Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042716.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 11:56 Sample : J1637-01MSD Misc : ALS Vial : 14 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.050 3.036 3.066 VV 201548 2592143 1.32% 0.081% 2 3.144 3.110 3.153 PV 231222 3387358 1.72% 0.105% 3 3.166 3.153 3.201 VV 291544 5772095 2.93% 0.180% 4 3.223 3.201 3.274 VV 638929 13701762 6.96% 0.426% 5 3.308 3.296 3.320 PV 199392 1765881 0.90% 0.055% 6 3.340 3.320 3.364 VV 353577 6741070 3.42% 0.210% 7 3.385 3.364 3.413 VV 686904 12525397 6.36% 0.390% 8 3.498 3.479 3.514 VV 377382 6369919 3.24% 0.198% 9 3.557 3.542 3.568 VV 406437 5657910 2.87% 0.176% 10 3.584 3.568 3.600 VV 539917 8757934 4.45% 0.272% 11 3.614 3.600 3.668 VV 510622 17289022 8.78% 0.538% 12 3.687 3.668 3.701 VV 521193 8827717 4.48% 0.275% 13 3.714 3.701 3.744 VV 644206 12332721 6.26% 0.384% 14 3.788 3.769 3.811 VV 406789 8620384 4.38% 0.268% 15 4.096 4.047 4.158 VV 10003187 112654759 57.22% 3.504% 16 4.291 4.261 4.335 PV 348141 6025580 3.06% 0.187% 17 4.381 4.358 4.404 VV 398346 5249614 2.67% 0.163% 18 4.453 4.433 4.503 VV 1937789 22579430 11.47% 0.702% 19 4.536 4.503 4.551 PV 401317 4316297 2.19% 0.134% 20 4.559 4.551 4.576 VV 154201 1410353 0.72% 0.044% 21 4.598 4.576 4.633 PV 366216 4413973 2.24% 0.137% 22 4.776 4.751 4.792 VV 2805121 29609561 15.04% 0.921% 23 4.805 4.792 4.831 VV 1466524 16453950 8.36% 0.512% 24 4.860 4.831 4.878 VV 406639 6156387 3.13% 0.192% 25 4.913 4.878 4.926 VV 336742 5987792 3.04% 0.186% 26 4.934 4.926 4.942 VV 293069 2650977 1.35% 0.082% 27 4.962 4.942 4.993 VV 2883230 33270567 16.90% 1.035% 28 5.077 5.059 5.093 PV 218976 2836853 1.44% 0.088% 29 5.125 5.093 5.139 VV 961529 13439534 6.83% 0.418% 30 5.161 5.139 5.193 VV 990264 17629231 8.95% 0.548% 31 5.221 5.193 5.230 VV 4062833 45264831 22.99% 1.408% 32 5.243 5.230 5.278 VV 5190510 66682781 33.87% 2.074% 33 5.302 5.278 5.341 VV 3306681 44688895 22.70% 1.390% 34 5.397 5.341 5.423 PV 2931230 40434356 20.54% 1.258% 35 5.433 5.423 5.442 VV 267035 2800567 1.42% 0.087% 36 5.461 5.442 5.467 VV 407558 4922901 2.50% 0.153% 37 5.487 5.467 5.509 VV 2470419 30524625 15.50% 0.950% 38 5.530 5.509 5.555 VV 2002801 31502810 16.00% 0.980% 39 5.566 5.555 5.599 VV 1131869 14473838 7.35% 0.450% 40 5.644 5.626 5.660 VV 527652 7248934 3.68% 0.225% 41 5.683 5.660 5.707 VV 2833335 37621306 19.11% 1.170% 42 5.722 5.707 5.745 VV 1203954 15156100 7.70% 0.471% 43 5.767 5.745 5.788 VV 1060579 13047826 6.63% 0.406% 44 5.819 5.788 5.862 VV 2164663 33884128 17.21% 1.054% 45 5.883 5.862 5.907 PV 722826 8513099 4.32% 0.265% 46 5.924 5.907 5.933 VV 146412 1789602 0.91% 0.056% 47 5.951 5.933 5.973 VV 148093 2382156 1.21% 0.074% 48 5.996 5.973 6.007 VV 76751 1199860 0.61% 0.037% 49 6.050 6.007 6.066 VV 2925939 37284625 18.94% 1.160% 50 6.075 6.066 6.094 VV 1256503 14926697 7.58% 0.464% 51 6.112 6.094 6.167 VV 871493 15138692 7.69% 0.471% 52 6.201 6.167 6.231 VV 592985 8173018 4.15% 0.254% 53 6.262 6.231 6.287 VV 4463681 55804733 28.34% 1.736% 54 6.315 6.287 6.349 VV 2566419 41815145 21.24% 1.301% 55 6.354 6.349 6.365 VV 389578 3585503 1.82% 0.112% 56 6.393 6.365 6.420 VV 3439109 46548131 23.64% 1.448% 57 6.464 6.420 6.490 VV 598635 16044308 8.15% 0.499% 58 6.494 6.490 6.499 VV 328362 1852800 0.94% 0.058% 59 6.526 6.499 6.549 VV 3003461 45608632 23.16% 1.419% 60 6.563 6.549 6.593 VV 1656084 26522914 13.47% 0.825% 61 6.621 6.593 6.651 VV 3683954 61261580 31.11% 1.906% 62 6.677 6.651 6.714 VV 3971725 73445572 37.30% 2.285% 63 6.729 6.714 6.754 VV 1468941 24892076 12.64% 0.774% 64 6.780 6.754 6.819 VV 7593696 105259229 53.46% 3.274% 65 6.844 6.819 6.868 VV 595070 15379516 7.81% 0.478% 66 6.897 6.868 6.924 VV 2256948 37274107 18.93% 1.159% 67 6.964 6.924 6.994 VV 2024685 42079015 21.37% 1.309% 68 7.030 6.994 7.054 VV 11255801 162585083 82.58% 5.057% 69 7.072 7.054 7.093 VV 3639322 50033384 25.41% 1.556% 70 7.111 7.093 7.134 VV 2641406 37722068 19.16% 1.173% 71 7.158 7.134 7.178 VV 5150194 68653422 34.87% 2.136% 72 7.187 7.178 7.207 VV 1375574 18259745 9.27% 0.568% 73 7.223 7.207 7.233 VV 831066 11993539 6.09% 0.373% 74 7.262 7.233 7.278 VV 1516435 30061099 15.27% 0.935% 75 7.307 7.278 7.330 VV 11016100 160060324 81.29% 4.979% 76 7.337 7.330 7.360 VV 2146512 29222911 14.84% 0.909% 77 7.384 7.360 7.413 VV 7502260 100987670 51.29% 3.141% 78 7.440 7.413 7.469 VV 4102999 59148079 30.04% 1.840% 79 7.571 7.544 7.579 VV 1704131 23309105 11.84% 0.725% 80 7.605 7.579 7.655 VV 6621256 111653652 56.71% 3.473% 81 7.683 7.655 7.715 VV 3842939 58012463 29.46% 1.805% 82 7.734 7.715 7.763 VV 2053752 31116249 15.80% 0.968% 83 7.791 7.763 7.809 VV 660826 13802223 7.01% 0.429% 84 7.835 7.809 7.864 VV 2379964 36533521 18.56% 1.136% 85 7.906 7.864 7.935 VV 15292013 196889562 100.00% 6.124% 86 7.952 7.935 7.991 VV 1044049 18220517 9.25% 0.567% 87 8.073 7.991 8.122 VV 422845 18819776 9.56% 0.585% 88 8.191 8.122 8.218 VV 6935098 122175820 62.05% 3.800% 89 8.243 8.218 8.321 VV 2832864 70819070 35.97% 2.203% 90 8.462 8.442 8.490 VV 308103 4714422 2.39% 0.147% 91 8.539 8.490 8.553 VV 223462 4582817 2.33% 0.143% 92 8.564 8.553 8.569 VV 204339 1903560 0.97% 0.059% 93 8.597 8.569 8.648 VV 1470860 23381167 11.88% 0.727% 94 8.830 8.785 8.864 PV 3055029 46997349 23.87% 1.462% 95 8.909 8.864 8.926 VV 322318 7764950 3.94% 0.242% 96 8.948 8.926 8.996 VV 264484 8447406 4.29% 0.263% 97 9.095 9.012 9.110 VV 136936 6639798 3.37% 0.207% 98 9.185 9.110 9.228 VV 1013262 23105181 11.74% 0.719% 99 9.262 9.228 9.296 VV 487784 10363455 5.26% 0.322% 100 9.403 9.296 9.433 VV 154718 10122571 5.14% 0.315% 101 9.472 9.433 9.519 VV 7323227 130492559 66.28% 4.059% 102 9.581 9.519 9.624 VV 247906 10491980 5.33% 0.326% 103 9.737 9.624 9.755 VV 110817 7511604 3.82% 0.234% 104 10.041 9.755 10.081 VV 66166 12029746 6.11% 0.374% 105 10.140 10.081 10.188 VV 65619 2103324 1.07% 0.065% Sum of corrected areas: 3214792249 Signal #2 : ECD2B.CH 1 2.546 2.514 2.572 BV 243778 3413855 0.95% 0.064% 2 2.588 2.572 2.637 VV 275914 8166897 2.27% 0.153% 3 2.668 2.637 2.696 PV 808086 14753112 4.10% 0.276% 4 2.701 2.696 2.731 VV 245431 2940357 0.82% 0.055% 5 3.041 3.030 3.103 VV 256898 4669802 1.30% 0.087% 6 3.346 3.319 3.449 VV 9695525 119954840 33.30% 2.242% 7 3.547 3.524 3.568 VV 345648 3766398 1.05% 0.070% 8 3.631 3.613 3.668 VV 500538 6059321 1.68% 0.113% 9 3.701 3.668 3.728 PV 1855452 22945918 6.37% 0.429% 10 3.743 3.728 3.793 VV 499906 9739062 2.70% 0.182% 11 3.855 3.834 3.883 VV 376996 6369881 1.77% 0.119% 12 3.984 3.959 4.037 VV 2804788 55419490 15.39% 1.036% 13 4.058 4.037 4.079 VV 497042 8658258 2.40% 0.162% 14 4.128 4.109 4.139 PV 366259 4325081 1.20% 0.081% 15 4.164 4.139 4.204 VV 2463698 39412917 10.94% 0.737% 16 4.209 4.204 4.223 VV 239109 2246801 0.62% 0.042% 17 4.275 4.223 4.290 VV 1027124 22595949 6.27% 0.422% 18 4.300 4.290 4.344 VV 639694 9625366 2.67% 0.180% 19 4.389 4.344 4.427 PV 5493402 114916089 31.91% 2.148% 20 4.445 4.427 4.530 VV 2834341 50592724 14.05% 0.946% 21 4.558 4.530 4.583 VV 2875760 37745034 10.48% 0.705% 22 4.600 4.583 4.619 VV 2431684 29578565 8.21% 0.553% 23 4.639 4.619 4.657 VV 2596266 35191590 9.77% 0.658% 24 4.666 4.657 4.697 VV 1109146 13119513 3.64% 0.245% 25 4.750 4.726 4.774 PV 540084 6765763 1.88% 0.126% 26 4.803 4.774 4.826 VV 2741147 36249292 10.06% 0.677% 27 4.839 4.826 4.857 VV 1144439 13359310 3.71% 0.250% 28 4.872 4.857 4.901 VV 852889 11097430 3.08% 0.207% 29 4.943 4.901 4.975 VV 1971727 32066695 8.90% 0.599% 30 5.013 4.975 5.049 VV 714226 9536930 2.65% 0.178% 31 5.071 5.049 5.083 PV 84074 1030589 0.29% 0.019% 32 5.107 5.083 5.119 VV 957538 11450045 3.18% 0.214% 33 5.139 5.119 5.164 VV 3476950 47736611 13.25% 0.892% 34 5.178 5.164 5.196 VV 745884 9435863 2.62% 0.176% 35 5.230 5.196 5.258 VV 589436 12664257 3.52% 0.237% 36 5.283 5.258 5.314 VV 3277821 56695147 15.74% 1.060% 37 5.333 5.314 5.373 VV 3330073 74196105 20.60% 1.387% 38 5.390 5.373 5.426 VV 3011995 46645649 12.95% 0.872% 39 5.444 5.426 5.468 VV 475823 9957042 2.76% 0.186% 40 5.528 5.468 5.558 VV 3408400 62397972 17.32% 1.166% 41 5.583 5.558 5.606 VV 1735120 31405593 8.72% 0.587% 42 5.647 5.606 5.654 VV 2433240 40427354 11.22% 0.756% 43 5.683 5.654 5.706 VV 7077755 139224587 38.65% 2.602% 44 5.723 5.706 5.764 VV 2902544 65642118 18.22% 1.227% 45 5.795 5.764 5.833 VV 10489546 161149367 44.74% 3.012% 46 5.854 5.833 5.871 VV 1350644 27786030 7.71% 0.519% 47 5.894 5.871 5.906 VV 2519324 39154720 10.87% 0.732% 48 5.923 5.906 5.954 VV 3686013 68128790 18.92% 1.273% 49 5.981 5.954 6.030 VV 14655030 234180087 65.02% 4.377% 50 6.054 6.030 6.096 VV 4824213 93366969 25.92% 1.745% 51 6.126 6.096 6.172 VV 13031567 212147029 58.90% 3.965% 52 6.198 6.172 6.222 VV 3005346 59007326 16.38% 1.103% 53 6.245 6.222 6.270 VV 5057501 85189098 23.65% 1.592% 54 6.297 6.270 6.316 VV 15866457 243137254 67.50% 4.544% 55 6.333 6.316 6.364 VV 12023610 190484306 52.89% 3.560% 56 6.386 6.364 6.459 VV 6760962 141247567 39.22% 2.640% 57 6.521 6.488 6.558 VV 2979561 73841553 20.50% 1.380% 58 6.584 6.558 6.609 VV 10392598 152509434 42.34% 2.850% 59 6.622 6.609 6.646 VV 2654186 43625463 12.11% 0.815% 60 6.678 6.646 6.705 VV 5991882 103412599 28.71% 1.933% 61 6.725 6.705 6.741 VV 3458531 51879507 14.40% 0.970% 62 6.755 6.741 6.785 VV 2854284 50929244 14.14% 0.952% 63 6.827 6.785 6.866 VV 24321636 360176725 100.00% 6.732% 64 6.880 6.866 6.905 VV 1262723 24159499 6.71% 0.452% 65 6.926 6.905 6.963 VV 1455369 34854007 9.68% 0.651% 66 7.017 6.963 7.044 VV 978904 34436869 9.56% 0.644% 67 7.098 7.044 7.128 VV 5683386 89339809 24.80% 1.670% 68 7.162 7.128 7.228 VV 14956126 237999311 66.08% 4.448% 69 7.255 7.228 7.289 VV 497779 14470056 4.02% 0.270% 70 7.318 7.289 7.323 VV 301410 5954347 1.65% 0.111% 71 7.328 7.323 7.333 VV 293244 1661676 0.46% 0.031% 72 7.357 7.333 7.393 VV 673019 13548861 3.76% 0.253% 73 7.418 7.393 7.435 VV 503695 8309582 2.31% 0.155% 74 7.447 7.435 7.484 VV 313409 6806260 1.89% 0.127% 75 7.518 7.484 7.574 VV 2314909 35153073 9.76% 0.657% 76 7.579 7.574 7.590 VV 84022 686981 0.19% 0.013% 77 7.651 7.590 7.684 VV 5246633 72971496 20.26% 1.364% 78 7.696 7.684 7.747 VV 354031 6588449 1.83% 0.123% 79 7.767 7.747 7.773 VV 57159 857741 0.24% 0.016% 80 7.824 7.773 7.841 VV 43968 1275721 0.35% 0.024% 81 7.914 7.841 7.951 PV 1584348 21696131 6.02% 0.405% 82 8.031 7.951 8.037 VV 30956 400112 0.11% 0.007% 83 8.126 8.037 8.191 PV 12469339 179034027 49.71% 3.346% 84 8.197 8.191 8.216 VB 86931 660125 0.18% 0.012% 85 8.432 8.231 8.439 BV 260151 18709034 5.19% 0.350% 86 8.448 8.439 8.461 VV 244876 3045228 0.85% 0.057% 87 8.496 8.461 8.511 VV 299039 7881723 2.19% 0.147% 88 8.535 8.511 8.543 VV 299088 5130600 1.42% 0.096% 89 8.663 8.543 8.694 VV 434100 33964716 9.43% 0.635% 90 8.733 8.694 8.756 VV 481887 16589642 4.61% 0.310% 91 8.848 8.756 8.898 VV 584199 44359543 12.32% 0.829% 92 9.005 8.898 9.018 VV 613848 39000763 10.83% 0.729% 93 9.084 9.018 9.103 VV 655632 30599882 8.50% 0.572% 94 9.105 9.103 9.109 VV 606300 2217092 0.62% 0.041% 95 9.189 9.109 9.196 VV 688506 33369703 9.26% 0.624% 96 9.254 9.196 9.259 VV 715649 26668837 7.40% 0.498% 97 9.276 9.259 9.286 VV 701813 10794354 3.00% 0.202% 98 9.310 9.286 9.319 VV 683675 13498444 3.75% 0.252% 99 9.326 9.319 9.333 VV 692233 5398490 1.50% 0.101% 100 9.363 9.333 9.374 VV 685563 16364831 4.54% 0.306% 101 9.421 9.374 9.436 VV 703223 25053547 6.96% 0.468% 102 9.486 9.436 9.501 VV 724869 27314570 7.58% 0.511% 103 9.510 9.501 9.517 VV 711261 6520847 1.81% 0.122% 104 9.553 9.517 9.559 VV 693054 17384040 4.83% 0.325% 105 9.568 9.559 9.574 VV 683685 5752058 1.60% 0.108% 106 9.580 9.574 9.596 VV 700748 9089747 2.52% 0.170% 107 9.708 9.596 9.745 VV 1070083 68725966 19.08% 1.284% 108 9.773 9.745 9.784 VV 689366 16092242 4.47% 0.301% 109 9.790 9.784 9.798 VV 675164 5416357 1.50% 0.101% 110 9.832 9.798 9.839 VV 654456 16133249 4.48% 0.302% 111 9.848 9.839 9.855 VV 666386 6355068 1.76% 0.119% 112 9.876 9.855 9.884 VV 660075 11203198 3.11% 0.209% 113 9.958 9.884 9.962 VV 679924 30496614 8.47% 0.570% 114 9.967 9.962 9.979 VV 683559 6820977 1.89% 0.127% 115 9.990 9.979 9.994 VV 672261 5823766 1.62% 0.109% 116 10.048 9.994 10.053 VV 641150 22627305 6.28% 0.423% 117 10.066 10.053 10.071 VV 612255 6712441 1.86% 0.125% 118 10.163 10.093 10.168 VV 625580 25841192 7.17% 0.483% 119 10.186 10.168 10.205 VV 593992 13178379 3.66% 0.246% 120 10.219 10.205 10.239 VV 600139 11746017 3.26% 0.220% 121 10.245 10.239 10.249 VV 580634 3343982 0.93% 0.062% 122 10.288 10.249 10.298 VV 570576 16379414 4.55% 0.306% 123 10.324 10.298 10.338 VV 560198 12735327 3.54% 0.238% 124 10.378 10.338 10.384 VV 488572 13365427 3.71% 0.250% 125 10.397 10.384 10.420 VV 501170 9882891 2.74% 0.185% 126 10.454 10.420 10.482 VV 457937 15800736 4.39% 0.295% 127 10.505 10.482 10.509 VV 430337 6575289 1.83% 0.123% 128 10.518 10.509 10.553 VV 454212 10509690 2.92% 0.196% 129 10.590 10.565 10.595 VV 369702 6249482 1.74% 0.117% 130 10.646 10.595 10.651 VV 327445 10722095 2.98% 0.200% 131 10.656 10.651 10.676 VV 328838 4361972 1.21% 0.082% 132 10.710 10.676 10.756 VV 327160 13452514 3.73% 0.251% 133 10.827 10.756 10.903 VV 331938 19709098 5.47% 0.368% 134 10.943 10.903 10.991 VB 109266 4207317 1.17% 0.079% 135 11.206 10.998 11.221 BV 143226 7674853 2.13% 0.143% 136 11.281 11.221 11.306 VV 93456 3987135 1.11% 0.075% 137 11.424 11.306 11.438 VV 100351 5480596 1.52% 0.102% 138 11.471 11.438 11.498 VV 101880 2798387 0.78% 0.052% 139 11.692 11.498 11.723 VV 73220 7414486 2.06% 0.139% 140 11.734 11.723 11.754 VV 35245 445751 0.12% 0.008% 141 11.804 11.754 11.856 PV 102760 3111792 0.86% 0.058% Sum of corrected areas: 5350497074