Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042725.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 14:15 Sample : J1399-11RE Misc : ALS Vial : 4 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.025 3.009 3.040 BV 336764 3094604 2.80% 0.128% 2 3.059 3.040 3.067 VV 633291 7248424 6.57% 0.301% 3 3.077 3.067 3.112 VV 778367 15884029 14.40% 0.659% 4 3.119 3.112 3.129 VV 324473 1984918 1.80% 0.082% 5 3.148 3.129 3.166 PV 4474797 52036102 47.16% 2.160% 6 3.170 3.166 3.194 VV 1501594 11995195 10.87% 0.498% 7 3.228 3.194 3.252 PV 1104616 13897294 12.60% 0.577% 8 3.276 3.252 3.316 VV 646037 12132740 11.00% 0.504% 9 3.361 3.316 3.371 VV 1376284 19705675 17.86% 0.818% 10 3.381 3.371 3.407 VV 1421940 17820159 16.15% 0.740% 11 3.443 3.407 3.471 VV 1676689 32681088 29.62% 1.357% 12 3.500 3.471 3.521 VV 1300274 22872539 20.73% 0.949% 13 3.555 3.521 3.574 VV 803584 17596846 15.95% 0.730% 14 3.593 3.574 3.627 VV 1001915 13293314 12.05% 0.552% 15 3.671 3.627 3.696 PV 1361030 21268772 19.28% 0.883% 16 3.720 3.696 3.755 VV 1413958 20708843 18.77% 0.860% 17 3.783 3.755 3.797 VV 828494 9256971 8.39% 0.384% 18 3.815 3.797 3.831 VV 1177938 13866870 12.57% 0.576% 19 3.848 3.831 3.880 VV 887883 18999842 17.22% 0.789% 20 3.890 3.880 3.903 VV 616711 6780637 6.15% 0.281% 21 3.942 3.903 3.975 VV 1386592 32492846 29.45% 1.349% 22 3.993 3.975 4.006 VV 715807 9405593 8.52% 0.390% 23 4.020 4.006 4.029 VV 852267 9479535 8.59% 0.393% 24 4.069 4.029 4.081 VV 2559426 65788880 59.63% 2.731% 25 4.101 4.081 4.123 VV 9131285 110334312 100.00% 4.580% 26 4.139 4.123 4.159 VV 913318 11853562 10.74% 0.492% 27 4.195 4.159 4.214 VV 1246042 25326996 22.95% 1.051% 28 4.220 4.214 4.244 VV 794393 8758245 7.94% 0.364% 29 4.275 4.244 4.304 VV 1376411 26240172 23.78% 1.089% 30 4.345 4.304 4.375 VV 1441558 42478700 38.50% 1.763% 31 4.394 4.375 4.427 VV 1372410 26515790 24.03% 1.101% 32 4.450 4.427 4.454 PV 935243 7956286 7.21% 0.330% 33 4.469 4.454 4.487 VV 1281139 18877069 17.11% 0.784% 34 4.518 4.487 4.522 VV 1926354 26855174 24.34% 1.115% 35 4.542 4.522 4.557 VV 2574093 45691607 41.41% 1.897% 36 4.571 4.557 4.594 VV 2139719 37649142 34.12% 1.563% 37 4.620 4.594 4.658 VV 1886423 47814780 43.34% 1.985% 38 4.683 4.658 4.699 VV 738615 14126656 12.80% 0.586% 39 4.721 4.699 4.741 VV 1101545 17308563 15.69% 0.718% 40 4.763 4.741 4.779 VV 956244 14407028 13.06% 0.598% 41 4.794 4.779 4.802 VV 752636 8492224 7.70% 0.353% 42 4.821 4.802 4.863 VV 1250901 31521962 28.57% 1.308% 43 4.904 4.863 4.920 VV 1184496 27423648 24.86% 1.138% 44 4.941 4.920 4.992 VV 1479687 39789814 36.06% 1.652% 45 5.028 4.992 5.036 VV 1224347 20635575 18.70% 0.857% 46 5.046 5.036 5.054 VV 1365165 13340736 12.09% 0.554% 47 5.068 5.054 5.104 VV 2051318 43749809 39.65% 1.816% 48 5.112 5.104 5.132 VV 999020 13582111 12.31% 0.564% 49 5.168 5.132 5.203 VV 2408973 50363639 45.65% 2.091% 50 5.247 5.203 5.280 VV 1227269 36360753 32.96% 1.509% 51 5.308 5.280 5.329 VV 836171 19327686 17.52% 0.802% 52 5.347 5.329 5.363 VV 703074 13646489 12.37% 0.566% 53 5.373 5.363 5.386 VV 633615 7831269 7.10% 0.325% 54 5.403 5.386 5.419 VV 962876 15987346 14.49% 0.664% 55 5.437 5.419 5.465 VV 943608 16983403 15.39% 0.705% 56 5.490 5.465 5.510 PV 645137 7717063 6.99% 0.320% 57 5.539 5.510 5.556 VV 933792 17875483 16.20% 0.742% 58 5.573 5.556 5.595 VV 1201754 20248914 18.35% 0.841% 59 5.614 5.595 5.643 VV 2291066 45344509 41.10% 1.882% 60 5.659 5.643 5.696 VV 1111617 27795620 25.19% 1.154% 61 5.714 5.696 5.722 VV 743036 9730221 8.82% 0.404% 62 5.738 5.722 5.782 VV 860342 18958104 17.18% 0.787% 63 5.800 5.782 5.807 VV 468288 4560074 4.13% 0.189% 64 5.821 5.807 5.833 VV 578361 7783266 7.05% 0.323% 65 5.851 5.833 5.874 VV 803211 15556103 14.10% 0.646% 66 5.892 5.874 5.919 VV 721285 15121161 13.70% 0.628% 67 5.955 5.937 5.972 VV 517970 7827188 7.09% 0.325% 68 5.991 5.972 6.007 VV 526242 7840040 7.11% 0.325% 69 6.030 6.007 6.068 VV 931260 24837639 22.51% 1.031% 70 6.081 6.068 6.096 VV 634725 8070558 7.31% 0.335% 71 6.102 6.096 6.108 VV 382611 2790637 2.53% 0.116% 72 6.132 6.108 6.166 VV 1005629 20798597 18.85% 0.863% 73 6.201 6.166 6.224 VV 967449 18042586 16.35% 0.749% 74 6.243 6.224 6.251 VV 422172 4814219 4.36% 0.200% 75 6.267 6.251 6.281 VV 728646 10238550 9.28% 0.425% 76 6.309 6.281 6.344 VV 4330605 72095746 65.34% 2.993% 77 6.362 6.344 6.376 VV 549508 9327459 8.45% 0.387% 78 6.398 6.376 6.427 VV 2606250 36476332 33.06% 1.514% 79 6.468 6.427 6.506 VV 565065 18349782 16.63% 0.762% 80 6.529 6.506 6.553 VV 7847029 84133112 76.25% 3.492% 81 6.592 6.553 6.609 VV 450042 10925168 9.90% 0.453% 82 6.631 6.609 6.659 VV 986769 19279133 17.47% 0.800% 83 6.670 6.659 6.691 VV 438668 7209742 6.53% 0.299% 84 6.706 6.691 6.720 VV 436632 6267915 5.68% 0.260% 85 6.734 6.720 6.747 VV 377716 5408977 4.90% 0.225% 86 6.766 6.747 6.786 VV 430341 8652407 7.84% 0.359% 87 6.809 6.786 6.846 VV 614266 13560375 12.29% 0.563% 88 6.865 6.846 6.887 VV 482605 8444748 7.65% 0.351% 89 6.951 6.887 7.000 VV 2014080 63728433 57.76% 2.645% 90 7.030 7.000 7.067 VV 3165637 62418999 56.57% 2.591% 91 7.073 7.067 7.097 VV 408912 4507547 4.09% 0.187% 92 7.111 7.097 7.118 PV 120113 976659 0.89% 0.041% 93 7.160 7.118 7.180 VV 365111 9519192 8.63% 0.395% 94 7.235 7.180 7.264 VV 377524 15752825 14.28% 0.654% 95 7.286 7.264 7.303 VV 544023 9865425 8.94% 0.410% 96 7.335 7.303 7.361 VV 820971 16252224 14.73% 0.675% 97 7.391 7.361 7.399 VV 457922 7316533 6.63% 0.304% 98 7.416 7.399 7.431 VV 745460 11701388 10.61% 0.486% 99 7.447 7.431 7.482 VV 797733 15875716 14.39% 0.659% 100 7.516 7.482 7.552 VV 893794 22940346 20.79% 0.952% 101 7.575 7.552 7.626 VV 590790 18470358 16.74% 0.767% 102 7.642 7.626 7.661 VV 286225 4804940 4.35% 0.199% 103 7.697 7.661 7.718 VV 375852 7331926 6.65% 0.304% 104 7.785 7.718 7.827 PV 828787 18137582 16.44% 0.753% 105 7.846 7.827 7.867 VV 227204 4679292 4.24% 0.194% 106 7.915 7.867 7.928 VV 393944 10084842 9.14% 0.419% 107 7.935 7.928 7.957 VV 338073 4899360 4.44% 0.203% 108 7.966 7.957 7.984 VV 227740 3217609 2.92% 0.134% 109 8.029 7.984 8.069 VV 878383 21008014 19.04% 0.872% 110 8.095 8.069 8.126 VV 209589 4562599 4.14% 0.189% 111 8.140 8.126 8.154 VV 140639 2142292 1.94% 0.089% 112 8.196 8.154 8.229 VV 250712 7938047 7.19% 0.329% 113 8.298 8.229 8.349 VV 269973 13521730 12.26% 0.561% 114 8.354 8.349 8.363 VV 129785 993997 0.90% 0.041% 115 8.387 8.363 8.398 VV 168181 3116183 2.82% 0.129% 116 8.429 8.398 8.448 VV 308290 6657639 6.03% 0.276% 117 8.470 8.448 8.512 VV 272544 8028665 7.28% 0.333% 118 8.535 8.512 8.549 VV 246087 4264297 3.86% 0.177% 119 8.570 8.549 8.594 VV 256103 5008062 4.54% 0.208% 120 8.689 8.657 8.703 VV 176231 3891297 3.53% 0.162% 121 8.748 8.703 8.765 VV 248468 6833970 6.19% 0.284% 122 8.786 8.765 8.819 VV 243403 4721288 4.28% 0.196% 123 8.911 8.867 8.936 VV 82855 2300316 2.08% 0.095% 124 9.018 8.971 9.042 VV 74567 1707173 1.55% 0.071% 125 9.078 9.042 9.100 PV 38557 575968 0.52% 0.024% 126 9.481 9.402 9.547 BV 3444073 60097996 54.47% 2.495% 127 9.589 9.547 9.689 VV 1491701 34159214 30.96% 1.418% 128 9.752 9.726 9.787 BV 108935 2025716 1.84% 0.084% 129 10.638 10.579 10.687 VV 136007 5326540 4.83% 0.221% 130 10.739 10.687 10.829 VV 281195 10172390 9.22% 0.422% Sum of corrected areas: 2409138282 Signal #2 : ECD2B.CH 1 2.540 2.506 2.558 BV 538657 6954270 4.50% 0.229% 2 2.579 2.558 2.638 PV 3729995 51638019 33.39% 1.700% 3 2.664 2.638 2.708 VV 503663 7547864 4.88% 0.248% 4 2.755 2.708 2.778 PV 678896 12696224 8.21% 0.418% 5 2.825 2.778 2.867 VV 944704 21214469 13.72% 0.698% 6 2.895 2.867 2.915 VV 749643 10552642 6.82% 0.347% 7 2.952 2.915 2.968 VV 615484 12391209 8.01% 0.408% 8 2.982 2.968 3.003 VV 626630 6471199 4.18% 0.213% 9 3.064 3.003 3.104 PV 827340 24557201 15.88% 0.808% 10 3.145 3.104 3.166 PV 547687 10402911 6.73% 0.342% 11 3.172 3.166 3.189 VV 266572 3202429 2.07% 0.105% 12 3.221 3.189 3.262 VV 823593 19506799 12.61% 0.642% 13 3.276 3.262 3.294 VV 487978 7067746 4.57% 0.233% 14 3.347 3.294 3.372 VV 9924718 154644796 100.00% 5.090% 15 3.381 3.372 3.444 VV 3566717 98829370 63.91% 3.253% 16 3.470 3.444 3.507 VV 1599863 45090354 29.16% 1.484% 17 3.530 3.507 3.540 VV 1165018 19732412 12.76% 0.649% 18 3.553 3.540 3.568 VV 1230237 18098602 11.70% 0.596% 19 3.620 3.568 3.647 VV 1813798 66298806 42.87% 2.182% 20 3.655 3.647 3.688 VV 1558126 23890666 15.45% 0.786% 21 3.745 3.688 3.759 VV 2933000 62386073 40.34% 2.053% 22 3.776 3.759 3.798 VV 2906294 59574385 38.52% 1.961% 23 3.815 3.798 3.846 VV 2469384 51941989 33.59% 1.710% 24 3.868 3.846 3.906 VV 2804732 63274052 40.92% 2.082% 25 3.955 3.906 3.980 VV 1381312 39817552 25.75% 1.310% 26 4.013 3.980 4.037 VV 1535258 40179686 25.98% 1.322% 27 4.056 4.037 4.081 VV 1594472 32340713 20.91% 1.064% 28 4.101 4.081 4.127 VV 1546980 30401209 19.66% 1.001% 29 4.197 4.147 4.222 VV 1931796 63285307 40.92% 2.083% 30 4.279 4.222 4.300 VV 2333858 73883781 47.78% 2.432% 31 4.333 4.300 4.361 VV 1536232 45672779 29.53% 1.503% 32 4.376 4.361 4.391 VV 963249 15388096 9.95% 0.506% 33 4.407 4.391 4.416 VV 992337 13309129 8.61% 0.438% 34 4.445 4.416 4.452 VV 1203578 23998347 15.52% 0.790% 35 4.457 4.452 4.483 VV 1203040 17704685 11.45% 0.583% 36 4.518 4.483 4.540 VV 1069959 28104871 18.17% 0.925% 37 4.558 4.540 4.575 VV 1028622 15852373 10.25% 0.522% 38 4.603 4.575 4.632 VV 1229485 25651865 16.59% 0.844% 39 4.655 4.632 4.675 VV 855144 12859123 8.32% 0.423% 40 4.716 4.675 4.723 VV 662859 13098327 8.47% 0.431% 41 4.749 4.723 4.783 VV 2070868 39555178 25.58% 1.302% 42 4.815 4.783 4.874 VV 2811917 91091499 58.90% 2.998% 43 4.890 4.874 4.924 VV 1140516 22839151 14.77% 0.752% 44 4.953 4.924 4.962 VV 917704 14868278 9.61% 0.489% 45 4.985 4.962 5.007 VV 1109641 25131982 16.25% 0.827% 46 5.018 5.007 5.033 VV 650748 8243493 5.33% 0.271% 47 5.053 5.033 5.074 VV 806443 14437004 9.34% 0.475% 48 5.106 5.074 5.119 VV 1120458 22087472 14.28% 0.727% 49 5.145 5.119 5.171 VV 1457146 31841272 20.59% 1.048% 50 5.188 5.171 5.215 VV 591456 12111811 7.83% 0.399% 51 5.240 5.215 5.253 VV 668985 11849612 7.66% 0.390% 52 5.274 5.253 5.301 VV 1530179 27936956 18.07% 0.919% 53 5.339 5.301 5.374 VV 2932510 67656115 43.75% 2.227% 54 5.393 5.374 5.432 VV 1887323 34879505 22.55% 1.148% 55 5.439 5.432 5.447 VV 573001 4770582 3.08% 0.157% 56 5.467 5.447 5.493 VV 3318958 44454055 28.75% 1.463% 57 5.530 5.493 5.563 VV 9900603 133206645 86.14% 4.384% 58 5.587 5.563 5.599 VV 751775 14863828 9.61% 0.489% 59 5.605 5.599 5.629 VV 719749 7669794 4.96% 0.252% 60 5.664 5.629 5.677 PV 398874 7355164 4.76% 0.242% 61 5.684 5.677 5.704 VV 397777 4511293 2.92% 0.148% 62 5.722 5.704 5.740 VV 406701 5304655 3.43% 0.175% 63 5.763 5.740 5.774 VV 330637 5105076 3.30% 0.168% 64 5.797 5.774 5.823 VV 504145 11063115 7.15% 0.364% 65 5.837 5.823 5.852 VV 289745 4634981 3.00% 0.153% 66 5.888 5.852 5.912 VV 438743 12701303 8.21% 0.418% 67 5.934 5.912 5.954 VV 690231 12429035 8.04% 0.409% 68 5.985 5.954 6.036 VV 1069891 31063938 20.09% 1.022% 69 6.061 6.036 6.075 VV 1730934 25425228 16.44% 0.837% 70 6.104 6.075 6.132 VV 2980701 78078121 50.49% 2.570% 71 6.160 6.132 6.227 VV 3715426 126709887 81.94% 4.170% 72 6.254 6.227 6.276 VV 1179246 30032260 19.42% 0.988% 73 6.300 6.276 6.320 VV 1652762 33373757 21.58% 1.098% 74 6.333 6.320 6.344 VV 1236547 17093877 11.05% 0.563% 75 6.357 6.344 6.417 VV 1271533 42209671 27.29% 1.389% 76 6.495 6.417 6.524 VV 1511409 61894167 40.02% 2.037% 77 6.547 6.524 6.569 VV 1659808 34444255 22.27% 1.134% 78 6.593 6.569 6.612 VV 1635932 35685452 23.08% 1.174% 79 6.623 6.612 6.649 VV 1315873 24482659 15.83% 0.806% 80 6.678 6.649 6.732 VV 1234079 44194252 28.58% 1.455% 81 6.756 6.732 6.782 VV 966514 22479415 14.54% 0.740% 82 6.873 6.854 6.895 VV 670778 10993555 7.11% 0.362% 83 6.934 6.895 6.969 VV 685171 21488137 13.90% 0.707% 84 6.994 6.969 7.033 VV 442905 14309699 9.25% 0.471% 85 7.064 7.033 7.087 VV 554817 13740862 8.89% 0.452% 86 7.106 7.087 7.122 VV 441850 8039034 5.20% 0.265% 87 7.147 7.122 7.208 VV 749682 22392328 14.48% 0.737% 88 7.250 7.208 7.284 VV 184749 5454466 3.53% 0.180% 89 7.309 7.284 7.324 VV 125750 2814424 1.82% 0.093% 90 7.353 7.324 7.412 VB 132256 4548036 2.94% 0.150% 91 7.458 7.416 7.486 BV 112984 1748563 1.13% 0.058% 92 7.544 7.486 7.571 VV 174111 4772343 3.09% 0.157% 93 7.591 7.571 7.612 VV 113839 1862871 1.20% 0.061% 94 7.639 7.612 7.670 VV 254516 4376305 2.83% 0.144% 95 7.720 7.670 7.757 PV 118933 3373164 2.18% 0.111% 96 7.818 7.757 7.846 VV 265557 6532242 4.22% 0.215% 97 7.870 7.846 7.896 VV 284305 4150732 2.68% 0.137% 98 7.919 7.896 7.957 VV 98250 1960855 1.27% 0.065% 99 8.016 7.957 8.046 PV 142392 3012515 1.95% 0.099% 100 8.131 8.046 8.167 PV 4090322 58831414 38.04% 1.936% 101 8.249 8.167 8.266 VV 68934 3147850 2.04% 0.104% 102 8.495 8.266 8.542 VV 1350474 29603317 19.14% 0.974% 103 8.613 8.542 8.637 VV 252433 7039000 4.55% 0.232% 104 8.652 8.637 8.682 VB 103403 1810748 1.17% 0.060% 105 8.824 8.694 8.841 BV 324760 7473778 4.83% 0.246% 106 8.859 8.841 8.887 VV 271898 5769296 3.73% 0.190% 107 8.989 8.887 9.009 VV 184840 11697239 7.56% 0.385% 108 9.132 9.009 9.142 VV 269266 14292273 9.24% 0.470% 109 9.245 9.142 9.257 VV 356033 19593492 12.67% 0.645% 110 9.319 9.257 9.391 VV 474593 27036128 17.48% 0.890% 111 9.872 9.391 9.886 VV 102377 41186715 26.63% 1.356% 112 10.026 9.886 10.071 VB 46625 5901035 3.82% 0.194% 113 10.385 10.072 10.447 BB 70116 5685164 3.68% 0.187% 114 10.727 10.567 10.772 BV 123120 5556563 3.59% 0.183% 115 10.845 10.772 10.911 VV 128530 6753937 4.37% 0.222% 116 10.953 10.911 11.003 VB 76621 2193900 1.42% 0.072% Sum of corrected areas: 3038420105