Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042720.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 12:56 Sample : J1399-09 Misc : ALS Vial : 5 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.060 3.036 3.085 VV 429252 10338309 5.98% 0.221% 2 3.093 3.085 3.129 VV 520089 8748897 5.06% 0.187% 3 3.146 3.129 3.155 PV 752273 7509392 4.35% 0.161% 4 3.168 3.155 3.189 VV 824217 12348039 7.15% 0.264% 5 3.220 3.189 3.245 VV 1937305 27729294 16.05% 0.594% 6 3.264 3.245 3.270 PV 653918 6146867 3.56% 0.132% 7 3.279 3.270 3.296 VV 750452 7954830 4.60% 0.170% 8 3.349 3.322 3.365 VV 1135345 21383198 12.37% 0.458% 9 3.379 3.365 3.399 VV 1084492 17868033 10.34% 0.383% 10 3.440 3.399 3.465 VV 1271769 37861305 21.91% 0.811% 11 3.497 3.465 3.515 VV 1241360 32125071 18.59% 0.688% 12 3.555 3.515 3.567 VV 1313337 36689267 21.23% 0.785% 13 3.586 3.567 3.621 VV 1505392 36317630 21.02% 0.777% 14 3.661 3.621 3.692 VV 1625035 55408756 32.06% 1.186% 15 3.716 3.692 3.754 VV 1728669 47165330 27.29% 1.010% 16 3.777 3.754 3.790 VV 1656850 26346235 15.25% 0.564% 17 3.809 3.790 3.825 VV 1782863 33804638 19.56% 0.724% 18 3.841 3.825 3.876 VV 1762213 49535186 28.66% 1.060% 19 3.884 3.876 3.896 VV 1636080 18929338 10.95% 0.405% 20 3.936 3.896 3.969 VV 1823006 72102431 41.72% 1.544% 21 3.987 3.969 4.000 VV 1756299 30644695 17.73% 0.656% 22 4.012 4.000 4.026 VV 1761090 26422704 15.29% 0.566% 23 4.054 4.026 4.065 VV 1862855 42223580 24.43% 0.904% 24 4.095 4.065 4.118 VV 13113172 172814668 100.00% 3.699% 25 4.130 4.118 4.153 VV 1911727 35516879 20.55% 0.760% 26 4.190 4.153 4.207 VV 1978642 57366060 33.20% 1.228% 27 4.216 4.207 4.237 VV 1910877 30323822 17.55% 0.649% 28 4.270 4.237 4.297 VV 2036910 66715676 38.61% 1.428% 29 4.339 4.297 4.371 VV 2048399 87151270 50.43% 1.866% 30 4.389 4.371 4.422 VV 2231662 64839066 37.52% 1.388% 31 4.464 4.422 4.479 VV 2265747 74309293 43.00% 1.591% 32 4.492 4.479 4.519 VV 2251425 53370739 30.88% 1.143% 33 4.537 4.519 4.550 VV 2466820 43963634 25.44% 0.941% 34 4.562 4.550 4.577 VV 2429676 38362467 22.20% 0.821% 35 4.590 4.577 4.621 VV 2417570 60588094 35.06% 1.297% 36 4.672 4.621 4.692 VV 2419063 98022110 56.72% 2.098% 37 4.714 4.692 4.734 VV 2481516 59328720 34.33% 1.270% 38 4.758 4.734 4.774 VV 2464637 57058853 33.02% 1.221% 39 4.787 4.774 4.794 VV 2485197 29673813 17.17% 0.635% 40 4.813 4.794 4.858 VV 2599391 94838317 54.88% 2.030% 41 4.897 4.858 4.904 VV 2623589 68628984 39.71% 1.469% 42 4.911 4.904 4.919 VV 2650264 23486617 13.59% 0.503% 43 4.934 4.919 4.968 VV 2861684 58371206 33.78% 1.250% 44 5.025 4.968 5.030 PV 2396769 49845811 28.84% 1.067% 45 5.033 5.030 5.049 VV 2384291 27289725 15.79% 0.584% 46 5.067 5.049 5.091 VV 2481462 61070400 35.34% 1.307% 47 5.098 5.091 5.104 VV 2422655 19275069 11.15% 0.413% 48 5.117 5.104 5.135 VV 2435628 44742672 25.89% 0.958% 49 5.163 5.135 5.195 VV 4039769 102373264 59.24% 2.192% 50 5.220 5.195 5.228 VV 2437342 46854884 27.11% 1.003% 51 5.237 5.228 5.274 VV 2417611 60157794 34.81% 1.288% 52 5.290 5.274 5.306 VV 2040018 35973027 20.82% 0.770% 53 5.327 5.306 5.340 VV 2059458 39686508 22.96% 0.850% 54 5.366 5.340 5.386 VV 2567930 58307556 33.74% 1.248% 55 5.404 5.386 5.421 VV 1888455 37218301 21.54% 0.797% 56 5.433 5.421 5.461 VV 1782181 39345973 22.77% 0.842% 57 5.487 5.461 5.506 VV 2181345 48567887 28.10% 1.040% 58 5.523 5.506 5.547 VV 2090928 31458199 18.20% 0.673% 59 5.581 5.547 5.591 VV 1064301 16547339 9.58% 0.354% 60 5.612 5.591 5.628 VV 2238921 35191593 20.36% 0.753% 61 5.639 5.628 5.654 VV 1987671 23876117 13.82% 0.511% 62 5.678 5.654 5.697 VV 2268724 42927890 24.84% 0.919% 63 5.723 5.697 5.739 VV 1986443 37837005 21.89% 0.810% 64 5.758 5.739 5.775 VV 1966268 38107866 22.05% 0.816% 65 5.789 5.775 5.811 VV 1878483 26984177 15.61% 0.578% 66 5.842 5.811 5.862 PV 2159164 47946507 27.74% 1.026% 67 5.883 5.862 5.913 VV 2251469 61515719 35.60% 1.317% 68 5.928 5.913 5.932 VV 1806136 20207796 11.69% 0.433% 69 5.946 5.932 5.965 VV 1862230 34661284 20.06% 0.742% 70 5.983 5.965 6.003 VV 1876127 41244170 23.87% 0.883% 71 6.052 6.003 6.064 VV 2372053 75034869 43.42% 1.606% 72 6.074 6.064 6.089 VV 2244584 32509610 18.81% 0.696% 73 6.094 6.089 6.110 VV 2030202 24782612 14.34% 0.531% 74 6.116 6.110 6.132 VV 1920252 25487149 14.75% 0.546% 75 6.140 6.132 6.160 VV 1840438 28460396 16.47% 0.609% 76 6.199 6.160 6.220 VV 1824554 61929963 35.84% 1.326% 77 6.263 6.220 6.290 VV 2480043 77098983 44.61% 1.650% 78 6.318 6.290 6.341 VV 4424217 79749618 46.15% 1.707% 79 6.351 6.341 6.367 VV 1800633 28275543 16.36% 0.605% 80 6.392 6.367 6.425 VV 5983901 106199080 61.45% 2.273% 81 6.445 6.425 6.501 VV 1542815 65557941 37.94% 1.403% 82 6.523 6.501 6.548 VV 8218628 107669665 62.30% 2.305% 83 6.560 6.548 6.586 VV 1345170 24970649 14.45% 0.535% 84 6.625 6.586 6.646 VV 1879381 46229047 26.75% 0.990% 85 6.669 6.646 6.699 VV 1321244 38312237 22.17% 0.820% 86 6.731 6.699 6.746 VV 1267544 34117409 19.74% 0.730% 87 6.776 6.746 6.800 VV 1191050 36631692 21.20% 0.784% 88 6.824 6.800 6.832 VV 1052397 20175928 11.67% 0.432% 89 6.863 6.832 6.880 VV 1187446 31334005 18.13% 0.671% 90 6.893 6.880 6.915 VV 1112962 22066475 12.77% 0.472% 91 6.954 6.915 6.994 VV 1521678 54500358 31.54% 1.167% 92 7.023 6.994 7.050 VV 2214666 46781138 27.07% 1.001% 93 7.066 7.050 7.089 VV 954610 20165332 11.67% 0.432% 94 7.154 7.089 7.177 VV 861208 41624997 24.09% 0.891% 95 7.183 7.177 7.194 VV 746286 7462159 4.32% 0.160% 96 7.224 7.194 7.242 VV 857134 22329391 12.92% 0.478% 97 7.261 7.242 7.269 VV 753533 12022113 6.96% 0.257% 98 7.329 7.269 7.360 VV 1224664 45423788 26.28% 0.972% 99 7.384 7.360 7.398 VV 737636 15430397 8.93% 0.330% 100 7.404 7.398 7.444 VV 661239 16613090 9.61% 0.356% 101 7.504 7.444 7.537 VV 619969 31521040 18.24% 0.675% 102 7.570 7.537 7.587 VV 603852 16961085 9.81% 0.363% 103 7.605 7.587 7.628 VV 672609 14273268 8.26% 0.306% 104 7.684 7.628 7.706 VV 594070 24148107 13.97% 0.517% 105 7.780 7.706 7.799 VV 562068 26587143 15.38% 0.569% 106 7.805 7.799 7.824 VV 449206 6342434 3.67% 0.136% 107 7.835 7.824 7.852 VV 432189 6949618 4.02% 0.149% 108 7.868 7.852 7.874 VV 393554 5178089 3.00% 0.111% 109 7.906 7.874 7.952 VV 580870 20270214 11.73% 0.434% 110 7.967 7.952 7.977 VV 361782 5097415 2.95% 0.109% 111 7.994 7.977 8.001 VV 342800 4740884 2.74% 0.101% 112 8.030 8.001 8.067 VV 320036 9892718 5.72% 0.212% 113 8.108 8.067 8.154 PV 268364 10543795 6.10% 0.226% 114 8.189 8.154 8.211 VV 221400 5411551 3.13% 0.116% 115 8.241 8.211 8.296 VB 156099 4337292 2.51% 0.093% 116 8.425 8.312 8.447 BV 207508 3915025 2.27% 0.084% 117 8.463 8.447 8.524 VV 121927 3072335 1.78% 0.066% 118 8.601 8.524 8.614 PV 83541 1764565 1.02% 0.038% 119 8.657 8.614 8.716 VB 100484 3565883 2.06% 0.076% 120 8.834 8.807 8.852 VV 113034 2440974 1.41% 0.052% 121 9.052 8.956 9.067 VV 105771 4713474 2.73% 0.101% 122 9.105 9.067 9.157 VV 97803 4153722 2.40% 0.089% 123 9.182 9.157 9.229 VV 104205 3277797 1.90% 0.070% 124 9.337 9.229 9.414 VV 115931 9753476 5.64% 0.209% 125 9.471 9.414 9.525 VV 4885204 85162481 49.28% 1.823% 126 9.576 9.525 9.655 VV 926271 20770030 12.02% 0.445% 127 9.833 9.655 9.982 VB 82867 9892729 5.72% 0.212% 128 10.726 10.675 10.845 VV 218946 8081124 4.68% 0.173% Sum of corrected areas: 4671311747 Signal #2 : ECD2B.CH 1 2.545 2.506 2.565 BV 666019 8292933 2.76% 0.205% 2 2.577 2.565 2.588 VV 510386 5013988 1.67% 0.124% 3 2.604 2.588 2.635 VV 876704 16449151 5.48% 0.406% 4 2.666 2.635 2.709 PV 1212638 30396416 10.12% 0.750% 5 2.755 2.709 2.777 VV 1221153 38664855 12.88% 0.954% 6 2.828 2.777 2.867 VV 1508838 64239068 21.40% 1.586% 7 2.896 2.867 2.917 VV 1641999 40023542 13.33% 0.988% 8 2.956 2.917 2.968 VV 1632006 44361653 14.78% 1.095% 9 2.981 2.968 3.005 VV 1668609 26923940 8.97% 0.665% 10 3.025 3.005 3.034 VV 1204984 15767611 5.25% 0.389% 11 3.064 3.034 3.104 VV 1749978 58279440 19.41% 1.439% 12 3.144 3.104 3.162 VV 1624039 43655200 14.54% 1.078% 13 3.177 3.162 3.192 VV 1593497 26476625 8.82% 0.654% 14 3.224 3.192 3.264 VV 1884716 74679628 24.87% 1.843% 15 3.274 3.264 3.286 VV 1762064 23015796 7.67% 0.568% 16 3.345 3.286 3.409 VV 15269612 300234530 100.00% 7.411% 17 3.415 3.409 3.431 VV 1770710 22206842 7.40% 0.548% 18 3.466 3.431 3.502 VV 2229440 83187278 27.71% 2.053% 19 3.530 3.502 3.536 VV 2230383 40418688 13.46% 0.998% 20 3.548 3.536 3.566 VV 2276746 40961627 13.64% 1.011% 21 3.602 3.566 3.615 VV 2483150 68084868 22.68% 1.681% 22 3.629 3.615 3.687 VV 2607493 107519541 35.81% 2.654% 23 3.703 3.687 3.715 VV 2521335 39777659 13.25% 0.982% 24 3.744 3.715 3.766 VV 2706681 79969196 26.64% 1.974% 25 3.956 3.874 3.974 PV 2314189 103092080 34.34% 2.545% 26 3.982 3.974 3.992 VV 2155811 23291998 7.76% 0.575% 27 4.017 3.992 4.033 VV 2379538 55119051 18.36% 1.361% 28 4.039 4.033 4.091 VV 2231221 69763679 23.24% 1.722% 29 4.104 4.091 4.121 VV 1782032 27913669 9.30% 0.689% 30 4.144 4.121 4.156 VV 1851751 33565525 11.18% 0.829% 31 4.171 4.156 4.188 VV 1940073 33113634 11.03% 0.817% 32 4.208 4.188 4.226 VV 1683519 32019986 10.66% 0.790% 33 4.260 4.226 4.277 VV 2104889 51563660 17.17% 1.273% 34 4.297 4.277 4.336 VV 2218099 56044704 18.67% 1.383% 35 4.370 4.336 4.376 VV 782430 9699822 3.23% 0.239% 36 4.394 4.376 4.424 VV 1740620 28492519 9.49% 0.703% 37 4.446 4.424 4.469 VV 1768161 33527083 11.17% 0.828% 38 4.499 4.469 4.523 VV 2113457 56475892 18.81% 1.394% 39 4.554 4.523 4.575 VV 2195291 45399883 15.12% 1.121% 40 4.607 4.575 4.625 PV 2099896 40189964 13.39% 0.992% 41 4.655 4.625 4.678 VV 2603309 62784276 20.91% 1.550% 42 4.714 4.678 4.722 VV 1947816 47092721 15.69% 1.162% 43 4.748 4.722 4.781 VV 3571638 90198261 30.04% 2.226% 44 4.813 4.781 4.835 VV 2611812 70730434 23.56% 1.746% 45 4.859 4.835 4.864 VV 2191405 36620562 12.20% 0.904% 46 4.886 4.864 4.921 VV 2274415 70643983 23.53% 1.744% 47 4.950 4.921 4.955 VV 2082149 38444423 12.80% 0.949% 48 4.957 4.955 4.963 VV 2064323 10866631 3.62% 0.268% 49 4.985 4.963 5.005 VV 2093077 50943476 16.97% 1.257% 50 5.017 5.005 5.034 VV 1928819 31910905 10.63% 0.788% 51 5.052 5.034 5.072 VV 1830062 39785780 13.25% 0.982% 52 5.105 5.072 5.122 VV 2090190 54173959 18.04% 1.337% 53 5.146 5.122 5.169 VV 2805353 58833408 19.60% 1.452% 54 5.186 5.169 5.200 VV 1749463 29924112 9.97% 0.739% 55 5.205 5.200 5.216 VV 1604248 15602421 5.20% 0.385% 56 5.237 5.216 5.255 VV 1689829 36754919 12.24% 0.907% 57 5.278 5.255 5.299 VV 1644568 38099179 12.69% 0.940% 58 5.332 5.299 5.372 VV 5258366 138532649 46.14% 3.420% 59 5.390 5.372 5.468 VV 4842217 112906056 37.61% 2.787% 60 5.528 5.468 5.563 VV 9160851 154529086 51.47% 3.814% 61 5.578 5.563 5.624 VV 1215800 38340557 12.77% 0.946% 62 5.645 5.624 5.668 VV 1001284 24322123 8.10% 0.600% 63 5.685 5.668 5.702 VV 1063874 18584079 6.19% 0.459% 64 5.719 5.702 5.763 VV 897574 24259209 8.08% 0.599% 65 5.797 5.763 5.819 VV 809288 19050629 6.35% 0.470% 66 5.834 5.819 5.852 VV 694161 13361217 4.45% 0.330% 67 5.887 5.852 5.911 VV 662765 21629018 7.20% 0.534% 68 5.933 5.911 5.954 VV 899367 18019372 6.00% 0.445% 69 5.978 5.954 5.997 VV 870785 18793284 6.26% 0.464% 70 6.009 5.997 6.031 VV 794639 10617344 3.54% 0.262% 71 6.054 6.031 6.073 VV 1004894 14652679 4.88% 0.362% 72 6.095 6.073 6.133 VV 1082838 25670728 8.55% 0.634% 73 6.155 6.133 6.221 VV 1042023 28885046 9.62% 0.713% 74 6.252 6.221 6.273 VV 429170 8102539 2.70% 0.200% 75 6.298 6.273 6.319 VV 697067 10745261 3.58% 0.265% 76 6.331 6.319 6.372 VV 327050 4740814 1.58% 0.117% 77 6.543 6.527 6.563 BV 122892 1352767 0.45% 0.033% 78 6.589 6.563 6.642 VV 139440 2640441 0.88% 0.065% 79 6.791 6.768 6.807 VV 104141 1783210 0.59% 0.044% 80 6.829 6.807 6.856 VV 238229 3764664 1.25% 0.093% 81 6.940 6.887 6.966 VV 175136 5914427 1.97% 0.146% 82 7.062 7.042 7.085 VV 264688 5139018 1.71% 0.127% 83 7.101 7.085 7.127 VV 220052 4919776 1.64% 0.121% 84 7.161 7.127 7.224 VV 270856 9104805 3.03% 0.225% 85 7.272 7.224 7.285 PV 149040 3914034 1.30% 0.097% 86 7.351 7.285 7.389 VV 144692 7512034 2.50% 0.185% 87 7.427 7.389 7.437 VV 57359 1567762 0.52% 0.039% 88 7.526 7.507 7.542 VV 54028 758658 0.25% 0.019% 89 7.652 7.595 7.679 VV 75576 2110989 0.70% 0.052% 90 7.715 7.679 7.752 VV 57416 1485147 0.49% 0.037% 91 7.819 7.752 7.844 VV 108891 2531626 0.84% 0.062% 92 7.865 7.844 7.894 VV 80149 1238807 0.41% 0.031% 93 7.917 7.894 7.932 PV 74393 918963 0.31% 0.023% 94 8.016 7.932 8.024 VV 63657 2000212 0.67% 0.049% 95 8.028 8.024 8.036 VV 46062 261113 0.09% 0.006% 96 8.126 8.036 8.172 VV 5635663 79407738 26.45% 1.960% 97 8.490 8.172 8.522 VV 1105086 62131429 20.69% 1.534% 98 8.574 8.522 8.682 VV 732191 57021137 18.99% 1.408% 99 8.709 8.682 8.714 VV 458655 8127327 2.71% 0.201% 100 8.777 8.714 8.787 VV 475647 19923130 6.64% 0.492% 101 8.820 8.787 8.838 VV 495766 14586848 4.86% 0.360% 102 8.854 8.838 8.871 VV 473818 8983972 2.99% 0.222% 103 8.894 8.871 8.910 VV 444921 10137326 3.38% 0.250% 104 9.029 8.910 9.035 VV 501112 34968825 11.65% 0.863% 105 9.237 9.035 9.247 VV 475458 58388269 19.45% 1.441% 106 9.311 9.247 9.344 VV 540052 26700435 8.89% 0.659% 107 9.443 9.344 9.539 VV 402320 40898201 13.62% 1.010% 108 9.713 9.539 9.726 VV 252039 28170243 9.38% 0.695% 109 9.745 9.726 9.762 VV 209734 4447840 1.48% 0.110% 110 9.771 9.762 9.799 VV 184748 3409270 1.14% 0.084% 111 9.949 9.799 9.964 VV 136997 10158789 3.38% 0.251% 112 9.985 9.964 10.031 VB 93211 2568379 0.86% 0.063% 113 10.202 10.063 10.284 PB 113210 6822935 2.27% 0.168% 114 10.511 10.417 10.616 BB 105228 5425904 1.81% 0.134% 115 10.819 10.619 10.892 BV 211277 14071713 4.69% 0.347% 116 11.179 11.094 11.234 VV 98065 5730926 1.91% 0.141% 117 11.409 11.328 11.465 PV 87092 3167424 1.05% 0.078% Sum of corrected areas: 4051190875