.354 8.274 8.369 VV 1860175 103658859 20.27% 0.701% 88 8.472 8.369 8.492 VV 1896685 137518446 26.89% 0.930% 89 8.520 8.492 8.549 VV 1903496 63304415 12.38% 0.428% 90 8.578 8.549 8.583 VV 1919519 37281743 7.29% 0.252% 91 8.646 8.583 8.656 VV 1954895 84497969 16.52% 0.572% 92 8.663 8.656 8.672 VV 1933551 18034974 3.53% 0.122% 93 8.696 8.672 8.700 VV 1994132 33091697 6.47% 0.224% 94 8.811 8.700 8.838 VV 2181223 171571731 33.54% 1.161% 95 8.859 8.838 8.866 VV 2102349 34182448 6.68% 0.231% 96 8.874 8.866 8.880 VV 2096839 18033328 3.53% 0.122% 97 8.989 8.880 8.999 VV 2120588 147930656 28.92% 1.001% 98 9.031 8.999 9.037 VV 2122786 48268538 9.44% 0.327% 99 9.078 9.037 9.082 VV 2137463 57883237 11.32% 0.392% 100 9.089 9.082 9.097 VV 2114198 18550593 3.63% 0.126% 101 9.174 9.097 9.186 VV 2121136 112090617 21.91% 0.758% 102 9.300 9.186 9.311 VV 2105816 157338381 30.76% 1.065% 103 9.366 9.311 9.375 VV 2070625 79720863 15.59% 0.539% 104 9.384 9.375 9.389 VV 2052123 16846094 3.29% 0.114% 105 9.413 9.389 9.444 VV 2042668 66621910 13.02% 0.451% 106 9.449 9.444 9.452 VV 1959056 9571479 1.87% 0.065% 107 9.507 9.452 9.515 VV 2001765 73865959 14.44% 0.500% 108 9.546 9.515 9.552 VV 1985557 44000127 8.60% 0.298% 109 9.573 9.552 9.591 VV 1991533 46280738 9.05% 0.313% 110 9.629 9.591 9.640 VV 1963368 57315712 11.21% 0.388% 111 9.673 9.640 9.681 VV 1957031 47308213 9.25% 0.320% 112 9.693 9.681 9.750 VV 1934803 72297973 14.13% 0.489% 113 9.824 9.750 9.831 VV 1703733 72852275 14.24% 0.493% 114 9.843 9.831 9.859 VV 1722804 28453785 5.56% 0.193% 115 9.875 9.859 9.907 VV 1708256 47996137 9.38% 0.325% 116 10.046 9.907 10.063 VV 1668820 154360155 30.18% 1.044% 117 10.286 10.063 10.326 VV 1521056 243655832 47.64% 1.649% 118 10.383 10.326 10.422 VV 1408340 79092178 15.46% 0.535% 119 10.554 10.422 10.594 VV 1274895 131436842 25.70% 0.889% 120 10.614 10.594 10.662 VV 1201979 44431298 8.69% 0.301% 121 10.771 10.662 10.823 VV 1036359 83184640 16.26% 0.563% 122 10.982 10.823 11.024 PV 670339 70493078 13.78% 0.477% 123 11.099 11.024 11.112 VV 468045 23583469 4.61% 0.160% 124 11.226 11.112 11.236 VV 269782 24401898 4.77% 0.165% 125 11.246 11.236 11.342 VB 251249 8653280 1.69% 0.059% 126 11.648 11.579 11.667 VV 73701 2975349 0.58% 0.020% 127 11.817 11.667 11.842 VV 46951 4606856 0.90% 0.031% Sum of corrected areas: 14780279983