Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_O\Data\PO030218\ Data File : PO042715.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 11:40 Operator : SM/UA Sample : J1637-01MS Misc : ALS Vial : 13 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Mar 01 12:30:59 2018 Quant Method : P:\HPCHEM1\ECD_O\methods\PO022118.M Quant Title : GC EXTRACTABLES QLast Update : Mon Feb 26 14:24:10 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Small noise peaks clipped Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30Mx0.32mmx 0.50µ Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 4.095 3.345 3206474 3548607 12.944 9.603 # 2) SA Decachlor... 9.469 8.123 3717117 5306023 14.708m 13.760 Target Compounds 3) L1 AR-1016-1 4.960 4.163 859058 1035292 127.916 109.371 4) L1 AR-1016-2 5.300 4.599 1367096 643252 152.663 78.502 # 5) L1 AR-1016-3 5.394 4.638 955558 617391 132.254m 59.425 # 6) L1 AR-1016-4 5.818 4.802 993769 1310103 139.877 117.973 7) L1 AR-1016-5 6.048 5.138 2431426 1186682 337.753 112.265 # 31) L7 AR-1260-1 6.778 5.793 2689472 4076150 195.491 168.839 32) L7 AR-1260-2 7.029 5.980 4562368 6376025 249.423 189.808 33) L7 AR-1260-3 7.305 6.125 4207694 4923578 202.502 172.959 34) L7 AR-1260-4 7.384 6.296 2547401 6608813 172.109 193.312 35) L7 AR-1260-5 7.904 6.826 5620304 9698811 166.262 143.314 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.