Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_O\Data\PO030218\ Data File : PO042724.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 13:56 Operator : SM/UA Sample : J1400-11MSD Misc : ALS Vial : 9 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Mar 01 15:09:02 2018 Quant Method : P:\HPCHEM1\ECD_O\methods\PO022118.M Quant Title : GC EXTRACTABLES QLast Update : Mon Feb 26 14:24:10 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Small noise peaks clipped Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30Mx0.32mmx 0.50µ Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 4.096 3.347 4582387 5730228 18.498m 15.507m 2) SA Decachlor... 9.472 8.125 2543349 2404824 10.063 6.236 # Target Compounds 3) L1 AR-1016-1 4.951 4.167 793638 1573821 118.175m 166.262m# 4) L1 AR-1016-2 5.302 4.603 1320318 1738605 147.439 212.179 # 5) L1 AR-1016-3 5.397 4.639 961712 2394443 133.106m 230.470 # 6) L1 AR-1016-4 5.829 4.803 186466 1538260 26.246m 138.518m# 7) L1 AR-1016-5 6.049 5.139 889821 1058347 123.606m 100.124 31) L7 AR-1260-1 6.781 5.795 1792735 2374319 130.310 98.347 32) L7 AR-1260-2 7.032 5.982 2345359 3430637 128.220 102.127 33) L7 AR-1260-3 7.308 6.127 2443614 2461879 117.603m 86.483 # 34) L7 AR-1260-4 7.385 6.298 1334913 2976408 90.190 87.062 35) L7 AR-1260-5 7.906 6.828 3195607 4182504 94.534 61.803 # --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.