Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_O\Data\PO030218\ Data File : PO042716.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 11:56 Operator : SM/UA Sample : J1637-01MSD Misc : ALS Vial : 14 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Mar 01 12:33:19 2018 Quant Method : P:\HPCHEM1\ECD_O\methods\PO022118.M Quant Title : GC EXTRACTABLES QLast Update : Mon Feb 26 14:24:10 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Small noise peaks clipped Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30Mx0.32mmx 0.50µ Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 4.096 3.346 3264634 3586232 13.179 9.705 # 2) SA Decachlor... 9.471 8.126 3846989 5478272 15.222m 14.206 Target Compounds 3) L1 AR-1016-1 4.962 4.164 860042 1051139 128.062 111.045 4) L1 AR-1016-2 5.302 4.600 1354668 650851 151.275 79.430 # 5) L1 AR-1016-3 5.397 4.639 901649 626168 124.793 60.270 # 6) L1 AR-1016-4 5.819 4.803 1016110 1132059 143.022 101.940 # 7) L1 AR-1016-5 6.050 5.139 1002304 1425270 139.232 134.836 31) L7 AR-1260-1 6.780 5.795 2686675 4122626 195.288 170.764 32) L7 AR-1260-2 7.030 5.981 4440215 6097653 242.745 181.521 # 33) L7 AR-1260-3 7.307 6.126 4426074 5249583 213.012 184.411 34) L7 AR-1260-4 7.384 6.297 2622069 6638220 177.153 194.172 35) L7 AR-1260-5 7.906 6.827 5597257 9610380 165.580 142.007 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.