Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042721.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 13:11 Sample : J1399-11MS Misc : ALS Vial : 6 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.058 3.037 3.086 VV 368266 10177080 4.17% 0.213% 2 3.168 3.132 3.191 PV 839631 19092410 7.82% 0.400% 3 3.221 3.191 3.247 VV 1581489 24699952 10.11% 0.518% 4 3.281 3.247 3.312 PV 816552 17306103 7.09% 0.363% 5 3.351 3.324 3.367 VV 1055961 20141661 8.25% 0.422% 6 3.379 3.367 3.400 VV 1053457 17029538 6.97% 0.357% 7 3.441 3.400 3.466 VV 1133464 34031702 13.94% 0.713% 8 3.499 3.466 3.517 VV 1076271 28793324 11.79% 0.604% 9 3.555 3.517 3.569 VV 1044237 29783018 12.20% 0.624% 10 3.588 3.569 3.622 VV 1222809 28633528 11.73% 0.600% 11 3.664 3.622 3.694 VV 1234779 41380806 16.95% 0.867% 12 3.716 3.694 3.755 VV 1250039 33069163 13.54% 0.693% 13 3.778 3.755 3.792 VV 1135679 18276969 7.48% 0.383% 14 3.810 3.792 3.827 VV 1207547 22150272 9.07% 0.464% 15 3.844 3.827 3.875 VV 1211606 32573960 13.34% 0.683% 16 3.886 3.875 3.898 VV 1116191 14251792 5.84% 0.299% 17 3.931 3.898 3.969 VV 1186530 46510449 19.05% 0.975% 18 3.989 3.969 4.001 VV 1116883 20262475 8.30% 0.425% 19 4.013 4.001 4.029 VV 1116447 17854937 7.31% 0.374% 20 4.039 4.029 4.045 VV 1139201 11235265 4.60% 0.236% 21 4.096 4.045 4.153 VV 15821669 226311749 92.67% 4.744% 22 4.190 4.153 4.206 VV 1270158 36461958 14.93% 0.764% 23 4.216 4.206 4.237 VV 1273479 21671288 8.87% 0.454% 24 4.288 4.237 4.353 VV 1550623 90819603 37.19% 1.904% 25 4.381 4.353 4.406 VV 1914137 48488748 19.86% 1.016% 26 4.452 4.406 4.480 VV 4358749 92224674 37.77% 1.933% 27 4.491 4.480 4.509 VV 1482513 24109300 9.87% 0.505% 28 4.536 4.509 4.550 VV 1771003 38740980 15.86% 0.812% 29 4.561 4.550 4.575 VV 1633002 23082517 9.45% 0.484% 30 4.597 4.575 4.622 VV 1830760 43878397 17.97% 0.920% 31 4.676 4.622 4.693 VV 1426845 57687340 23.62% 1.209% 32 4.715 4.693 4.735 VV 1439500 34749520 14.23% 0.728% 33 4.776 4.735 4.792 VV 5464933 90578964 37.09% 1.899% 34 4.805 4.792 4.852 VV 3727208 77946462 31.92% 1.634% 35 4.865 4.852 4.875 VV 1592896 21354139 8.74% 0.448% 36 4.891 4.875 4.899 VV 1694869 23247094 9.52% 0.487% 37 4.913 4.899 4.924 VV 1863248 27006696 11.06% 0.566% 38 4.935 4.924 4.944 VV 2031794 22336393 9.15% 0.468% 39 4.955 4.944 4.975 VV 2743953 30255209 12.39% 0.634% 40 4.985 4.975 4.994 PV 372316 2751891 1.13% 0.058% 41 5.034 4.994 5.050 VV 1403339 36206661 14.83% 0.759% 42 5.076 5.050 5.101 VV 1521270 43916608 17.98% 0.921% 43 5.124 5.101 5.139 VV 2514489 42493757 17.40% 0.891% 44 5.161 5.139 5.195 VV 4518713 83957985 34.38% 1.760% 45 5.220 5.195 5.229 VV 7044362 84507566 34.61% 1.772% 46 5.241 5.229 5.277 VV 8233834 116601279 47.75% 2.444% 47 5.301 5.277 5.341 VV 4849542 86376091 35.37% 1.811% 48 5.370 5.341 5.380 VV 1936588 34462831 14.11% 0.722% 49 5.397 5.380 5.420 VV 4506492 61689727 25.26% 1.293% 50 5.432 5.420 5.463 VV 1199108 25206686 10.32% 0.528% 51 5.487 5.463 5.508 VV 4077926 57638898 23.60% 1.208% 52 5.527 5.508 5.552 VV 3154634 38089293 15.60% 0.798% 53 5.566 5.552 5.591 VV 771596 10788879 4.42% 0.226% 54 5.614 5.591 5.628 PV 1476878 18211137 7.46% 0.382% 55 5.640 5.628 5.654 VV 1447529 16219945 6.64% 0.340% 56 5.681 5.654 5.703 VV 4794893 66476302 27.22% 1.394% 57 5.723 5.703 5.746 VV 2284298 38813288 15.89% 0.814% 58 5.765 5.746 5.784 VV 1861236 31006948 12.70% 0.650% 59 5.793 5.784 5.806 VV 955313 11355711 4.65% 0.238% 60 5.825 5.806 5.863 VV 2219506 47609578 19.50% 0.998% 61 5.882 5.863 5.912 VV 2091846 39719663 16.26% 0.833% 62 5.926 5.912 5.966 VV 900298 26184298 10.72% 0.549% 63 5.991 5.966 6.004 VV 842347 17560638 7.19% 0.368% 64 6.050 6.004 6.068 VV 3891239 73441453 30.07% 1.540% 65 6.073 6.068 6.093 VV 1930665 22718167 9.30% 0.476% 66 6.114 6.093 6.161 VV 1280620 41144308 16.85% 0.863% 67 6.200 6.161 6.223 VV 1273511 31403449 12.86% 0.658% 68 6.262 6.223 6.289 VV 4371290 72866182 29.84% 1.528% 69 6.316 6.289 6.341 VV 4810712 74475784 30.50% 1.561% 70 6.353 6.341 6.366 VV 911916 13372681 5.48% 0.280% 71 6.392 6.366 6.430 VV 7126722 101172833 41.43% 2.121% 72 6.463 6.430 6.494 VV 790986 24817441 10.16% 0.520% 73 6.524 6.494 6.550 VV 20942912 244203885 100.00% 5.119% 74 6.563 6.550 6.587 VV 1550502 19941681 8.17% 0.418% 75 6.620 6.587 6.650 VV 2360404 40284347 16.50% 0.845% 76 6.677 6.650 6.713 VV 3379447 60861495 24.92% 1.276% 77 6.727 6.713 6.751 VV 1248324 19447298 7.96% 0.408% 78 6.780 6.751 6.811 VV 5972915 80528196 32.98% 1.688% 79 6.819 6.811 6.829 VV 440570 4642019 1.90% 0.097% 80 6.863 6.829 6.876 VV 570346 13500305 5.53% 0.283% 81 6.897 6.876 6.918 VV 1430778 21399247 8.76% 0.449% 82 6.962 6.918 6.994 VV 1809170 43655212 17.88% 0.915% 83 7.031 6.994 7.054 VV 7895003 113271278 46.38% 2.375% 84 7.072 7.054 7.093 VV 2561158 33804597 13.84% 0.709% 85 7.112 7.093 7.134 VV 1798495 24757071 10.14% 0.519% 86 7.157 7.134 7.177 VV 3402113 44897155 18.39% 0.941% 87 7.187 7.177 7.209 VV 825933 11410496 4.67% 0.239% 88 7.262 7.209 7.278 VV 899368 24202658 9.91% 0.507% 89 7.307 7.278 7.360 VV 7266817 134636374 55.13% 2.822% 90 7.384 7.360 7.415 VV 4837704 65410327 26.79% 1.371% 91 7.441 7.415 7.474 VV 2753361 38044717 15.58% 0.798% 92 7.512 7.474 7.548 VV 336854 11960391 4.90% 0.251% 93 7.571 7.548 7.581 VV 1113157 14441784 5.91% 0.303% 94 7.605 7.581 7.654 VV 4267634 68861827 28.20% 1.444% 95 7.682 7.654 7.713 VV 2527377 36485711 14.94% 0.765% 96 7.734 7.713 7.759 VV 1259589 19363202 7.93% 0.406% 97 7.785 7.759 7.809 VV 436346 10078315 4.13% 0.211% 98 7.836 7.809 7.863 VV 1601444 22704357 9.30% 0.476% 99 7.906 7.863 7.935 VV 10290113 130711801 53.53% 2.740% 100 7.953 7.935 7.993 VV 753535 14098942 5.77% 0.296% 101 8.018 7.993 8.068 VV 396952 10343758 4.24% 0.217% 102 8.137 8.068 8.148 PV 225509 8211095 3.36% 0.172% 103 8.192 8.148 8.219 VV 4727551 84124455 34.45% 1.764% 104 8.243 8.219 8.255 VV 2036133 31387261 12.85% 0.658% 105 8.261 8.255 8.316 VV 1758803 24201285 9.91% 0.507% 106 8.422 8.343 8.435 VV 201208 8715986 3.57% 0.183% 107 8.464 8.435 8.509 VV 356335 8766444 3.59% 0.184% 108 8.540 8.509 8.566 VV 236382 5179174 2.12% 0.109% 109 8.596 8.566 8.633 VV 962212 16089179 6.59% 0.337% 110 8.831 8.798 8.871 VV 2067528 30408463 12.45% 0.637% 111 8.908 8.884 8.949 BV 137587 2489257 1.02% 0.052% 112 9.187 9.141 9.223 VV 663248 11027232 4.52% 0.231% 113 9.272 9.223 9.309 VV 95738 2583128 1.06% 0.054% 114 9.472 9.416 9.531 PV 5930298 102154863 41.83% 2.142% 115 9.579 9.531 9.643 VV 1255892 25849118 10.59% 0.542% 116 9.743 9.701 9.776 BV 109133 2152030 0.88% 0.045% 117 10.040 9.996 10.071 PV 194099 4055208 1.66% 0.085% 118 10.090 10.071 10.138 VV 132612 2731247 1.12% 0.057% 119 10.731 10.673 10.812 BV 379944 10631987 4.35% 0.223% Sum of corrected areas: 4770169248 Signal #2 : ECD2B.CH 1 2.546 2.506 2.568 BV 556402 6061610 1.75% 0.088% 2 2.579 2.568 2.589 PV 293816 2563423 0.74% 0.037% 3 2.608 2.589 2.638 VV 779053 14948711 4.31% 0.217% 4 2.668 2.638 2.687 PV 1146253 21601260 6.23% 0.314% 5 2.692 2.687 2.711 VV 642535 6671978 1.92% 0.097% 6 2.758 2.711 2.781 VV 1237840 38934471 11.23% 0.566% 7 2.829 2.781 2.848 VV 1523165 49381681 14.24% 0.718% 8 2.857 2.848 2.870 VV 1157569 14393979 4.15% 0.209% 9 2.899 2.870 2.918 VV 1598521 39552058 11.40% 0.575% 10 2.956 2.918 2.970 VV 1564797 42945069 12.38% 0.624% 11 2.984 2.970 3.007 VV 1609101 26703050 7.70% 0.388% 12 3.026 3.007 3.035 VV 1201330 15029481 4.33% 0.218% 13 3.065 3.035 3.105 VV 1744783 59293378 17.10% 0.862% 14 3.145 3.105 3.165 VV 1711796 47888225 13.81% 0.696% 15 3.179 3.165 3.193 VV 1648924 26514839 7.64% 0.385% 16 3.224 3.193 3.263 VV 1937304 75088427 21.65% 1.091% 17 3.277 3.263 3.291 VV 1873055 30261105 8.72% 0.440% 18 3.347 3.291 3.380 VV 20451052 316545775 91.27% 4.600% 19 3.389 3.380 3.432 VV 2560011 65451189 18.87% 0.951% 20 3.469 3.432 3.506 VV 2341647 94157923 27.15% 1.368% 21 3.549 3.506 3.572 VV 2966651 95064958 27.41% 1.382% 22 3.581 3.572 3.586 VV 2371677 20197116 5.82% 0.294% 23 3.605 3.586 3.612 VV 2610040 38348621 11.06% 0.557% 24 3.631 3.612 3.671 VV 3429155 101006944 29.12% 1.468% 25 3.702 3.671 3.731 VV 5848219 131077057 37.79% 1.905% 26 3.746 3.731 3.776 VV 3137438 77581839 22.37% 1.127% 27 3.853 3.845 3.875 VV 2637652 28789650 8.30% 0.418% 28 3.922 3.875 3.931 PV 2209910 50466445 14.55% 0.733% 29 3.984 3.931 4.044 VV 6464251 238691437 68.82% 3.469% 30 4.058 4.044 4.096 VV 2609187 69529864 20.05% 1.010% 31 4.103 4.096 4.117 VV 1890050 22488795 6.48% 0.327% 32 4.165 4.117 4.193 VV 5010292 121916211 35.15% 1.772% 33 4.210 4.193 4.225 VV 1784551 30816843 8.89% 0.448% 34 4.240 4.225 4.251 VV 2434236 32236059 9.29% 0.468% 35 4.275 4.251 4.289 VV 2842662 58508891 16.87% 0.850% 36 4.299 4.289 4.338 VV 2815683 49473342 14.26% 0.719% 37 4.391 4.338 4.425 PV 7858297 152168734 43.87% 2.211% 38 4.445 4.425 4.480 VV 5141563 90642256 26.13% 1.317% 39 4.496 4.480 4.525 VV 1753651 42231352 12.18% 0.614% 40 4.557 4.525 4.579 VV 5587211 80920305 23.33% 1.176% 41 4.601 4.579 4.621 VV 4493707 65850847 18.99% 0.957% 42 4.641 4.621 4.703 VV 4687192 143875694 41.48% 2.091% 43 4.714 4.703 4.723 VV 1632365 18744404 5.40% 0.272% 44 4.747 4.723 4.779 VV 3731693 81484376 23.49% 1.184% 45 4.804 4.779 4.828 VV 4726469 89552592 25.82% 1.301% 46 4.840 4.828 4.857 VV 2893675 43917638 12.66% 0.638% 47 4.874 4.857 4.905 VV 2787347 66664074 19.22% 0.969% 48 4.943 4.905 4.973 VV 3705249 94971630 27.38% 1.380% 49 4.987 4.973 4.997 VV 1673410 23654005 6.82% 0.344% 50 5.013 4.997 5.038 VV 2110996 41552994 11.98% 0.604% 51 5.059 5.038 5.078 VV 1468491 32418401 9.35% 0.471% 52 5.107 5.078 5.120 VV 2133375 41425322 11.94% 0.602% 53 5.142 5.120 5.169 VV 5171012 91126054 26.27% 1.324% 54 5.183 5.169 5.200 VV 1641015 27112943 7.82% 0.394% 55 5.232 5.200 5.256 VV 1655781 46748710 13.48% 0.679% 56 5.283 5.256 5.307 VV 3888511 70141021 20.22% 1.019% 57 5.335 5.307 5.373 VV 6325117 165081223 47.60% 2.399% 58 5.390 5.373 5.467 VV 5920341 123593149 35.63% 1.796% 59 5.529 5.467 5.567 VV 25074719 346832715 100.00% 5.040% 60 5.583 5.567 5.622 VV 1737000 43789548 12.63% 0.636% 61 5.646 5.622 5.656 VV 2196441 33717827 9.72% 0.490% 62 5.684 5.656 5.705 VV 4563861 87166225 25.13% 1.267% 63 5.721 5.705 5.764 VV 2254689 53150611 15.32% 0.772% 64 5.796 5.764 5.848 VV 6851737 117866782 33.98% 1.713% 65 5.857 5.848 5.873 VV 956081 14262487 4.11% 0.207% 66 5.894 5.873 5.906 VV 1361854 22377055 6.45% 0.325% 67 5.927 5.906 5.956 VV 2516380 51051423 14.72% 0.742% 68 5.982 5.956 6.032 VV 8681330 142690734 41.14% 2.074% 69 6.055 6.032 6.075 VV 1832355 31622628 9.12% 0.460% 70 6.097 6.075 6.104 VV 1547650 22305027 6.43% 0.324% 71 6.127 6.104 6.182 VV 6996911 132649816 38.25% 1.928% 72 6.199 6.182 6.223 VV 1400826 25721094 7.42% 0.374% 73 6.246 6.223 6.270 VV 2488178 42788745 12.34% 0.622% 74 6.298 6.270 6.317 VV 8425194 126634586 36.51% 1.840% 75 6.333 6.317 6.366 VV 6299003 97922754 28.23% 1.423% 76 6.387 6.366 6.453 VV 3123765 62107155 17.91% 0.903% 77 6.492 6.472 6.500 VV 595276 9321720 2.69% 0.135% 78 6.522 6.500 6.559 VV 1312080 32475626 9.36% 0.472% 79 6.585 6.559 6.610 VV 4717617 70459789 20.32% 1.024% 80 6.621 6.610 6.646 VV 1123742 18141929 5.23% 0.264% 81 6.679 6.646 6.707 VV 2739934 47253374 13.62% 0.687% 82 6.726 6.707 6.742 VV 1450518 20586266 5.94% 0.299% 83 6.755 6.742 6.786 VV 1179650 20132335 5.80% 0.293% 84 6.827 6.786 6.866 VV 10779928 154804233 44.63% 2.250% 85 6.926 6.900 6.969 VV 574238 12956149 3.74% 0.188% 86 7.068 7.038 7.077 VV 341952 5207211 1.50% 0.076% 87 7.099 7.077 7.130 VV 2273074 32019705 9.23% 0.465% 88 7.163 7.130 7.227 VV 6590148 100634951 29.02% 1.463% 89 7.357 7.293 7.396 VV 215337 3267602 0.94% 0.047% 90 7.420 7.396 7.436 PV 162912 1870930 0.54% 0.027% 91 7.449 7.436 7.469 VV 79969 1029114 0.30% 0.015% 92 7.519 7.469 7.568 VV 949620 13492704 3.89% 0.196% 93 7.652 7.608 7.684 VV 2175296 28749941 8.29% 0.418% 94 7.699 7.684 7.721 VV 142968 2065680 0.60% 0.030% 95 7.819 7.721 7.847 VV 114804 2390120 0.69% 0.035% 96 7.868 7.847 7.891 PV 143635 2013494 0.58% 0.029% 97 7.915 7.891 7.956 VV 676059 9647355 2.78% 0.140% 98 8.010 7.956 8.034 VV 94268 2896665 0.84% 0.042% 99 8.126 8.034 8.189 VV 7020087 102944187 29.68% 1.496% 100 8.200 8.189 8.204 VV 243267 2092008 0.60% 0.030% 101 8.208 8.204 8.226 VV 235769 2850575 0.82% 0.041% 102 8.251 8.226 8.262 VV 243048 4934207 1.42% 0.072% 103 8.489 8.262 8.538 VV 1510886 80552410 23.23% 1.171% 104 8.541 8.538 8.552 VV 534342 4567493 1.32% 0.066% 105 8.606 8.552 8.639 VV 745878 31484641 9.08% 0.458% 106 8.646 8.639 8.660 VV 607706 7477670 2.16% 0.109% 107 8.816 8.660 8.839 VV 1083733 72767665 20.98% 1.058% 108 8.851 8.839 8.878 VV 880838 18994042 5.48% 0.276% 109 8.897 8.878 8.912 VV 742076 14798034 4.27% 0.215% 110 8.947 8.912 8.953 VV 726467 17756099 5.12% 0.258% 111 8.978 8.953 9.005 VV 751975 22815177 6.58% 0.332% 112 9.025 9.005 9.034 VV 723619 12356152 3.56% 0.180% 113 9.092 9.034 9.097 VV 790728 28927521 8.34% 0.420% 114 9.121 9.097 9.139 VV 792059 19161389 5.52% 0.278% 115 9.167 9.139 9.184 VV 819298 21680954 6.25% 0.315% 116 9.191 9.184 9.209 VV 787425 11301212 3.26% 0.164% 117 9.267 9.209 9.273 VV 809842 30571722 8.81% 0.444% 118 9.309 9.273 9.386 VV 1130066 59807330 17.24% 0.869% 119 9.427 9.386 9.451 VV 752234 29005484 8.36% 0.422% 120 9.777 9.451 9.806 VV 720593 150299511 43.33% 2.184% 121 10.325 9.806 10.369 VV 507062 190186199 54.84% 2.764% 122 10.463 10.369 10.488 VV 380850 27023907 7.79% 0.393% 123 10.640 10.488 10.651 VV 336735 31232394 9.01% 0.454% 124 10.700 10.651 10.736 VV 341826 15490162 4.47% 0.225% 125 10.815 10.736 10.904 VV 395555 25356903 7.31% 0.369% 126 10.945 10.904 11.003 VB 114846 4415925 1.27% 0.064% Sum of corrected areas: 6880984505