Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042724.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 13:56 Sample : J1400-11MSD Misc : ALS Vial : 9 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.018 3.006 3.037 BV 199360 1871581 1.12% 0.055% 2 3.068 3.037 3.088 PV 462206 10505542 6.29% 0.309% 3 3.095 3.088 3.124 VV 472797 6087840 3.65% 0.179% 4 3.146 3.124 3.157 PV 556250 6898253 4.13% 0.203% 5 3.171 3.157 3.192 VV 638442 10116646 6.06% 0.298% 6 3.223 3.192 3.253 VV 1122135 22583149 13.53% 0.665% 7 3.262 3.253 3.274 VV 365455 3690126 2.21% 0.109% 8 3.284 3.274 3.297 VV 386058 3228854 1.93% 0.095% 9 3.311 3.297 3.319 PV 280856 2291436 1.37% 0.067% 10 3.348 3.319 3.367 VV 743432 15716930 9.41% 0.463% 11 3.381 3.367 3.410 VV 597981 12449353 7.46% 0.366% 12 3.417 3.410 3.425 VV 411021 3465473 2.08% 0.102% 13 3.443 3.425 3.456 VV 695732 10508810 6.30% 0.309% 14 3.464 3.456 3.485 VV 565707 9011662 5.40% 0.265% 15 3.504 3.485 3.518 VV 600937 9677016 5.80% 0.285% 16 3.555 3.518 3.571 VV 646047 16885714 10.12% 0.497% 17 3.588 3.571 3.605 VV 743604 12783570 7.66% 0.376% 18 3.614 3.605 3.624 VV 670212 7245082 4.34% 0.213% 19 3.637 3.624 3.654 VV 785099 12946276 7.76% 0.381% 20 3.663 3.654 3.674 VV 749077 8673538 5.20% 0.255% 21 3.681 3.674 3.701 VV 705125 9780925 5.86% 0.288% 22 3.723 3.701 3.738 VV 729415 13512732 8.09% 0.398% 23 3.779 3.760 3.791 VV 670979 10845371 6.50% 0.319% 24 3.809 3.791 3.827 VV 664351 13005027 7.79% 0.383% 25 3.841 3.827 3.881 VV 722873 19613201 11.75% 0.577% 26 3.936 3.912 3.970 VV 486030 13841541 8.29% 0.407% 27 3.992 3.970 4.028 VV 426749 11628623 6.97% 0.342% 28 4.038 4.028 4.048 VV 313117 3419868 2.05% 0.101% 29 4.097 4.048 4.154 VV 14267403 166935212 100.00% 4.914% 30 4.192 4.154 4.210 VV 336463 8463925 5.07% 0.249% 31 4.222 4.210 4.244 VV 290246 4886252 2.93% 0.144% 32 4.289 4.244 4.332 VV 519642 13330127 7.99% 0.392% 33 4.382 4.356 4.411 VV 658934 9707375 5.82% 0.286% 34 4.453 4.430 4.502 VV 2832984 32993335 19.76% 0.971% 35 4.565 4.551 4.579 VV 228031 3001022 1.80% 0.088% 36 4.598 4.579 4.629 VV 706307 13402167 8.03% 0.395% 37 4.777 4.750 4.793 VV 4581736 62713741 37.57% 1.846% 38 4.805 4.793 4.845 VV 3074851 58174186 34.85% 1.713% 39 4.862 4.845 4.878 VV 1698420 30185285 18.08% 0.889% 40 4.891 4.878 4.901 VV 1624484 21568987 12.92% 0.635% 41 4.914 4.901 4.927 VV 1834094 28279876 16.94% 0.833% 42 4.951 4.940 4.977 VV 2144751 29398085 17.61% 0.865% 43 5.018 4.977 5.030 PV 1646094 41274615 24.72% 1.215% 44 5.065 5.030 5.090 VV 1709029 59041299 35.37% 1.738% 45 5.125 5.090 5.140 VV 2503199 57763165 34.60% 1.701% 46 5.160 5.140 5.185 VV 2471994 54813430 32.84% 1.614% 47 5.221 5.185 5.230 VV 6122925 89818938 53.80% 2.644% 48 5.242 5.230 5.275 VV 7185778 103902367 62.24% 3.059% 49 5.302 5.275 5.341 VV 4172310 84169300 50.42% 2.478% 50 5.364 5.341 5.379 VV 1674481 30901374 18.51% 0.910% 51 5.398 5.379 5.423 VV 3795290 55024101 32.96% 1.620% 52 5.432 5.423 5.442 VV 1079944 11929124 7.15% 0.351% 53 5.488 5.442 5.511 VV 3809735 81316720 48.71% 2.394% 54 5.527 5.511 5.552 VV 3065650 36559192 21.90% 1.076% 55 5.566 5.552 5.592 VV 622059 9247035 5.54% 0.272% 56 5.611 5.592 5.627 VV 998174 11739601 7.03% 0.346% 57 5.638 5.627 5.652 VV 547792 4420924 2.65% 0.130% 58 5.681 5.652 5.700 PV 3613528 46056259 27.59% 1.356% 59 5.724 5.700 5.745 VV 2333867 41603208 24.92% 1.225% 60 5.766 5.745 5.807 VV 2147696 52274137 31.31% 1.539% 61 5.829 5.807 5.851 VV 1880986 33695127 20.18% 0.992% 62 5.884 5.851 5.912 VV 1809925 50785061 30.42% 1.495% 63 5.941 5.912 5.958 VV 1156913 30404002 18.21% 0.895% 64 5.988 5.958 6.017 VV 1497445 43029677 25.78% 1.267% 65 6.049 6.017 6.067 VV 3469340 62330332 37.34% 1.835% 66 6.075 6.067 6.094 VV 1791692 25279947 15.14% 0.744% 67 6.111 6.094 6.143 VV 1469857 36135167 21.65% 1.064% 68 6.200 6.169 6.228 VV 1367181 39227307 23.50% 1.155% 69 6.263 6.228 6.290 VV 3531745 66940670 40.10% 1.971% 70 6.316 6.290 6.371 VV 2277182 62926362 37.70% 1.853% 71 6.393 6.371 6.429 VV 2597660 48265590 28.91% 1.421% 72 6.465 6.429 6.493 VV 883114 30611785 18.34% 0.901% 73 6.526 6.493 6.548 VV 1945883 40865966 24.48% 1.203% 74 6.564 6.548 6.589 VV 1600147 27695745 16.59% 0.815% 75 6.620 6.589 6.646 VV 2092641 36211293 21.69% 1.066% 76 6.677 6.646 6.714 VV 3108751 61945471 37.11% 1.824% 77 6.728 6.714 6.754 VV 1265681 21431567 12.84% 0.631% 78 6.781 6.754 6.833 VV 5399170 83319953 49.91% 2.453% 79 6.865 6.833 6.873 VV 521144 12554473 7.52% 0.370% 80 6.898 6.873 6.923 VV 1357232 24770228 14.84% 0.729% 81 6.965 6.923 6.993 VV 1364093 30697214 18.39% 0.904% 82 7.032 6.993 7.055 VV 6605592 89889326 53.85% 2.646% 83 7.072 7.055 7.094 VV 2326443 31540355 18.89% 0.929% 84 7.112 7.094 7.134 VV 1597489 23115810 13.85% 0.681% 85 7.158 7.134 7.178 VV 2924368 39931442 23.92% 1.176% 86 7.189 7.178 7.210 VV 787569 11198042 6.71% 0.330% 87 7.263 7.210 7.279 VV 839913 21229648 12.72% 0.625% 88 7.308 7.279 7.330 VV 6344167 90771761 54.38% 2.672% 89 7.338 7.330 7.361 VV 1158014 15860936 9.50% 0.467% 90 7.385 7.361 7.415 VV 4165005 54794183 32.82% 1.613% 91 7.442 7.415 7.472 VV 2049652 27971705 16.76% 0.823% 92 7.571 7.516 7.580 VV 869812 13687173 8.20% 0.403% 93 7.606 7.580 7.650 VV 3631534 55461393 33.22% 1.633% 94 7.683 7.650 7.716 VV 2011472 28014167 16.78% 0.825% 95 7.735 7.716 7.763 VV 1049184 13724620 8.22% 0.404% 96 7.791 7.763 7.810 VV 235557 4059800 2.43% 0.120% 97 7.836 7.810 7.861 VV 1200439 15553018 9.32% 0.458% 98 7.906 7.861 7.935 VV 8623589 105995113 63.49% 3.120% 99 7.953 7.935 7.987 VV 438264 6043926 3.62% 0.178% 100 8.193 8.071 8.218 BV 3992164 64063448 38.38% 1.886% 101 8.245 8.218 8.256 VV 1530483 23620306 14.15% 0.695% 102 8.260 8.256 8.309 VB 1342331 14089734 8.44% 0.415% 103 8.463 8.363 8.490 BV 173049 4179756 2.50% 0.123% 104 8.542 8.490 8.569 VV 135399 2700282 1.62% 0.079% 105 8.598 8.569 8.634 VV 808254 11144967 6.68% 0.328% 106 8.662 8.634 8.709 VB 53981 1293107 0.77% 0.038% 107 8.831 8.721 8.876 BV 1774742 26152229 15.67% 0.770% 108 8.908 8.888 8.948 VB 101869 1647092 0.99% 0.048% 109 9.187 9.128 9.239 BV 526746 8676152 5.20% 0.255% 110 9.472 9.394 9.531 BV 5086723 84117382 50.39% 2.476% Sum of corrected areas: 3396828314 Signal #2 : ECD2B.CH 1 2.551 2.506 2.570 BV 584828 5103712 1.77% 0.081% 2 2.604 2.570 2.639 VV 749987 20190756 7.01% 0.319% 3 2.675 2.639 2.699 PV 991812 24675150 8.57% 0.390% 4 2.705 2.699 2.729 VV 820695 14269505 4.96% 0.225% 5 2.745 2.729 2.756 VV 902654 13352974 4.64% 0.211% 6 2.804 2.756 2.823 VV 1177411 42292346 14.69% 0.668% 7 2.834 2.823 2.868 VV 1302802 31095841 10.80% 0.491% 8 2.900 2.868 2.922 VV 1491080 40446831 14.05% 0.639% 9 2.936 2.922 2.943 VV 1310586 16229739 5.64% 0.256% 10 2.962 2.943 3.008 VV 1566819 57051209 19.82% 0.901% 11 3.021 3.008 3.035 VV 1469076 22826756 7.93% 0.360% 12 3.052 3.035 3.106 VV 1682115 66963266 23.26% 1.057% 13 3.129 3.106 3.142 VV 1654848 33482545 11.63% 0.529% 14 3.148 3.142 3.165 VV 1657443 21830999 7.58% 0.345% 15 3.178 3.165 3.198 VV 1767749 33254340 11.55% 0.525% 16 3.225 3.198 3.250 VV 1915020 55714656 19.36% 0.880% 17 3.255 3.250 3.276 VV 1900651 29547504 10.26% 0.467% 18 3.300 3.276 3.309 VV 2060377 39012508 13.55% 0.616% 19 3.348 3.309 3.383 VV 18406656 287855983 100.00% 4.545% 20 3.388 3.383 3.429 VV 2763057 67978469 23.62% 1.073% 21 3.450 3.429 3.470 VV 2446045 59870676 20.80% 0.945% 22 3.485 3.470 3.510 VV 2515927 58792998 20.42% 0.928% 23 3.550 3.510 3.570 VV 3001028 95203123 33.07% 1.503% 24 3.579 3.570 3.588 VV 2700844 30231759 10.50% 0.477% 25 3.602 3.588 3.614 VV 2783293 41394099 14.38% 0.654% 26 3.632 3.614 3.670 VV 3577251 103036924 35.79% 1.627% 27 3.702 3.670 3.737 VV 6114907 152239947 52.89% 2.404% 28 3.828 3.801 3.844 VV 3121316 77744078 27.01% 1.228% 29 3.923 3.876 3.928 PV 2220745 41761049 14.51% 0.659% 30 3.958 3.928 3.963 VV 2631943 51801855 18.00% 0.818% 31 3.984 3.963 4.034 VV 6428043 173427056 60.25% 2.738% 32 4.056 4.034 4.094 VV 2703323 84145968 29.23% 1.329% 33 4.106 4.094 4.120 VV 1939833 28390693 9.86% 0.448% 34 4.167 4.120 4.192 VV 4676267 113794481 39.53% 1.797% 35 4.211 4.192 4.227 VV 1799003 32089819 11.15% 0.507% 36 4.275 4.227 4.283 VV 3050630 72719194 25.26% 1.148% 37 4.298 4.283 4.338 VV 3439622 67185462 23.34% 1.061% 38 4.392 4.338 4.425 PV 6838254 127844277 44.41% 2.019% 39 4.446 4.425 4.473 VV 4631951 68465391 23.78% 1.081% 40 4.498 4.473 4.523 VV 2267945 51519804 17.90% 0.813% 41 4.556 4.523 4.579 VV 5815329 84550527 29.37% 1.335% 42 4.603 4.579 4.619 VV 4518514 64244015 22.32% 1.014% 43 4.639 4.619 4.658 VV 5609771 99331966 34.51% 1.568% 44 4.666 4.658 4.706 VV 3632318 79472127 27.61% 1.255% 45 4.715 4.706 4.721 VV 1986570 17609856 6.12% 0.278% 46 4.755 4.721 4.781 VV 2625017 84898027 29.49% 1.341% 47 4.803 4.781 4.827 VV 5938639 112522539 39.09% 1.777% 48 4.840 4.827 4.857 VV 3802594 60861352 21.14% 0.961% 49 4.871 4.857 4.893 VV 3620210 65606038 22.79% 1.036% 50 4.942 4.893 4.979 VV 5031412 167214866 58.09% 2.640% 51 5.012 4.979 5.047 VV 3041106 100273426 34.83% 1.583% 52 5.070 5.047 5.077 VV 2020529 34471588 11.98% 0.544% 53 5.107 5.077 5.119 VV 2576562 57871535 20.10% 0.914% 54 5.139 5.119 5.165 VV 5114740 93701650 32.55% 1.480% 55 5.178 5.165 5.198 VV 2420377 43903127 15.25% 0.693% 56 5.230 5.198 5.258 VV 2279625 72194094 25.08% 1.140% 57 5.283 5.258 5.305 VV 4518845 75512193 26.23% 1.192% 58 5.334 5.305 5.373 VV 3582796 104641644 36.35% 1.652% 59 5.390 5.373 5.465 VV 3109997 105011895 36.48% 1.658% 60 5.529 5.465 5.562 VV 2787110 99443059 34.55% 1.570% 61 5.584 5.562 5.621 VV 1940490 54978275 19.10% 0.868% 62 5.647 5.621 5.656 VV 2398914 39582581 13.75% 0.625% 63 5.683 5.656 5.705 VV 4770345 94175601 32.72% 1.487% 64 5.722 5.705 5.766 VV 2486129 66660598 23.16% 1.053% 65 5.795 5.766 5.843 VV 7062928 127668436 44.35% 2.016% 66 5.854 5.843 5.873 VV 1197037 21093580 7.33% 0.333% 67 5.895 5.873 5.906 VV 1642190 27617441 9.59% 0.436% 68 5.924 5.906 5.955 VV 2422098 48782775 16.95% 0.770% 69 5.982 5.955 6.031 VV 8406235 136323962 47.36% 2.153% 70 6.055 6.031 6.082 VV 1016456 24965455 8.67% 0.394% 71 6.127 6.082 6.175 VV 6659966 120123574 41.73% 1.897% 72 6.199 6.175 6.224 VV 1296297 26956846 9.36% 0.426% 73 6.246 6.224 6.270 VV 2261840 38321344 13.31% 0.605% 74 6.298 6.270 6.317 VV 7291761 111123809 38.60% 1.755% 75 6.334 6.317 6.366 VV 5518316 85638517 29.75% 1.352% 76 6.387 6.366 6.446 VV 2921544 53853341 18.71% 0.850% 77 6.521 6.475 6.557 VV 1148441 30274095 10.52% 0.478% 78 6.585 6.557 6.610 VV 4426039 63138576 21.93% 0.997% 79 6.622 6.610 6.647 VV 909671 13928225 4.84% 0.220% 80 6.679 6.647 6.706 VV 2496725 38952019 13.53% 0.615% 81 6.726 6.706 6.742 VV 1290608 17740842 6.16% 0.280% 82 6.756 6.742 6.788 VV 1017362 16414089 5.70% 0.259% 83 6.828 6.788 6.867 VV 10451187 145063924 50.39% 2.291% 84 6.881 6.867 6.906 VV 313510 4791819 1.66% 0.076% 85 6.926 6.906 6.988 VB 352350 5464081 1.90% 0.086% 86 7.099 7.044 7.132 PV 2066726 28693220 9.97% 0.453% 87 7.163 7.132 7.241 VV 6215516 91214680 31.69% 1.440% 88 7.359 7.331 7.394 VV 200456 3084179 1.07% 0.049% 89 7.419 7.394 7.435 PV 112606 1127372 0.39% 0.018% 90 7.519 7.484 7.555 BV 891860 11832664 4.11% 0.187% 91 7.653 7.619 7.684 PV 2056198 26312190 9.14% 0.415% 92 7.697 7.684 7.723 VV 105699 1451499 0.50% 0.023% 93 7.872 7.723 7.881 VV 17414 1634119 0.57% 0.026% 94 7.915 7.881 7.956 PV 603416 7930870 2.76% 0.125% 95 8.125 7.956 8.175 VV 6020124 85900097 29.84% 1.356% 96 8.343 8.175 8.349 VV 271584 21917528 7.61% 0.346% 97 8.492 8.349 8.512 VV 488500 34117747 11.85% 0.539% 98 8.614 8.512 8.653 VV 650552 40365027 14.02% 0.637% 99 8.720 8.653 8.726 VV 507295 21969827 7.63% 0.347% 100 8.962 8.726 8.970 VV 592752 80689109 28.03% 1.274% 101 8.979 8.970 8.984 VV 585931 4542311 1.58% 0.072% 102 9.126 8.984 9.133 VV 591145 52077095 18.09% 0.822% 103 9.241 9.133 9.248 VV 639445 42145925 14.64% 0.665% 104 9.316 9.248 9.353 VV 637300 39073627 13.57% 0.617% 105 9.362 9.353 9.374 VV 597964 7567618 2.63% 0.119% 106 9.541 9.374 9.547 VV 555358 58288659 20.25% 0.920% 107 9.569 9.547 9.574 VV 548159 8507583 2.96% 0.134% 108 9.718 9.574 9.788 VV 850482 76303973 26.51% 1.205% 109 9.814 9.788 9.843 VV 500277 16113474 5.60% 0.254% 110 9.882 9.843 9.888 VV 459205 12354032 4.29% 0.195% 111 9.893 9.888 9.898 VV 462784 2681419 0.93% 0.042% 112 9.957 9.898 9.962 VV 437789 16854718 5.86% 0.266% 113 10.026 9.962 10.031 VV 428697 17500244 6.08% 0.276% 114 10.052 10.031 10.057 VV 413554 6534426 2.27% 0.103% 115 10.084 10.057 10.093 VV 375723 7936891 2.76% 0.125% 116 10.324 10.261 10.341 VV 288828 13194942 4.58% 0.208% 117 10.706 10.619 10.718 VV 37396 1465646 0.51% 0.023% Sum of corrected areas: 6333185781