Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042722.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 13:26 Sample : J1399-11MSD Misc : ALS Vial : 7 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.061 3.036 3.081 VV 384255 8648244 3.72% 0.200% 2 3.168 3.133 3.191 PV 837992 19053652 8.21% 0.440% 3 3.222 3.191 3.248 VV 1691810 25755889 11.09% 0.595% 4 3.281 3.248 3.313 PV 805269 17709550 7.63% 0.409% 5 3.352 3.313 3.366 VV 1062626 20547701 8.85% 0.475% 6 3.381 3.366 3.401 VV 1046995 17831632 7.68% 0.412% 7 3.442 3.401 3.467 VV 1130377 34562501 14.89% 0.799% 8 3.500 3.467 3.517 VV 1103567 28583365 12.31% 0.661% 9 3.553 3.517 3.568 VV 1084596 30675623 13.21% 0.709% 10 3.589 3.568 3.622 VV 1297140 30914466 13.31% 0.714% 11 3.664 3.622 3.694 VV 1371255 45781889 19.72% 1.058% 12 3.716 3.694 3.755 VV 1422934 37576096 16.18% 0.868% 13 3.778 3.755 3.792 VV 1316557 21197513 9.13% 0.490% 14 3.809 3.792 3.827 VV 1371386 25618501 11.03% 0.592% 15 3.843 3.827 3.876 VV 1361733 37350586 16.09% 0.863% 16 3.886 3.876 3.898 VV 1229044 15190742 6.54% 0.351% 17 3.933 3.898 3.970 VV 1296212 51029153 21.98% 1.179% 18 3.987 3.970 4.002 VV 1157915 20964987 9.03% 0.484% 19 4.013 4.002 4.025 VV 1146764 15460164 6.66% 0.357% 20 4.096 4.025 4.154 VV 15482300 232188105 100.00% 5.365% 21 4.191 4.154 4.211 VV 1065660 33545954 14.45% 0.775% 22 4.214 4.211 4.238 VV 1028881 15270925 6.58% 0.353% 23 4.290 4.238 4.325 VV 1270437 54740381 23.58% 1.265% 24 4.336 4.325 4.363 VV 1016126 22532533 9.70% 0.521% 25 4.382 4.363 4.429 VV 1591541 47653363 20.52% 1.101% 26 4.453 4.429 4.481 VV 3838307 64144900 27.63% 1.482% 27 4.491 4.481 4.510 VV 1214547 20716092 8.92% 0.479% 28 4.537 4.510 4.551 VV 1561760 32662860 14.07% 0.755% 29 4.561 4.551 4.575 VV 1422654 20270634 8.73% 0.468% 30 4.597 4.575 4.625 VV 1619410 40756905 17.55% 0.942% 31 4.776 4.735 4.792 VV 5129863 84912022 36.57% 1.962% 32 4.805 4.792 4.851 VV 3511241 71294735 30.71% 1.648% 33 4.865 4.851 4.876 VV 1465254 20855957 8.98% 0.482% 34 4.890 4.876 4.899 VV 1556276 20871494 8.99% 0.482% 35 4.914 4.899 4.923 VV 1723876 23195739 9.99% 0.536% 36 4.935 4.923 4.944 VV 1882506 22183241 9.55% 0.513% 37 4.956 4.944 4.975 VV 2572746 29599080 12.75% 0.684% 38 4.985 4.975 4.996 PV 341511 2725357 1.17% 0.063% 39 5.027 4.996 5.050 VV 1277770 33034283 14.23% 0.763% 40 5.074 5.050 5.093 VV 1386264 33092954 14.25% 0.765% 41 5.125 5.093 5.139 VV 2290917 45417884 19.56% 1.050% 42 5.162 5.139 5.196 VV 4723542 84133929 36.24% 1.944% 43 5.221 5.196 5.229 VV 6584485 77694114 33.46% 1.795% 44 5.241 5.229 5.276 VV 7955349 111400078 47.98% 2.574% 45 5.302 5.276 5.339 VV 4740488 80864614 34.83% 1.869% 46 5.371 5.339 5.379 VV 1810209 32449721 13.98% 0.750% 47 5.396 5.379 5.420 VV 4206267 59460113 25.61% 1.374% 48 5.432 5.420 5.464 VV 1115192 23733414 10.22% 0.548% 49 5.487 5.464 5.508 VV 3919077 53484806 23.04% 1.236% 50 5.527 5.508 5.553 VV 2935734 36396831 15.68% 0.841% 51 5.567 5.553 5.592 VV 761667 10694424 4.61% 0.247% 52 5.614 5.592 5.628 PV 1389028 16858512 7.26% 0.390% 53 5.640 5.628 5.655 VV 1362610 15914409 6.85% 0.368% 54 5.682 5.655 5.703 VV 4484777 61833360 26.63% 1.429% 55 5.723 5.703 5.745 VV 2059715 34149967 14.71% 0.789% 56 5.765 5.745 5.804 VV 1717145 37936088 16.34% 0.877% 57 5.824 5.804 5.861 VV 2031388 42499132 18.30% 0.982% 58 5.882 5.861 5.912 VV 1821731 34383647 14.81% 0.795% 59 5.928 5.912 5.967 VV 725778 21055750 9.07% 0.487% 60 5.994 5.967 6.005 VV 672588 14105887 6.08% 0.326% 61 6.050 6.005 6.093 VV 3598655 86086114 37.08% 1.989% 62 6.113 6.093 6.164 VV 1152600 36950545 15.91% 0.854% 63 6.200 6.164 6.223 VV 1138509 25693299 11.07% 0.594% 64 6.263 6.223 6.289 VV 4100714 66017940 28.43% 1.526% 65 6.316 6.289 6.342 VV 4426621 71487186 30.79% 1.652% 66 6.354 6.342 6.368 VV 867709 12635910 5.44% 0.292% 67 6.393 6.368 6.430 VV 6663448 93196585 40.14% 2.154% 68 6.463 6.430 6.496 VV 646624 21197670 9.13% 0.490% 69 6.524 6.496 6.550 VV 19710431 227184551 97.85% 5.250% 70 6.563 6.550 6.591 VV 1364598 18424989 7.94% 0.426% 71 6.621 6.591 6.650 VV 2196452 35670877 15.36% 0.824% 72 6.677 6.650 6.715 VV 2928630 54043289 23.28% 1.249% 73 6.728 6.715 6.753 VV 1058809 15729742 6.77% 0.363% 74 6.780 6.753 6.833 VV 5365997 74401219 32.04% 1.719% 75 6.862 6.833 6.875 VV 431799 8904453 3.84% 0.206% 76 6.897 6.875 6.918 VV 1180475 17645769 7.60% 0.408% 77 6.962 6.918 6.994 VV 1669293 37399581 16.11% 0.864% 78 7.031 6.994 7.054 VV 7618401 105292417 45.35% 2.433% 79 7.072 7.054 7.093 VV 2279557 29509555 12.71% 0.682% 80 7.112 7.093 7.134 VV 1522394 20269207 8.73% 0.468% 81 7.157 7.134 7.178 VV 2922122 37784160 16.27% 0.873% 82 7.188 7.178 7.209 VV 631374 7960999 3.43% 0.184% 83 7.263 7.209 7.279 VV 733593 17930274 7.72% 0.414% 84 7.308 7.279 7.360 VV 6818010 121957656 52.53% 2.818% 85 7.385 7.360 7.418 VV 4529931 59576638 25.66% 1.377% 86 7.442 7.418 7.473 VV 2480145 34025481 14.65% 0.786% 87 7.511 7.473 7.546 VV 255274 9024771 3.89% 0.209% 88 7.571 7.546 7.580 VV 964144 12385350 5.33% 0.286% 89 7.605 7.580 7.653 VV 3998555 60635339 26.11% 1.401% 90 7.683 7.653 7.714 VV 2219559 31870262 13.73% 0.736% 91 7.735 7.714 7.760 VV 1169519 16435415 7.08% 0.380% 92 7.786 7.760 7.810 VV 414942 9110034 3.92% 0.211% 93 7.836 7.810 7.863 VV 1451155 20793305 8.96% 0.480% 94 7.906 7.863 7.936 VV 9476532 119370060 51.41% 2.758% 95 7.953 7.936 7.994 VV 644194 11502347 4.95% 0.266% 96 8.019 7.994 8.067 VV 414614 9675898 4.17% 0.224% 97 8.192 8.067 8.218 PV 4373265 81288504 35.01% 1.878% 98 8.245 8.218 8.339 VV 1739227 51252718 22.07% 1.184% 99 8.462 8.339 8.502 VV 274453 13644200 5.88% 0.315% 100 8.541 8.502 8.569 VV 203466 4593978 1.98% 0.106% 101 8.597 8.569 8.628 VV 917752 13157036 5.67% 0.304% 102 8.671 8.628 8.714 VB 58321 1960916 0.84% 0.045% 103 8.831 8.799 8.868 PV 1885517 27586416 11.88% 0.637% 104 8.908 8.868 8.931 PB 109695 1682788 0.72% 0.039% 105 9.186 9.149 9.226 BV 608272 9802740 4.22% 0.227% 106 9.473 9.226 9.526 PV 5452804 101186890 43.58% 2.338% 107 9.578 9.526 9.658 VV 1287720 27799152 11.97% 0.642% 108 9.746 9.658 9.796 VV 139699 4037035 1.74% 0.093% 109 10.043 9.841 10.072 PV 183429 5670633 2.44% 0.131% 110 10.099 10.072 10.133 VV 107614 2090687 0.90% 0.048% 111 10.625 10.433 10.686 BV 134709 9068507 3.91% 0.210% 112 10.730 10.686 10.823 VV 363659 9670382 4.16% 0.223% Sum of corrected areas: 4327437915 Signal #2 : ECD2B.CH 1 2.547 2.506 2.568 BV 570181 7544369 2.35% 0.122% 2 2.579 2.568 2.589 PV 294893 2581842 0.80% 0.042% 3 2.608 2.589 2.638 VV 777913 14904311 4.64% 0.241% 4 2.668 2.638 2.688 PV 1148749 21647649 6.75% 0.351% 5 2.692 2.688 2.711 VV 621055 6226766 1.94% 0.101% 6 2.760 2.711 2.782 VV 1230076 39237564 12.23% 0.635% 7 2.830 2.782 2.848 VV 1511681 48704990 15.18% 0.789% 8 2.857 2.848 2.869 VV 1151821 13714553 4.27% 0.222% 9 2.898 2.869 2.919 VV 1586378 39975100 12.46% 0.647% 10 2.956 2.919 2.971 VV 1546286 42912562 13.37% 0.695% 11 2.984 2.971 3.007 VV 1599035 26193917 8.16% 0.424% 12 3.027 3.007 3.035 VV 1182165 14632215 4.56% 0.237% 13 3.069 3.035 3.106 VV 1746669 59625445 18.58% 0.966% 14 3.147 3.106 3.166 VV 1710974 48179561 15.01% 0.780% 15 3.179 3.166 3.194 VV 1651733 26273096 8.19% 0.425% 16 3.224 3.194 3.266 VV 1925931 77152921 24.04% 1.249% 17 3.278 3.266 3.293 VV 1860261 29605096 9.23% 0.479% 18 3.347 3.293 3.381 VV 20460435 315329439 98.26% 5.107% 19 3.389 3.381 3.432 VV 2533685 64990195 20.25% 1.052% 20 3.468 3.432 3.506 VV 2334904 93850764 29.25% 1.520% 21 3.549 3.506 3.586 VV 2959369 114157373 35.57% 1.849% 22 3.632 3.586 3.673 VV 3459243 143502416 44.72% 2.324% 23 3.702 3.673 3.731 VV 5911178 129733382 40.43% 2.101% 24 3.746 3.731 3.778 VV 3186028 82397014 25.68% 1.334% 25 3.852 3.846 3.875 VV 2682537 27288689 8.50% 0.442% 26 3.984 3.875 4.044 PV 6683384 301999353 94.11% 4.891% 27 4.058 4.044 4.093 VV 2762086 69275077 21.59% 1.122% 28 4.101 4.093 4.118 VV 2008565 27799015 8.66% 0.450% 29 4.165 4.118 4.193 VV 5225898 128293330 39.98% 2.078% 30 4.210 4.193 4.224 VV 1904897 31922411 9.95% 0.517% 31 4.274 4.224 4.287 VV 3079672 98557109 30.71% 1.596% 32 4.299 4.287 4.339 VV 3016083 55752200 17.37% 0.903% 33 4.391 4.339 4.426 VV 8099558 156728181 48.84% 2.538% 34 4.446 4.426 4.481 VV 5222427 92367615 28.78% 1.496% 35 4.496 4.481 4.525 VV 1821528 44137403 13.75% 0.715% 36 4.557 4.525 4.579 VV 5690892 82030427 25.56% 1.328% 37 4.602 4.579 4.621 VV 4480649 66249085 20.64% 1.073% 38 4.642 4.621 4.703 VV 4709855 142895811 44.53% 2.314% 39 4.714 4.703 4.724 VV 1621513 20492746 6.39% 0.332% 40 4.748 4.724 4.779 VV 3654453 79492995 24.77% 1.287% 41 4.805 4.779 4.828 VV 4631329 88877976 27.70% 1.439% 42 4.840 4.828 4.858 VV 2865512 43605881 13.59% 0.706% 43 4.874 4.858 4.906 VV 2777961 65826547 20.51% 1.066% 44 4.944 4.906 4.974 VV 3714159 95320798 29.70% 1.544% 45 4.986 4.974 4.997 VV 1688146 22757343 7.09% 0.369% 46 5.014 4.997 5.037 VV 2118620 41799079 13.03% 0.677% 47 5.059 5.037 5.079 VV 1466401 34054983 10.61% 0.552% 48 5.107 5.079 5.121 VV 2146479 41184730 12.83% 0.667% 49 5.143 5.121 5.170 VV 5149088 90884248 28.32% 1.472% 50 5.183 5.170 5.212 VV 1644059 36213405 11.28% 0.586% 51 5.232 5.212 5.256 VV 1633648 36827885 11.48% 0.596% 52 5.283 5.256 5.309 VV 3789729 70261995 21.90% 1.138% 53 5.335 5.309 5.373 VV 6094482 157302689 49.02% 2.547% 54 5.391 5.373 5.468 VV 5586370 115959334 36.14% 1.878% 55 5.529 5.468 5.567 VV 23305821 320903280 100.00% 5.197% 56 5.584 5.567 5.622 VV 1514487 37407352 11.66% 0.606% 57 5.647 5.622 5.658 VV 1955895 30968023 9.65% 0.502% 58 5.684 5.658 5.706 VV 4259276 79138565 24.66% 1.282% 59 5.722 5.706 5.765 VV 2013895 47651305 14.85% 0.772% 60 5.796 5.765 5.848 VV 6438811 108463350 33.80% 1.756% 61 5.855 5.848 5.873 VV 819707 11932214 3.72% 0.193% 62 5.894 5.873 5.906 VV 1239198 20044343 6.25% 0.325% 63 5.927 5.906 5.955 VV 2339850 46778842 14.58% 0.758% 64 5.982 5.955 6.032 VV 8210946 135425143 42.20% 2.193% 65 6.055 6.032 6.075 VV 1755894 30150677 9.40% 0.488% 66 6.096 6.075 6.104 VV 1518765 21238567 6.62% 0.344% 67 6.127 6.104 6.182 VV 6798556 128803079 40.14% 2.086% 68 6.200 6.182 6.223 VV 1337341 24241656 7.55% 0.393% 69 6.246 6.223 6.270 VV 2387783 40650948 12.67% 0.658% 70 6.298 6.270 6.317 VV 8151551 121739480 37.94% 1.971% 71 6.333 6.317 6.368 VV 6138644 94252494 29.37% 1.526% 72 6.387 6.368 6.453 VV 3055788 57984653 18.07% 0.939% 73 6.522 6.453 6.559 VV 1260741 45507359 14.18% 0.737% 74 6.585 6.559 6.611 VV 4531666 68192975 21.25% 1.104% 75 6.622 6.611 6.646 VV 1096636 17038079 5.31% 0.276% 76 6.679 6.646 6.707 VV 2672164 45240224 14.10% 0.733% 77 6.727 6.707 6.743 VV 1369027 19866836 6.19% 0.322% 78 6.756 6.743 6.788 VV 1114661 19417680 6.05% 0.314% 79 6.828 6.788 6.868 VV 10386414 148565606 46.30% 2.406% 80 6.927 6.904 6.966 VV 573686 12479151 3.89% 0.202% 81 7.100 7.038 7.130 VV 2225915 37053677 11.55% 0.600% 82 7.163 7.130 7.225 VV 6376292 98010262 30.54% 1.587% 83 7.358 7.334 7.398 VV 211596 3006661 0.94% 0.049% 84 7.420 7.398 7.436 PV 149291 1733159 0.54% 0.028% 85 7.449 7.436 7.464 VV 82012 995600 0.31% 0.016% 86 7.519 7.464 7.568 VV 889869 12717017 3.96% 0.206% 87 7.590 7.568 7.604 VV 36617 429973 0.13% 0.007% 88 7.653 7.604 7.686 PV 2088136 27490280 8.57% 0.445% 89 7.697 7.686 7.726 VV 138141 2047805 0.64% 0.033% 90 7.819 7.726 7.841 VV 122125 2677327 0.83% 0.043% 91 7.868 7.841 7.891 PV 125749 1620967 0.51% 0.026% 92 7.916 7.891 7.954 PV 590011 7573981 2.36% 0.123% 93 8.127 7.954 8.166 PV 6519823 82371328 25.67% 1.334% 94 8.490 8.414 8.534 BV 1113513 22532184 7.02% 0.365% 95 8.607 8.534 8.629 VV 332241 10776369 3.36% 0.175% 96 8.643 8.629 8.679 VV 212184 5656035 1.76% 0.092% 97 8.818 8.679 8.839 VV 628493 25999258 8.10% 0.421% 98 8.853 8.839 8.879 VV 451808 9489571 2.96% 0.154% 99 8.977 8.879 8.993 VV 358794 23280593 7.25% 0.377% 100 9.313 8.993 9.355 VV 688526 83291757 25.96% 1.349% 101 9.715 9.355 9.728 VV 322782 69045619 21.52% 1.118% 102 9.765 9.728 9.813 VV 290302 13568031 4.23% 0.220% 103 10.230 9.813 10.248 VV 74354 37349380 11.64% 0.605% 104 10.330 10.248 10.361 VB 71206 3394320 1.06% 0.055% 105 10.710 10.528 10.741 BV 167578 9606876 2.99% 0.156% 106 10.817 10.741 10.916 VV 258278 13071482 4.07% 0.212% 107 10.947 10.916 10.975 VV 49986 1059012 0.33% 0.017% 108 11.419 11.328 11.529 BB 122962 5811796 1.81% 0.094% Sum of corrected areas: 6174973078