Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042728.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 15:00 Sample : J1688-07 Misc : ALS Vial : 11 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.162 3.134 3.182 PV 117829 1552984 0.96% 0.374% 2 3.221 3.199 3.279 VV 1015157 10992064 6.79% 2.650% 3 3.576 3.468 3.603 PV 180286 5053268 3.12% 1.218% 4 3.618 3.603 3.644 VV 112891 2038092 1.26% 0.491% 5 3.649 3.644 3.671 VB 51138 417086 0.26% 0.101% 6 4.097 4.065 4.201 PV 14652425 161944492 100.00% 39.047% 7 4.388 4.343 4.424 BB 198362 2311786 1.43% 0.557% 8 4.934 4.901 4.950 BV 258272 2704412 1.67% 0.652% 9 5.164 5.138 5.198 VV 1256787 14944261 9.23% 3.603% 10 5.222 5.198 5.228 VV 318510 3439089 2.12% 0.829% 11 5.243 5.228 5.281 VV 589599 8846686 5.46% 2.133% 12 5.397 5.380 5.451 VV 239066 3134742 1.94% 0.756% 13 5.529 5.511 5.552 PV 122120 1326396 0.82% 0.320% 14 5.683 5.646 5.706 BV 168417 1908585 1.18% 0.460% 15 5.818 5.787 5.865 PV 179946 3613795 2.23% 0.871% 16 6.047 6.021 6.061 BV 124558 1567785 0.97% 0.378% 17 6.076 6.061 6.095 VV 212130 2558262 1.58% 0.617% 18 6.112 6.095 6.149 VV 224814 3010018 1.86% 0.726% 19 6.263 6.216 6.286 PV 232029 2480988 1.53% 0.598% 20 6.524 6.485 6.573 PV 1099696 13047558 8.06% 3.146% 21 7.023 6.953 7.049 BV 203304 2553441 1.58% 0.616% 22 8.046 7.704 8.051 PV 57255 5604485 3.46% 1.351% 23 8.071 8.051 8.087 VV 51988 1022969 0.63% 0.247% 24 8.119 8.087 8.127 VV 64383 1221868 0.75% 0.295% 25 8.196 8.127 8.209 VV 71775 2851916 1.76% 0.688% 26 8.488 8.209 8.501 VV 122901 18998987 11.73% 4.581% 27 8.637 8.501 8.656 VV 141214 11876812 7.33% 2.864% 28 9.187 8.656 9.221 VV 130156 39198080 24.20% 9.451% 29 9.474 9.221 9.566 VB 4377726 84525981 52.19% 20.380% Sum of corrected areas: 414746888 Signal #2 : ECD2B.CH 1 2.740 2.714 2.789 PV 149772 2613928 1.07% 0.322% 2 3.347 3.317 3.460 PV 19711998 243528824 100.00% 29.967% 3 3.632 3.613 3.669 BV 309450 4054096 1.66% 0.499% 4 3.745 3.723 3.778 BV 119416 2250849 0.92% 0.277% 5 3.824 3.808 3.938 VV 354378 5385397 2.21% 0.663% 6 4.160 4.144 4.173 BV 169879 1957962 0.80% 0.241% 7 4.255 4.233 4.353 VV 1428738 19857806 8.15% 2.444% 8 4.390 4.353 4.451 PV 905017 16164025 6.64% 1.989% 9 4.558 4.523 4.583 PV 358172 4451408 1.83% 0.548% 10 4.602 4.583 4.622 VV 154508 1984818 0.82% 0.244% 11 4.639 4.622 4.657 VV 142195 1554694 0.64% 0.191% 12 4.804 4.786 4.828 VV 280548 4017985 1.65% 0.494% 13 4.943 4.908 4.992 VV 285430 5998934 2.46% 0.738% 14 5.106 5.088 5.126 VV 174241 2342560 0.96% 0.288% 15 5.141 5.126 5.164 VV 303611 3989275 1.64% 0.491% 16 5.178 5.164 5.254 VV 277822 4082401 1.68% 0.502% 17 5.305 5.269 5.328 PV 123279 1560335 0.64% 0.192% 18 5.529 5.473 5.572 BV 1460755 17484346 7.18% 2.152% 19 6.054 6.031 6.166 VV 233726 3325404 1.37% 0.409% 20 7.742 7.589 7.747 BV 14098 872631 0.36% 0.107% 21 7.919 7.747 7.931 PV 30252 475213 0.20% 0.058% 22 7.935 7.931 7.941 VV 20117 53514 0.02% 0.007% 23 8.127 7.941 8.173 PV 5315209 75629943 31.06% 9.307% 24 8.586 8.173 8.599 VV 377206 64868754 26.64% 7.982% 25 8.606 8.599 8.611 VV 381781 2665999 1.09% 0.328% 26 8.758 8.611 8.763 VV 414631 36479865 14.98% 4.489% 27 8.858 8.763 8.869 VV 467651 27427086 11.26% 3.375% 28 9.150 8.869 9.154 VV 451582 76703814 31.50% 9.439% 29 9.175 9.154 9.184 VV 450597 7940884 3.26% 0.977% 30 9.258 9.184 9.263 VV 436811 20745388 8.52% 2.553% 31 9.270 9.263 9.274 VV 448092 2858588 1.17% 0.352% 32 9.280 9.274 9.292 VV 442381 4741734 1.95% 0.583% 33 9.322 9.292 9.327 VV 432653 8856983 3.64% 1.090% 34 9.361 9.327 9.366 VV 412064 9414502 3.87% 1.158% 35 9.439 9.366 9.454 VV 394929 20817789 8.55% 2.562% 36 9.533 9.454 9.539 VV 362822 18342014 7.53% 2.257% 37 9.603 9.539 9.607 VV 328172 13841997 5.68% 1.703% 38 9.654 9.607 9.671 VV 322375 11890479 4.88% 1.463% 39 9.724 9.671 9.806 VV 471666 28615105 11.75% 3.521% 40 9.843 9.806 9.868 VV 249098 8849336 3.63% 1.089% 41 9.913 9.868 9.931 VV 191112 7197443 2.96% 0.886% 42 9.983 9.931 9.989 VV 174739 5827494 2.39% 0.717% 43 10.057 9.989 10.066 VV 131255 6487100 2.66% 0.798% 44 10.110 10.066 10.131 VV 87579 3323500 1.36% 0.409% 45 10.156 10.131 10.164 VV 41353 741476 0.30% 0.091% 46 10.209 10.181 10.216 VV 31285 383442 0.16% 0.047% Sum of corrected areas: 812657121