Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042715.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 11:40 Sample : J1637-01MS Misc : ALS Vial : 13 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.055 3.034 3.107 VV 324412 7692366 4.08% 0.209% 2 3.143 3.128 3.152 VV 230028 2714710 1.44% 0.074% 3 3.165 3.152 3.196 VV 280092 5368336 2.85% 0.146% 4 3.222 3.196 3.270 VV 609116 13298441 7.05% 0.362% 5 3.307 3.295 3.318 PV 200846 1619470 0.86% 0.044% 6 3.339 3.318 3.363 VV 342885 6751399 3.58% 0.184% 7 3.384 3.363 3.425 VV 693834 14621589 7.75% 0.398% 8 3.497 3.479 3.514 VV 397017 7086428 3.76% 0.193% 9 3.553 3.541 3.568 VV 376029 5414387 2.87% 0.147% 10 3.583 3.568 3.600 VV 538940 8892003 4.72% 0.242% 11 3.611 3.600 3.633 VV 491962 8940871 4.74% 0.243% 12 3.685 3.666 3.700 VV 541391 9503900 5.04% 0.258% 13 3.713 3.700 3.763 VV 651230 16152543 8.57% 0.439% 14 4.095 4.064 4.122 VV 9875343 108710653 57.65% 2.956% 15 4.290 4.258 4.333 PV 336383 6542046 3.47% 0.178% 16 4.379 4.356 4.405 VV 399753 5311169 2.82% 0.144% 17 4.451 4.429 4.507 VV 1953479 22249675 11.80% 0.605% 18 4.534 4.507 4.550 PV 394298 4160915 2.21% 0.113% 19 4.596 4.574 4.631 VV 350354 4527890 2.40% 0.123% 20 4.775 4.731 4.791 VV 2815146 31540064 16.72% 0.858% 21 4.803 4.791 4.830 VV 1546749 17480317 9.27% 0.475% 22 4.858 4.830 4.878 VV 426217 7287005 3.86% 0.198% 23 4.913 4.878 4.924 VV 366204 6569288 3.48% 0.179% 24 4.932 4.924 4.939 VV 305050 2688307 1.43% 0.073% 25 4.960 4.939 4.989 VV 2833027 33882847 17.97% 0.921% 26 5.074 5.056 5.089 PV 237983 2959611 1.57% 0.080% 27 5.123 5.089 5.138 VV 976027 14199400 7.53% 0.386% 28 5.161 5.138 5.188 VV 1403810 22696241 12.04% 0.617% 29 5.219 5.188 5.228 VV 4137454 46109418 24.45% 1.254% 30 5.240 5.228 5.276 VV 5110096 67287501 35.68% 1.830% 31 5.300 5.276 5.339 VV 3343955 46194386 24.50% 1.256% 32 5.395 5.339 5.420 VV 2956914 42281850 22.42% 1.150% 33 5.434 5.420 5.444 VV 354005 4555369 2.42% 0.124% 34 5.459 5.444 5.466 VV 504905 5754461 3.05% 0.156% 35 5.485 5.466 5.508 VV 2571486 32549598 17.26% 0.885% 36 5.528 5.508 5.547 VV 2144651 31014821 16.45% 0.843% 37 5.564 5.547 5.596 VV 2612145 37154654 19.70% 1.010% 38 5.642 5.623 5.658 VV 699623 10859996 5.76% 0.295% 39 5.681 5.658 5.706 VV 3053244 42491563 22.53% 1.155% 40 5.721 5.706 5.742 VV 1357951 18719996 9.93% 0.509% 41 5.764 5.742 5.786 VV 1221164 17796900 9.44% 0.484% 42 5.818 5.786 5.858 VV 2264282 43016942 22.81% 1.170% 43 5.882 5.858 5.904 VV 963929 15204347 8.06% 0.413% 44 5.924 5.904 5.935 VV 432742 7413838 3.93% 0.202% 45 5.948 5.935 5.970 VV 449156 8525716 4.52% 0.232% 46 6.048 6.001 6.068 VV 5428248 81259361 43.09% 2.210% 47 6.072 6.068 6.093 VV 1802485 19882064 10.54% 0.541% 48 6.110 6.093 6.148 VV 1359874 29918572 15.87% 0.814% 49 6.199 6.174 6.226 VV 1083120 24149565 12.81% 0.657% 50 6.260 6.226 6.285 VV 4962040 74900962 39.72% 2.037% 51 6.314 6.285 6.361 VV 3137331 68163812 36.15% 1.854% 52 6.391 6.361 6.418 VV 3974086 65048234 34.49% 1.769% 53 6.462 6.418 6.486 VV 1266535 41433985 21.97% 1.127% 54 6.524 6.486 6.547 VV 3721943 73488742 38.97% 1.998% 55 6.562 6.547 6.593 VV 2416851 48062017 25.49% 1.307% 56 6.619 6.593 6.649 VV 5307360 100612922 53.35% 2.736% 57 6.675 6.649 6.712 VV 4838170 107316455 56.91% 2.918% 58 6.727 6.712 6.753 VV 2390585 47319369 25.09% 1.287% 59 6.778 6.753 6.817 VV 8670661 142299185 75.46% 3.870% 60 6.839 6.817 6.867 VV 1628044 35876426 19.02% 0.976% 61 6.896 6.867 6.922 PV 3213924 58410307 30.97% 1.588% 62 6.962 6.922 6.990 VV 2799794 74825598 39.68% 2.035% 63 7.029 6.990 7.052 VV 12232663 188581696 100.00% 5.128% 64 7.070 7.052 7.091 VV 4263981 62843219 33.32% 1.709% 65 7.110 7.091 7.132 VV 3054281 48556715 25.75% 1.320% 66 7.156 7.132 7.177 VV 5284138 77998342 41.36% 2.121% 67 7.186 7.177 7.205 VV 1618987 22292060 11.82% 0.606% 68 7.221 7.205 7.235 VV 994221 16399717 8.70% 0.446% 69 7.261 7.235 7.277 VV 1509326 27693928 14.69% 0.753% 70 7.305 7.277 7.328 VV 10438615 151654432 80.42% 4.124% 71 7.335 7.328 7.359 VV 2056649 28115534 14.91% 0.765% 72 7.384 7.359 7.413 VV 6850970 90327123 47.90% 2.456% 73 7.439 7.413 7.471 VV 3667268 45129991 23.93% 1.227% 74 7.570 7.543 7.577 VV 1361032 14615899 7.75% 0.397% 75 7.603 7.577 7.654 VV 6467520 94416455 50.07% 2.568% 76 7.680 7.654 7.714 VV 3462989 45967708 24.38% 1.250% 77 7.733 7.714 7.747 VV 1826667 22764633 12.07% 0.619% 78 7.783 7.747 7.814 VV 2662582 77054883 40.86% 2.095% 79 7.832 7.814 7.874 VV 2562721 43541312 23.09% 1.184% 80 7.904 7.874 7.934 VV 14888056 187419807 99.38% 5.097% 81 7.952 7.934 7.981 VV 861101 10658495 5.65% 0.290% 82 8.071 7.981 8.103 VV 278558 5996709 3.18% 0.163% 83 8.191 8.103 8.216 VV 6713630 117592138 62.36% 3.198% 84 8.240 8.216 8.251 VV 2584942 38456277 20.39% 1.046% 85 8.258 8.251 8.303 VV 2458394 29223602 15.50% 0.795% 86 8.461 8.433 8.498 VV 315727 5286448 2.80% 0.144% 87 8.534 8.498 8.552 VV 239424 4448571 2.36% 0.121% 88 8.594 8.552 8.644 VV 1552954 25616247 13.58% 0.697% 89 8.829 8.774 8.861 PV 3221515 46457813 24.64% 1.263% 90 8.869 8.861 8.874 VV 124191 933544 0.50% 0.025% 91 8.908 8.874 8.925 VV 294956 6392545 3.39% 0.174% 92 8.951 8.925 8.993 VV 266384 8501649 4.51% 0.231% 93 9.183 9.107 9.232 VV 948319 20316134 10.77% 0.552% 94 9.260 9.232 9.298 VV 387765 7758878 4.11% 0.211% 95 9.399 9.366 9.426 VV 57098 1254728 0.67% 0.034% 96 9.469 9.426 9.526 VV 7230179 120493395 63.89% 3.277% 97 9.591 9.526 9.626 PV 166424 5333289 2.83% 0.145% 98 9.645 9.626 9.679 VB 81943 1765567 0.94% 0.048% 99 9.845 9.798 9.906 PV 282686 6741500 3.57% 0.183% Sum of corrected areas: 3677361787 Signal #2 : ECD2B.CH 1 2.542 2.506 2.568 BV 250145 3306766 0.89% 0.057% 2 2.591 2.568 2.638 VV 225196 6136637 1.65% 0.107% 3 2.667 2.638 2.739 PV 755672 16151024 4.35% 0.280% 4 3.345 3.286 3.448 BV 9616912 119323976 32.17% 2.072% 5 3.503 3.485 3.527 VV 172723 2452095 0.66% 0.043% 6 3.546 3.527 3.571 VV 344804 4031385 1.09% 0.070% 7 3.630 3.611 3.666 VV 502544 6044243 1.63% 0.105% 8 3.701 3.666 3.727 PV 1875445 23062616 6.22% 0.400% 9 3.743 3.727 3.798 VV 521513 10574674 2.85% 0.184% 10 3.855 3.798 3.884 VV 389364 9667378 2.61% 0.168% 11 3.983 3.958 4.038 VV 2745168 55252640 14.90% 0.959% 12 4.057 4.038 4.077 VV 486320 8177450 2.20% 0.142% 13 4.090 4.077 4.108 VV 302627 3645939 0.98% 0.063% 14 4.127 4.108 4.138 PV 363172 4146784 1.12% 0.072% 15 4.163 4.138 4.221 VV 2455250 41751778 11.26% 0.725% 16 4.255 4.221 4.264 VV 1066904 14917204 4.02% 0.259% 17 4.274 4.264 4.290 VV 1105191 13471447 3.63% 0.234% 18 4.298 4.290 4.345 VV 670103 10433367 2.81% 0.181% 19 4.388 4.345 4.425 VV 5564198 117622377 31.71% 2.042% 20 4.443 4.425 4.526 VV 2917481 56795792 15.31% 0.986% 21 4.557 4.526 4.581 VV 3040032 42228040 11.39% 0.733% 22 4.599 4.581 4.618 VV 2598947 33648235 9.07% 0.584% 23 4.638 4.618 4.656 VV 2774793 39730778 10.71% 0.690% 24 4.664 4.656 4.698 VV 1316519 18569605 5.01% 0.322% 25 4.747 4.719 4.767 VV 737019 10574015 2.85% 0.184% 26 4.802 4.767 4.824 PV 3033137 43997733 11.86% 0.764% 27 4.838 4.824 4.856 VV 1466631 19734759 5.32% 0.343% 28 4.871 4.856 4.885 VV 1204492 16061995 4.33% 0.279% 29 4.896 4.885 4.906 VV 952855 10982689 2.96% 0.191% 30 4.941 4.906 4.974 VV 2350012 49511025 13.35% 0.860% 31 5.012 4.974 5.048 VV 1163460 29550260 7.97% 0.513% 32 5.067 5.048 5.083 VV 580455 11177903 3.01% 0.194% 33 5.106 5.083 5.118 VV 1475550 22400245 6.04% 0.389% 34 5.138 5.118 5.149 VV 4061916 52315351 14.11% 0.908% 35 5.161 5.149 5.197 VV 4116689 72301492 19.49% 1.255% 36 5.229 5.197 5.257 VV 1284052 38138177 10.28% 0.662% 37 5.282 5.257 5.313 VV 3975403 79420091 21.41% 1.379% 38 5.332 5.313 5.371 VV 4039139 99243765 26.76% 1.723% 39 5.389 5.371 5.429 VV 3843330 75684326 20.41% 1.314% 40 5.527 5.487 5.559 PV 4188705 83360786 22.48% 1.448% 41 5.583 5.559 5.610 VV 2506864 57509743 15.51% 0.999% 42 5.646 5.610 5.653 VV 3213369 58228769 15.70% 1.011% 43 5.682 5.653 5.705 VV 7686173 161230570 43.47% 2.800% 44 5.722 5.705 5.762 VV 3650828 90432059 24.38% 1.570% 45 5.793 5.762 5.832 VV 11191146 189608773 51.12% 3.292% 46 5.852 5.832 5.869 VV 2019792 42936850 11.58% 0.746% 47 5.893 5.869 5.905 VV 3203059 53826258 14.51% 0.935% 48 5.922 5.905 5.951 VV 4307227 84456222 22.77% 1.467% 49 5.980 5.951 6.029 VV 16541910 278574777 75.11% 4.837% 50 6.052 6.029 6.082 VV 5232573 93895403 25.32% 1.630% 51 6.125 6.082 6.171 VV 13461269 246329940 66.41% 4.277% 52 6.197 6.171 6.220 VV 3442287 71784786 19.35% 1.247% 53 6.244 6.220 6.269 VV 5372435 99454541 26.81% 1.727% 54 6.296 6.269 6.315 VV 16667539 256558037 69.17% 4.455% 55 6.331 6.315 6.363 VV 12631279 203165796 54.78% 3.528% 56 6.385 6.363 6.459 VV 7009872 162899723 43.92% 2.829% 57 6.520 6.493 6.555 VV 3278818 81331307 21.93% 1.412% 58 6.583 6.555 6.607 VV 10659429 162385932 43.78% 2.820% 59 6.620 6.607 6.644 VV 2924381 49033478 13.22% 0.851% 60 6.676 6.644 6.705 VV 6263495 113391578 30.57% 1.969% 61 6.725 6.705 6.740 VV 3557348 54965063 14.82% 0.954% 62 6.753 6.740 6.784 VV 3080040 56516082 15.24% 0.981% 63 6.826 6.784 6.866 VV 24302734 370896068 100.00% 6.440% 64 6.879 6.866 6.903 VV 1385209 26173092 7.06% 0.454% 65 6.924 6.903 6.967 VV 1558402 41852066 11.28% 0.727% 66 7.016 6.996 7.041 VV 1075763 19765938 5.33% 0.343% 67 7.097 7.041 7.125 VV 5939784 105399767 28.42% 1.830% 68 7.161 7.125 7.228 VV 15993094 284672142 76.75% 4.943% 69 7.253 7.228 7.285 VV 503288 13986348 3.77% 0.243% 70 7.355 7.285 7.386 VV 560284 14638887 3.95% 0.254% 71 7.417 7.386 7.434 PV 410016 4962090 1.34% 0.086% 72 7.445 7.434 7.463 VB 177108 1825122 0.49% 0.032% 73 7.517 7.483 7.588 BV 2287917 30896751 8.33% 0.537% 74 7.650 7.588 7.681 PV 5296323 70969116 19.13% 1.232% 75 7.696 7.681 7.723 VV 328948 4839075 1.30% 0.084% 76 7.743 7.723 7.748 VV 51521 529647 0.14% 0.009% 77 7.761 7.748 7.767 VV 50497 445419 0.12% 0.008% 78 7.823 7.767 7.832 VV 35249 719909 0.19% 0.013% 79 7.912 7.832 7.946 PV 1537836 20704208 5.58% 0.360% 80 8.123 7.946 8.186 PV 12590635 188841743 50.92% 3.279% 81 8.208 8.186 8.224 VV 122728 2452669 0.66% 0.043% 82 8.245 8.224 8.272 VV 108818 2045980 0.55% 0.036% 83 8.350 8.272 8.357 VV 109282 4378070 1.18% 0.076% 84 8.373 8.357 8.377 VV 109167 1033884 0.28% 0.018% 85 8.490 8.377 8.504 VV 139406 7619599 2.05% 0.132% 86 8.588 8.504 8.593 VV 118314 3920297 1.06% 0.068% 87 8.616 8.593 8.621 VV 134926 1980196 0.53% 0.034% 88 8.641 8.621 8.648 VV 151374 2036604 0.55% 0.035% 89 8.663 8.648 8.675 VV 123852 1686070 0.45% 0.029% 90 8.678 8.675 8.684 VV 58985 263294 0.07% 0.005% 91 8.796 8.684 8.825 VV 260021 13285980 3.58% 0.231% 92 8.848 8.825 8.886 VB 190511 4791189 1.29% 0.083% 93 8.959 8.894 8.968 BV 171368 4770256 1.29% 0.083% 94 9.010 8.968 9.015 VV 202447 4924437 1.33% 0.086% 95 9.064 9.015 9.072 VV 242318 6947122 1.87% 0.121% 96 9.083 9.072 9.109 VV 266523 5124016 1.38% 0.089% 97 9.225 9.109 9.241 VV 362879 22740010 6.13% 0.395% 98 9.245 9.241 9.248 VV 329360 1419433 0.38% 0.025% 99 9.290 9.248 9.304 VV 342047 10856523 2.93% 0.189% 100 9.341 9.304 9.345 VV 344033 8281693 2.23% 0.144% 101 9.406 9.345 9.439 VV 368683 18585211 5.01% 0.323% 102 9.483 9.439 9.501 VV 370375 12190683 3.29% 0.212% 103 9.506 9.501 9.510 VV 368432 1747205 0.47% 0.030% 104 9.636 9.510 9.641 VV 376555 28305180 7.63% 0.492% 105 9.706 9.641 9.746 VV 730249 27311466 7.36% 0.474% 106 9.867 9.746 9.898 PV 229013 15557652 4.19% 0.270% 107 10.012 9.898 10.019 VV 176677 11247358 3.03% 0.195% 108 10.033 10.019 10.078 VB 138434 3189235 0.86% 0.055% 109 10.123 10.084 10.129 BV 129525 1530987 0.41% 0.027% 110 10.148 10.129 10.159 VV 181635 2648624 0.71% 0.046% 111 10.176 10.159 10.182 VV 186721 2219975 0.60% 0.039% 112 10.289 10.182 10.296 VV 274707 14578860 3.93% 0.253% 113 10.298 10.296 10.323 VV 263484 3868772 1.04% 0.067% 114 10.370 10.323 10.376 VV 297215 8220576 2.22% 0.143% 115 10.382 10.376 10.410 VV 298604 5296729 1.43% 0.092% 116 10.457 10.410 10.478 VV 347826 11435626 3.08% 0.199% 117 10.510 10.478 10.548 VV 374088 14564875 3.93% 0.253% 118 10.621 10.548 10.663 VV 419023 26036402 7.02% 0.452% 119 10.743 10.663 10.816 VV 493609 35295367 9.52% 0.613% 120 10.981 10.816 11.018 PV 402885 40857522 11.02% 0.709% 121 11.093 11.018 11.138 VV 359913 23141217 6.24% 0.402% 122 11.200 11.138 11.233 VV 383041 19955341 5.38% 0.347% 123 11.424 11.233 11.437 VV 332802 36831887 9.93% 0.640% 124 11.450 11.437 11.462 VV 295721 4079170 1.10% 0.071% 125 11.473 11.462 11.491 VV 277004 4153287 1.12% 0.072% 126 11.620 11.491 11.628 VV 166732 15677757 4.23% 0.272% 127 11.639 11.628 11.664 VV 158482 3114641 0.84% 0.054% 128 11.808 11.664 11.844 VB 114725 10473090 2.82% 0.182% Sum of corrected areas: 5758901931