Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042729.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 15:15 Sample : J1686-01 Misc : ALS Vial : 12 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.161 3.142 3.191 PV 141832 1893191 0.97% 0.433% 2 3.222 3.191 3.268 VV 683545 8358746 4.26% 1.911% 3 3.591 3.487 3.617 PV 234927 6676188 3.40% 1.527% 4 3.640 3.617 3.664 VV 191318 4415445 2.25% 1.010% 5 3.670 3.664 3.699 VV 142249 2383552 1.22% 0.545% 6 3.713 3.699 3.731 VV 94053 1548443 0.79% 0.354% 7 3.736 3.731 3.767 VB 67203 737317 0.38% 0.169% 8 4.097 4.067 4.371 PV 17229846 196097548 100.00% 44.839% 9 4.388 4.371 4.461 PV 203766 2111300 1.08% 0.483% 10 4.934 4.891 4.982 BV 180646 2261826 1.15% 0.517% 11 5.164 5.141 5.206 BV 760052 8108604 4.13% 1.854% 12 5.988 5.967 6.032 PV 111597 1441069 0.73% 0.330% 13 6.620 6.566 6.706 BB 121360 2202056 1.12% 0.504% 14 7.909 7.766 7.936 VV 64482 3802275 1.94% 0.869% 15 7.997 7.936 8.002 VV 54957 1823879 0.93% 0.417% 16 8.355 8.002 8.360 VV 127069 17291962 8.82% 3.954% 17 8.467 8.360 8.483 VV 155745 9912177 5.05% 2.267% 18 8.544 8.483 8.549 VV 129912 4994104 2.55% 1.142% 19 8.554 8.549 8.559 VV 127930 746679 0.38% 0.171% 20 8.591 8.559 8.610 VV 143231 4012679 2.05% 0.918% 21 8.652 8.610 8.682 VV 151084 5946906 3.03% 1.360% 22 8.775 8.682 8.783 VV 159213 8757518 4.47% 2.002% 23 9.188 8.783 9.219 VV 122981 30621030 15.62% 7.002% 24 9.473 9.219 9.571 VV 5791089 111187874 56.70% 25.424% Sum of corrected areas: 437332368 Signal #2 : ECD2B.CH 1 2.546 2.506 2.572 BV 117199 1088234 0.40% 0.133% 2 2.741 2.714 2.775 PV 201893 2883766 1.05% 0.352% 3 3.348 3.297 3.437 PV 22596928 274217094 100.00% 33.473% 4 3.513 3.487 3.536 PV 88849 1100501 0.40% 0.134% 5 3.633 3.592 3.684 BV 343070 4824633 1.76% 0.589% 6 3.825 3.805 3.875 VV 277573 4107626 1.50% 0.501% 7 4.256 4.236 4.351 VV 1001229 16462881 6.00% 2.010% 8 4.387 4.351 4.524 VV 270902 9257261 3.38% 1.130% 9 4.779 4.742 4.792 BV 96405 736477 0.27% 0.090% 10 4.938 4.914 4.980 VV 243559 3659443 1.33% 0.447% 11 7.674 7.454 7.680 PV 18943 787362 0.29% 0.096% 12 7.916 7.680 7.939 PV 52299 661234 0.24% 0.081% 13 8.127 7.939 8.179 PV 7240132 102250976 37.29% 12.482% 14 8.731 8.179 8.737 VV 423100 96225861 35.09% 11.746% 15 8.767 8.737 8.773 VV 421207 8789136 3.21% 1.073% 16 8.804 8.773 8.808 VV 422517 8864397 3.23% 1.082% 17 9.006 8.808 9.018 VV 466750 56743458 20.69% 6.927% 18 9.193 9.018 9.199 VV 470387 49756118 18.14% 6.074% 19 9.219 9.199 9.232 VV 465643 9224007 3.36% 1.126% 20 9.284 9.232 9.289 VV 459990 15155884 5.53% 1.850% 21 9.324 9.289 9.329 VV 455227 10626784 3.88% 1.297% 22 9.413 9.329 9.427 VV 432200 25219118 9.20% 3.078% 23 9.449 9.427 9.455 VV 412756 6689694 2.44% 0.817% 24 9.498 9.455 9.502 VV 381719 10942008 3.99% 1.336% 25 9.516 9.502 9.525 VV 386024 5167306 1.88% 0.631% 26 9.537 9.525 9.549 VV 376676 5242490 1.91% 0.640% 27 9.554 9.549 9.559 VV 361942 2124214 0.77% 0.259% 28 9.581 9.559 9.589 VV 363773 6393142 2.33% 0.780% 29 9.593 9.589 9.598 VV 361796 1846442 0.67% 0.225% 30 9.680 9.598 9.686 VV 336534 17980500 6.56% 2.195% 31 9.733 9.686 9.737 VV 322964 9784703 3.57% 1.194% 32 9.766 9.737 9.770 VV 306745 6039215 2.20% 0.737% 33 9.815 9.770 9.821 VV 270953 8417483 3.07% 1.028% 34 10.029 9.850 10.043 VV 192392 23791485 8.68% 2.904% 35 10.092 10.043 10.108 VV 137102 5479590 2.00% 0.669% 36 10.125 10.108 10.133 VV 106821 1542095 0.56% 0.188% 37 10.138 10.133 10.145 VV 105799 704216 0.26% 0.086% 38 10.192 10.145 10.206 VV 72649 2573414 0.94% 0.314% 39 10.244 10.206 10.268 VV 45605 1440915 0.53% 0.176% 40 10.290 10.268 10.297 VV 30699 410284 0.15% 0.050% Sum of corrected areas: 819211450