Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042726.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 14:30 Sample : J1399-09RE Misc : ALS Vial : 5 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.057 3.035 3.085 VV 419030 10747143 6.36% 0.303% 2 3.092 3.085 3.130 VV 542591 9363441 5.55% 0.264% 3 3.147 3.130 3.156 PV 782269 7752732 4.59% 0.218% 4 3.168 3.156 3.190 VV 865382 12972144 7.68% 0.365% 5 3.221 3.190 3.246 VV 2002086 29191143 17.29% 0.822% 6 3.265 3.246 3.271 PV 673428 6107124 3.62% 0.172% 7 3.280 3.271 3.297 VV 753663 8085956 4.79% 0.228% 8 3.350 3.322 3.367 VV 1176213 22921505 13.58% 0.646% 9 3.379 3.367 3.400 VV 1112974 17558356 10.40% 0.494% 10 3.440 3.400 3.467 VV 1279539 38704503 22.92% 1.090% 11 3.498 3.467 3.516 VV 1244837 31167971 18.46% 0.878% 12 3.554 3.516 3.571 VV 1298504 37803296 22.39% 1.065% 13 3.587 3.571 3.622 VV 1507549 34032306 20.16% 0.958% 14 3.664 3.622 3.692 VV 1625942 54013217 31.99% 1.521% 15 3.717 3.692 3.755 VV 1694283 46966418 27.82% 1.323% 16 3.778 3.755 3.791 VV 1613941 25463252 15.08% 0.717% 17 3.809 3.791 3.827 VV 1735576 32984680 19.54% 0.929% 18 3.844 3.827 3.875 VV 1719244 46533694 27.56% 1.311% 19 3.885 3.875 3.897 VV 1593282 20010486 11.85% 0.564% 20 3.935 3.897 3.969 VV 1756590 68741222 40.71% 1.936% 21 3.988 3.969 4.001 VV 1696031 30169090 17.87% 0.850% 22 4.013 4.001 4.025 VV 1705193 23878795 14.14% 0.672% 23 4.054 4.025 4.069 VV 1841918 47179165 27.94% 1.329% 24 4.096 4.069 4.118 VV 13310158 168848000 100.00% 4.755% 25 4.130 4.118 4.154 VV 1870481 35293491 20.90% 0.994% 26 4.190 4.154 4.210 VV 1951152 58765929 34.80% 1.655% 27 4.217 4.210 4.237 VV 1872510 26990798 15.99% 0.760% 28 4.271 4.237 4.300 VV 1999377 67748055 40.12% 1.908% 29 4.340 4.300 4.371 VV 1998508 82664747 48.96% 2.328% 30 4.390 4.371 4.422 VV 2170622 62794469 37.19% 1.768% 31 4.458 4.422 4.478 VV 2187611 71485414 42.34% 2.013% 32 4.492 4.478 4.517 VV 2235384 50093217 29.67% 1.411% 33 4.537 4.517 4.550 VV 2368987 45225093 26.78% 1.274% 34 4.563 4.550 4.579 VV 2382577 39032281 23.12% 1.099% 35 4.591 4.579 4.626 VV 2316844 62509971 37.02% 1.760% 36 4.672 4.626 4.692 VV 2290696 86254642 51.08% 2.429% 37 4.716 4.692 4.735 VV 2342332 58811117 34.83% 1.656% 38 4.758 4.735 4.775 VV 2334629 54715404 32.41% 1.541% 39 4.786 4.775 4.795 VV 2344824 27671633 16.39% 0.779% 40 4.812 4.795 4.859 VV 2424478 88736737 52.55% 2.499% 41 4.892 4.859 4.920 VV 2426927 85710579 50.76% 2.414% 42 4.936 4.920 4.969 VV 2648751 53508427 31.69% 1.507% 43 4.990 4.969 4.994 PV 1065140 9902081 5.86% 0.279% 44 5.026 4.994 5.050 VV 2157174 60315193 35.72% 1.699% 45 5.067 5.050 5.093 VV 2201672 56229710 33.30% 1.584% 46 5.113 5.093 5.135 VV 2105775 52414297 31.04% 1.476% 47 5.163 5.135 5.200 VV 3571630 94352310 55.88% 2.657% 48 5.221 5.200 5.229 VV 2011039 33519001 19.85% 0.944% 49 5.238 5.229 5.276 VV 2009312 50620882 29.98% 1.426% 50 5.292 5.276 5.310 VV 1677551 31815651 18.84% 0.896% 51 5.328 5.310 5.341 VV 1624024 28546159 16.91% 0.804% 52 5.367 5.341 5.386 VV 2012755 46334202 27.44% 1.305% 53 5.403 5.386 5.421 VV 1480350 28676897 16.98% 0.808% 54 5.434 5.421 5.461 VV 1398383 30967346 18.34% 0.872% 55 5.488 5.461 5.507 VV 1663285 38935170 23.06% 1.097% 56 5.524 5.507 5.548 VV 1584109 24369250 14.43% 0.686% 57 5.582 5.548 5.592 VV 857030 13487995 7.99% 0.380% 58 5.614 5.592 5.629 VV 1872949 28993832 17.17% 0.817% 59 5.640 5.629 5.654 VV 1624977 19258368 11.41% 0.542% 60 5.679 5.654 5.698 VV 1717153 33843567 20.04% 0.953% 61 5.724 5.698 5.740 VV 1446285 28457571 16.85% 0.801% 62 5.759 5.740 5.776 VV 1429452 28558078 16.91% 0.804% 63 5.789 5.776 5.813 VV 1351611 20065322 11.88% 0.565% 64 5.843 5.813 5.863 PV 1571091 34266932 20.29% 0.965% 65 5.883 5.863 5.915 VV 1641247 45876291 27.17% 1.292% 66 5.947 5.915 5.964 VV 1300056 37139104 22.00% 1.046% 67 5.984 5.964 6.005 VV 1298828 30674373 18.17% 0.864% 68 6.055 6.005 6.068 VV 1753158 53798963 31.86% 1.515% 69 6.074 6.068 6.089 VV 1526145 18470850 10.94% 0.520% 70 6.095 6.089 6.111 VV 1336632 17599687 10.42% 0.496% 71 6.123 6.111 6.164 VV 1287976 37946096 22.47% 1.069% 72 6.198 6.164 6.224 VV 1163350 38767399 22.96% 1.092% 73 6.264 6.224 6.289 VV 1723479 46964021 27.81% 1.323% 74 6.317 6.289 6.343 VV 3324049 59075627 34.99% 1.664% 75 6.351 6.343 6.366 VV 942845 12946299 7.67% 0.365% 76 6.393 6.366 6.434 VV 4326621 75591616 44.77% 2.129% 77 6.524 6.501 6.550 VV 6115297 77796279 46.07% 2.191% 78 6.626 6.587 6.648 VV 1056042 25695062 15.22% 0.724% 79 6.672 6.648 6.699 VV 554062 15648724 9.27% 0.441% 80 6.732 6.699 6.748 VV 516839 14379215 8.52% 0.405% 81 6.779 6.748 6.826 VV 511868 20673503 12.24% 0.582% 82 6.864 6.826 6.886 VV 468693 14123790 8.36% 0.398% 83 6.897 6.886 6.913 VV 360128 5497838 3.26% 0.155% 84 6.955 6.913 6.996 VV 783532 21860743 12.95% 0.616% 85 7.025 6.996 7.055 VV 1419947 23287671 13.79% 0.656% 86 7.071 7.055 7.091 VV 211872 3388166 2.01% 0.095% 87 7.228 7.182 7.245 VV 113677 1352651 0.80% 0.038% 88 7.330 7.269 7.359 BV 334844 5513232 3.27% 0.155% 89 7.385 7.359 7.401 PV 62640 566696 0.34% 0.016% 90 7.515 7.471 7.541 VV 93145 2307272 1.37% 0.065% 91 7.607 7.582 7.641 VV 149744 2491060 1.48% 0.070% 92 7.685 7.641 7.707 VV 78850 1616147 0.96% 0.046% 93 7.781 7.707 7.812 PV 155833 4199979 2.49% 0.118% 94 7.845 7.812 7.874 VV 91758 2515509 1.49% 0.071% 95 7.908 7.874 7.928 VV 174449 3371043 2.00% 0.095% 96 7.964 7.928 7.977 VV 112872 2791086 1.65% 0.079% 97 8.020 7.977 8.072 VV 352779 8189860 4.85% 0.231% 98 8.110 8.072 8.146 PB 71121 2228456 1.32% 0.063% 99 8.188 8.149 8.212 BV 87362 1510691 0.89% 0.043% 100 8.261 8.212 8.277 PV 31956 1076515 0.64% 0.030% 101 8.424 8.309 8.445 BV 106773 925701 0.55% 0.026% 102 8.666 8.504 8.682 BV 65140 3740907 2.22% 0.105% 103 8.741 8.682 8.757 VV 85383 2450353 1.45% 0.069% 104 8.782 8.757 8.814 VV 101193 2457600 1.46% 0.069% 105 9.187 8.814 9.214 VV 117736 18021093 10.67% 0.508% 106 9.474 9.214 9.531 VV 3920367 77093078 45.66% 2.171% 107 9.583 9.531 9.697 VV 827187 19978482 11.83% 0.563% 108 9.737 9.697 9.796 VB 45344 1313998 0.78% 0.037% 109 10.734 10.674 10.829 BB 152772 4773992 2.83% 0.134% Sum of corrected areas: 3550824173 Signal #2 : ECD2B.CH 1 2.546 2.506 2.565 BV 647662 6898041 2.06% 0.152% 2 2.578 2.565 2.588 VV 485261 4782380 1.43% 0.105% 3 2.606 2.588 2.636 VV 881421 16658279 4.97% 0.367% 4 2.667 2.636 2.710 PV 1230044 30783432 9.18% 0.678% 5 2.758 2.710 2.779 VV 1241498 39834442 11.88% 0.877% 6 2.828 2.779 2.869 VV 1535737 64956532 19.36% 1.431% 7 2.898 2.869 2.919 VV 1664583 40893051 12.19% 0.901% 8 2.958 2.919 2.969 VV 1666461 44417972 13.24% 0.978% 9 2.982 2.969 3.006 VV 1676428 27253094 8.12% 0.600% 10 3.026 3.006 3.034 VV 1219896 14986628 4.47% 0.330% 11 3.069 3.034 3.105 VV 1791885 60124152 17.92% 1.324% 12 3.145 3.105 3.163 VV 1684547 44898186 13.38% 0.989% 13 3.176 3.163 3.192 VV 1616228 26754679 7.98% 0.589% 14 3.224 3.192 3.247 VV 1951656 58540007 17.45% 1.290% 15 3.253 3.247 3.264 VV 1807922 18232601 5.44% 0.402% 16 3.278 3.264 3.289 VV 1827375 26574682 7.92% 0.585% 17 3.346 3.289 3.411 VV 15642786 309010959 92.12% 6.807% 18 3.469 3.432 3.503 VV 2330206 86604622 25.82% 1.908% 19 3.547 3.503 3.567 VV 2396228 84935022 25.32% 1.871% 20 3.604 3.567 3.617 VV 2612945 72774047 21.69% 1.603% 21 3.631 3.617 3.689 VV 2701346 110599277 32.97% 2.436% 22 3.703 3.689 3.716 VV 2594173 40368673 12.03% 0.889% 23 3.746 3.716 3.821 VV 2785090 164515253 49.04% 3.624% 24 3.957 3.876 3.973 PV 2423595 105153665 31.35% 2.316% 25 3.982 3.973 3.992 VV 2263301 25454160 7.59% 0.561% 26 4.018 3.992 4.033 VV 2526644 57876936 17.25% 1.275% 27 4.040 4.033 4.093 VV 2372880 75850954 22.61% 1.671% 28 4.104 4.093 4.122 VV 1884896 29449877 8.78% 0.649% 29 4.145 4.122 4.157 VV 1970817 35505259 10.58% 0.782% 30 4.171 4.157 4.191 VV 2071485 36425547 10.86% 0.802% 31 4.209 4.191 4.227 VV 1801956 32852235 9.79% 0.724% 32 4.263 4.227 4.278 VV 2236816 54454201 16.23% 1.200% 33 4.298 4.278 4.338 VV 2387841 59955799 17.87% 1.321% 34 4.371 4.338 4.377 VV 790740 9718058 2.90% 0.214% 35 4.395 4.377 4.425 VV 1793589 29234020 8.72% 0.644% 36 4.447 4.425 4.470 VV 1872653 34534846 10.30% 0.761% 37 4.499 4.470 4.524 VV 2233198 59183577 17.64% 1.304% 38 4.554 4.524 4.576 VV 2280908 47416294 14.14% 1.044% 39 4.608 4.576 4.626 PV 2191769 40980190 12.22% 0.903% 40 4.656 4.626 4.680 VV 2708904 66599665 19.85% 1.467% 41 4.749 4.680 4.780 VV 3625726 139870821 41.70% 3.081% 42 4.815 4.780 4.837 VV 2633887 74672916 22.26% 1.645% 43 4.883 4.837 4.922 VV 2340925 110699991 33.00% 2.439% 44 4.951 4.922 4.964 VV 2147483 50326062 15.00% 1.109% 45 4.984 4.964 5.007 VV 2165245 54584556 16.27% 1.202% 46 5.017 5.007 5.034 VV 1993675 30750265 9.17% 0.677% 47 5.054 5.034 5.074 VV 1882643 43226450 12.89% 0.952% 48 5.106 5.074 5.123 VV 2113217 54657131 16.29% 1.204% 49 5.147 5.123 5.170 VV 2797592 59449559 17.72% 1.310% 50 5.187 5.170 5.216 VV 1779787 45542825 13.58% 1.003% 51 5.236 5.216 5.257 VV 1694881 38866892 11.59% 0.856% 52 5.278 5.257 5.298 VV 1634167 36442838 10.86% 0.803% 53 5.333 5.298 5.372 VV 4920432 132712083 39.56% 2.923% 54 5.391 5.372 5.471 VV 4517679 109561995 32.66% 2.413% 55 5.529 5.471 5.624 VV 7876500 176180609 52.52% 3.881% 56 5.645 5.624 5.669 VV 948582 23402624 6.98% 0.516% 57 5.687 5.669 5.706 VV 1024925 20036203 5.97% 0.441% 58 5.718 5.706 5.764 VV 815536 23277779 6.94% 0.513% 59 5.798 5.764 5.820 VV 758183 20545638 6.12% 0.453% 60 5.835 5.820 5.847 VV 631898 10104682 3.01% 0.223% 61 5.890 5.847 5.913 VV 600078 22619409 6.74% 0.498% 62 5.934 5.913 5.955 VV 760935 15736904 4.69% 0.347% 63 5.979 5.955 5.996 VV 771161 15825846 4.72% 0.349% 64 6.009 5.996 6.031 VV 674179 9864044 2.94% 0.217% 65 6.055 6.031 6.075 VV 1022808 15582876 4.65% 0.343% 66 6.096 6.075 6.134 VV 1029407 23561630 7.02% 0.519% 67 6.156 6.134 6.223 VV 1014015 26695514 7.96% 0.588% 68 6.253 6.223 6.274 VV 347386 7067743 2.11% 0.156% 69 6.298 6.274 6.319 VV 552575 8709600 2.60% 0.192% 70 6.333 6.319 6.384 VV 285532 4655686 1.39% 0.103% 71 6.545 6.524 6.565 BV 127172 1406103 0.42% 0.031% 72 6.588 6.565 6.647 VV 140911 3170605 0.95% 0.070% 73 6.827 6.811 6.858 VV 176340 2676426 0.80% 0.059% 74 6.931 6.887 6.966 PV 100920 2570481 0.77% 0.057% 75 7.064 6.966 7.084 VV 173879 5271755 1.57% 0.116% 76 7.103 7.084 7.122 VV 149890 2725575 0.81% 0.060% 77 7.157 7.122 7.224 VV 247676 7470142 2.23% 0.165% 78 7.356 7.224 7.370 PV 55227 4964836 1.48% 0.109% 79 7.650 7.370 7.671 VV 46309 2324364 0.69% 0.051% 80 7.822 7.671 7.839 PV 59023 1144574 0.34% 0.025% 81 7.869 7.839 7.889 VV 98864 1555679 0.46% 0.034% 82 7.916 7.889 7.940 VV 71254 1057459 0.32% 0.023% 83 8.127 7.940 8.171 VV 4647162 71692441 21.37% 1.579% 84 8.491 8.171 8.534 VV 1107908 83184725 24.80% 1.832% 85 8.602 8.534 8.647 VV 680420 43386344 12.93% 0.956% 86 9.316 8.647 9.371 VV 875434 302217298 90.09% 6.657% 87 10.354 9.371 10.363 VV 396560 335443848 100.00% 7.389% 88 10.830 10.363 10.914 VB 143415 66139301 19.72% 1.457% Sum of corrected areas: 4539674419