Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_O\Data\PO030218\ Data File : PO042722.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 13:26 Operator : SM/UA Sample : J1399-11MSD Misc : ALS Vial : 7 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Mar 01 14:55:49 2018 Quant Method : P:\HPCHEM1\ECD_O\methods\PO022118.M Quant Title : GC EXTRACTABLES QLast Update : Mon Feb 26 14:24:10 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Small noise peaks clipped Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30Mx0.32mmx 0.50µ Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 4.096 3.347 4561562 6368641 18.414m 17.234 2) SA Decachlor... 9.473 8.127 2926954 2616699 11.581m 6.786 # Target Compounds 3) L1 AR-1016-1 4.956 4.165 852578 1704089 126.951 180.024m# 4) L1 AR-1016-2 5.302 4.601 1613887 1731496 180.222 211.312 5) L1 AR-1016-3 5.396 4.641 1231766 2409533 170.483m 231.922m# 6) L1 AR-1016-4 5.824 4.804 668740 1768158 94.128 159.220 # 7) L1 AR-1016-5 6.050 5.143 1296385 1860558 180.083m 176.016 31) L7 AR-1260-1 6.780 5.796 1965496 2341898 142.867 97.004 # 32) L7 AR-1260-2 7.031 5.982 3036880 3312910 166.025 98.622 # 33) L7 AR-1260-3 7.307 6.127 2802435 2667382 134.872m 93.702m# 34) L7 AR-1260-4 7.385 6.298 1671473 3346719 112.929 97.894 35) L7 AR-1260-5 7.906 6.828 3448959 4142325 102.028 61.209 # --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.