Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042718.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 12:26 Sample : AR1660CCC500 Misc : ALS Vial : 3 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.158 3.138 3.201 BV 220953 2520056 0.51% 0.039% 2 3.219 3.201 3.255 PV 738014 6876332 1.40% 0.106% 3 3.588 3.467 3.612 PV 251724 7306146 1.49% 0.113% 4 3.631 3.612 3.663 VV 192298 5044676 1.03% 0.078% 5 3.678 3.663 3.703 VV 126036 2694270 0.55% 0.042% 6 3.723 3.703 3.745 VV 107310 2150714 0.44% 0.033% 7 3.797 3.766 3.815 VV 62682 1294130 0.26% 0.020% 8 4.094 4.015 4.223 BV 36341928 413349941 84.07% 6.386% 9 4.291 4.261 4.348 VV 869911 13781950 2.80% 0.213% 10 4.379 4.348 4.425 PV 1474466 20290794 4.13% 0.313% 11 4.451 4.425 4.568 VV 6010924 76918099 15.65% 1.188% 12 4.595 4.568 4.638 VV 968720 11221836 2.28% 0.173% 13 4.775 4.733 4.790 PV 8716322 99055791 20.15% 1.530% 14 4.803 4.790 4.840 VV 5187192 62249271 12.66% 0.962% 15 4.859 4.840 4.876 VV 1124690 13029053 2.65% 0.201% 16 4.889 4.876 4.899 VV 463204 4862242 0.99% 0.075% 17 4.912 4.899 4.934 VV 632799 7818940 1.59% 0.121% 18 4.960 4.934 5.025 VV 8656687 104000654 21.15% 1.607% 19 5.069 5.043 5.099 BV 316150 4290533 0.87% 0.066% 20 5.124 5.099 5.138 PV 2671134 30139236 6.13% 0.466% 21 5.151 5.138 5.190 VV 1870747 27121538 5.52% 0.419% 22 5.219 5.190 5.228 VV 12889108 136440616 27.75% 2.108% 23 5.240 5.228 5.277 VV 17053172 228075543 46.39% 3.524% 24 5.300 5.277 5.366 VV 10441448 146140354 29.72% 2.258% 25 5.395 5.366 5.439 VV 8970114 117153355 23.83% 1.810% 26 5.458 5.439 5.464 VV 989735 9721621 1.98% 0.150% 27 5.484 5.464 5.508 VV 6921630 87169455 17.73% 1.347% 28 5.528 5.508 5.554 VV 6084992 98690492 20.07% 1.525% 29 5.563 5.554 5.637 VV 3230185 40545476 8.25% 0.626% 30 5.680 5.653 5.704 BV 8400402 108615679 22.09% 1.678% 31 5.720 5.704 5.743 VV 3806887 50546659 10.28% 0.781% 32 5.764 5.743 5.786 VV 3013439 38684277 7.87% 0.598% 33 5.817 5.786 5.858 VV 7554782 119794066 24.37% 1.851% 34 5.881 5.858 5.913 VV 2539949 33125111 6.74% 0.512% 35 5.935 5.913 5.970 VV 400532 6117170 1.24% 0.095% 36 5.995 5.970 6.019 VV 449092 6270936 1.28% 0.097% 37 6.047 6.019 6.063 VV 8081881 99214896 20.18% 1.533% 38 6.072 6.063 6.093 VV 3547230 41579552 8.46% 0.642% 39 6.110 6.093 6.173 VV 2635823 38001384 7.73% 0.587% 40 6.197 6.173 6.231 VV 981652 12241810 2.49% 0.189% 41 6.260 6.231 6.289 VV 7343216 91086013 18.53% 1.407% 42 6.299 6.289 6.368 VV 387637 6806144 1.38% 0.105% 43 6.461 6.438 6.492 BV 269231 3404384 0.69% 0.053% 44 6.533 6.492 6.544 VV 1361698 15119145 3.08% 0.234% 45 6.562 6.544 6.591 VV 3206238 40526232 8.24% 0.626% 46 6.617 6.591 6.648 VV 3757112 47116688 9.58% 0.728% 47 6.675 6.648 6.712 VV 9316375 148811333 30.27% 2.299% 48 6.725 6.712 6.750 VV 2566518 31332907 6.37% 0.484% 49 6.778 6.750 6.830 VV 17389550 215799613 43.89% 3.334% 50 6.896 6.869 6.925 PV 2589423 32203541 6.55% 0.498% 51 6.961 6.925 6.999 VV 3629962 44597692 9.07% 0.689% 52 7.029 6.999 7.052 VV 23467498 278829964 56.71% 4.308% 53 7.070 7.052 7.091 VV 6558608 81082844 16.49% 1.253% 54 7.110 7.091 7.132 VV 5537741 66949036 13.62% 1.034% 55 7.155 7.132 7.175 VV 10211673 122644791 24.95% 1.895% 56 7.186 7.175 7.224 VV 2188616 26391029 5.37% 0.408% 57 7.260 7.224 7.276 VV 2202808 33006263 6.71% 0.510% 58 7.305 7.276 7.328 VV 22925829 315889379 64.25% 4.881% 59 7.335 7.328 7.359 VV 3350864 43549453 8.86% 0.673% 60 7.382 7.359 7.413 VV 18136337 225808623 45.93% 3.489% 61 7.439 7.413 7.500 VV 9597152 117099942 23.82% 1.809% 62 7.568 7.520 7.580 PV 3553115 41958900 8.53% 0.648% 63 7.604 7.580 7.652 VV 15837090 226077263 45.98% 3.493% 64 7.680 7.652 7.715 VV 8141608 115307176 23.45% 1.782% 65 7.732 7.715 7.763 VV 4315007 52751711 10.73% 0.815% 66 7.789 7.763 7.808 VV 810756 10423940 2.12% 0.161% 67 7.833 7.808 7.868 VV 4611494 62200061 12.65% 0.961% 68 7.904 7.868 7.934 VV 39165444 491644312 100.00% 7.596% 69 7.950 7.934 7.995 VV 2318035 31655399 6.44% 0.489% 70 8.189 8.111 8.216 PV 16779710 297294826 60.47% 4.593% 71 8.244 8.216 8.253 VV 7409376 107016254 21.77% 1.653% 72 8.259 8.253 8.313 VV 7309299 83031848 16.89% 1.283% 73 8.461 8.416 8.494 BV 502077 6951531 1.41% 0.107% 74 8.538 8.507 8.570 PV 445234 9434054 1.92% 0.146% 75 8.593 8.570 8.636 VV 3950237 53510194 10.88% 0.827% 76 8.828 8.766 8.881 BV 8647219 127738635 25.98% 1.974% 77 8.906 8.881 8.948 VB 455376 6826666 1.39% 0.105% 78 9.183 9.126 9.225 BV 2060926 32106713 6.53% 0.496% 79 9.468 9.417 9.568 PV 21982021 394269986 80.19% 6.092% Sum of corrected areas: 6472399138 Signal #2 : ECD2B.CH 1 2.540 2.506 2.595 BV 196059 1982920 0.21% 0.017% 2 3.344 3.308 3.493 BV 46310993 577908633 60.19% 4.941% 3 3.546 3.523 3.605 VV 1460677 20557584 2.14% 0.176% 4 3.628 3.605 3.672 VV 2239822 28435923 2.96% 0.243% 5 3.699 3.672 3.768 VV 7904923 103053811 10.73% 0.881% 6 3.785 3.768 3.830 VV 201980 4155585 0.43% 0.036% 7 3.855 3.830 3.908 VV 1160285 15265223 1.59% 0.131% 8 3.982 3.950 4.037 VV 11969166 225007054 23.44% 1.924% 9 4.056 4.037 4.076 VV 1565727 20467173 2.13% 0.175% 10 4.089 4.076 4.107 VV 699753 9046843 0.94% 0.077% 11 4.125 4.107 4.137 VV 929971 10935864 1.14% 0.094% 12 4.162 4.137 4.198 VV 10608239 156192552 16.27% 1.336% 13 4.208 4.198 4.234 VV 566393 8324863 0.87% 0.071% 14 4.274 4.234 4.288 VV 3928183 54417487 5.67% 0.465% 15 4.298 4.288 4.343 VV 2635973 36282642 3.78% 0.310% 16 4.387 4.343 4.424 VV 26188814 533716734 55.59% 4.564% 17 4.443 4.424 4.525 VV 13562644 233421905 24.31% 1.996% 18 4.556 4.525 4.579 VV 13014554 170300388 17.74% 1.456% 19 4.598 4.579 4.617 VV 10631202 135647119 14.13% 1.160% 20 4.637 4.617 4.655 VV 11748316 163240629 17.00% 1.396% 21 4.664 4.655 4.762 VV 5102156 78264993 8.15% 0.669% 22 4.801 4.762 4.824 VV 12756717 175779763 18.31% 1.503% 23 4.837 4.824 4.854 VV 5786553 72937153 7.60% 0.624% 24 4.869 4.854 4.898 VV 4887640 66271153 6.90% 0.567% 25 4.941 4.898 4.978 VV 10650810 195758761 20.39% 1.674% 26 5.009 4.978 5.044 VV 3829447 64663281 6.74% 0.553% 27 5.070 5.044 5.084 VV 848731 15144856 1.58% 0.129% 28 5.105 5.084 5.118 VV 3541285 43035583 4.48% 0.368% 29 5.137 5.118 5.162 VV 13874502 185806162 19.35% 1.589% 30 5.176 5.162 5.212 VV 3690072 62141505 6.47% 0.531% 31 5.226 5.212 5.254 VV 1739277 26784888 2.79% 0.229% 32 5.281 5.254 5.318 VV 10374334 139472686 14.53% 1.193% 33 5.365 5.318 5.433 VV 1242852 44297267 4.61% 0.379% 34 5.500 5.478 5.557 VV 566363 14174249 1.48% 0.121% 35 5.582 5.557 5.613 VV 2215513 32266126 3.36% 0.276% 36 5.645 5.613 5.655 VV 4972410 60036634 6.25% 0.513% 37 5.681 5.655 5.703 VV 16735871 264671738 27.57% 2.263% 38 5.719 5.703 5.763 VV 6087708 123054823 12.82% 1.052% 39 5.793 5.763 5.838 VV 28169009 383530201 39.95% 3.279% 40 5.853 5.838 5.872 VV 926561 15075247 1.57% 0.129% 41 5.893 5.872 5.902 VV 2318772 28211554 2.94% 0.241% 42 5.921 5.902 5.952 VV 6931533 102550244 10.68% 0.877% 43 5.980 5.952 6.088 VV 38787162 535383654 55.76% 4.578% 44 6.124 6.088 6.173 VV 32854117 447189451 46.58% 3.824% 45 6.197 6.173 6.220 VV 4073287 59368676 6.18% 0.508% 46 6.243 6.220 6.268 VV 9620062 133251478 13.88% 1.139% 47 6.296 6.268 6.314 VV 35085031 503968693 52.49% 4.309% 48 6.331 6.314 6.363 VV 33149742 475929406 49.57% 4.069% 49 6.384 6.363 6.455 VV 16645995 246456946 25.67% 2.107% 50 6.519 6.491 6.554 VV 6157437 100328652 10.45% 0.858% 51 6.583 6.554 6.609 VV 26419895 365706985 38.09% 3.127% 52 6.619 6.609 6.642 VV 3535959 47944708 4.99% 0.410% 53 6.676 6.642 6.704 VV 14257372 218098505 22.72% 1.865% 54 6.724 6.704 6.740 VV 7463574 100216112 10.44% 0.857% 55 6.753 6.740 6.785 VV 6084085 97410173 10.15% 0.833% 56 6.825 6.785 6.866 VV 68642025 960106036 100.00% 8.210% 57 6.878 6.866 6.902 VV 2272871 36464721 3.80% 0.312% 58 6.923 6.902 6.988 VV 3135331 65194330 6.79% 0.557% 59 7.096 7.038 7.131 PV 15851018 234812880 24.46% 2.008% 60 7.161 7.131 7.287 VV 42700785 657560091 68.49% 5.623% 61 7.312 7.287 7.317 VV 333584 5917741 0.62% 0.051% 62 7.319 7.317 7.327 VV 308459 1863149 0.19% 0.016% 63 7.354 7.327 7.392 VV 1103608 19759818 2.06% 0.169% 64 7.417 7.392 7.433 VV 982732 14644462 1.53% 0.125% 65 7.444 7.433 7.487 VV 777625 12572348 1.31% 0.108% 66 7.516 7.487 7.588 VV 6916565 95606347 9.96% 0.817% 67 7.598 7.588 7.608 VV 94931 940540 0.10% 0.008% 68 7.650 7.608 7.682 VV 16089920 210438153 21.92% 1.799% 69 7.694 7.682 7.753 VV 959572 16358428 1.70% 0.140% 70 7.912 7.808 7.971 PV 3698431 51524055 5.37% 0.441% 71 7.996 7.971 8.002 VV 72192 1172058 0.12% 0.010% 72 8.123 8.002 8.211 VV 45738869 626120797 65.21% 5.354% 73 8.270 8.211 8.274 VV 294314 10334908 1.08% 0.088% 74 8.508 8.274 8.513 VV 421495 50750550 5.29% 0.434% 75 8.618 8.513 8.625 VV 518348 30824739 3.21% 0.264% 76 8.674 8.625 8.679 VV 509490 16516181 1.72% 0.141% 77 8.693 8.679 8.698 VV 513376 5533926 0.58% 0.047% 78 8.801 8.698 8.806 VV 576668 33615883 3.50% 0.287% 79 8.955 8.806 8.959 VV 574149 50525827 5.26% 0.432% 80 8.973 8.959 8.978 VV 578256 6219447 0.65% 0.053% 81 8.991 8.978 8.996 VV 577786 6019460 0.63% 0.051% 82 9.011 8.996 9.017 VV 586594 7372669 0.77% 0.063% 83 9.117 9.017 9.126 VV 640389 39189836 4.08% 0.335% 84 9.146 9.126 9.153 VV 625835 9808579 1.02% 0.084% 85 9.247 9.153 9.254 VV 661708 38324335 3.99% 0.328% 86 9.260 9.254 9.265 VV 646538 4252235 0.44% 0.036% 87 9.298 9.265 9.328 VV 668201 23565659 2.45% 0.202% 88 9.372 9.328 9.376 VV 652090 18532287 1.93% 0.158% 89 9.387 9.376 9.393 VV 650896 6357815 0.66% 0.054% 90 9.402 9.393 9.420 VV 650552 9999091 1.04% 0.085% 91 9.490 9.420 9.494 VV 606628 26958763 2.81% 0.231% 92 9.558 9.494 9.562 VV 587482 24081645 2.51% 0.206% 93 9.598 9.562 9.607 VV 610715 15858985 1.65% 0.136% 94 9.628 9.607 9.633 VV 620769 9005433 0.94% 0.077% 95 9.652 9.633 9.656 VV 595677 8125949 0.85% 0.069% 96 9.684 9.656 9.694 VV 593619 13301272 1.39% 0.114% 97 9.723 9.694 9.738 VV 564123 14445466 1.50% 0.124% 98 9.782 9.738 9.786 VV 543151 15197769 1.58% 0.130% 99 9.854 9.786 9.867 VV 522736 25299962 2.64% 0.216% 100 9.887 9.867 9.902 VV 507869 10652816 1.11% 0.091% 101 9.913 9.902 9.924 VV 513525 6526276 0.68% 0.056% 102 9.934 9.924 9.949 VV 526591 7342862 0.76% 0.063% 103 9.956 9.949 9.967 VV 512453 5523377 0.58% 0.047% 104 9.980 9.967 9.985 VV 505381 5172226 0.54% 0.044% 105 10.026 9.985 10.055 VV 469178 19041970 1.98% 0.163% 106 10.066 10.055 10.078 VV 438547 5857086 0.61% 0.050% 107 10.122 10.078 10.136 VV 400698 13808610 1.44% 0.118% 108 10.149 10.136 10.154 VV 378085 4086965 0.43% 0.035% 109 10.183 10.154 10.187 VV 368239 7109856 0.74% 0.061% 110 10.192 10.187 10.198 VV 364129 2242358 0.23% 0.019% 111 10.217 10.198 10.224 VV 376902 5352241 0.56% 0.046% 112 10.249 10.224 10.273 VV 361521 9752692 1.02% 0.083% 113 10.304 10.273 10.325 VV 327366 9148695 0.95% 0.078% 114 10.350 10.325 10.360 VV 272769 5508662 0.57% 0.047% 115 10.368 10.360 10.381 VV 261714 2935344 0.31% 0.025% 116 10.430 10.381 10.434 VV 184599 6208030 0.65% 0.053% 117 10.450 10.434 10.456 VV 183767 2249778 0.23% 0.019% 118 10.585 10.555 10.595 VV 70026 1249983 0.13% 0.011% 119 10.611 10.595 10.616 VV 44961 401436 0.04% 0.003% 120 10.625 10.616 10.633 VV 49189 263636 0.03% 0.002% Sum of corrected areas: 11695052763