Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042731.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 15:45 Sample : J1688-07RE Misc : ALS Vial : 11 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.222 3.185 3.287 PV 943105 10963062 6.29% 2.619% 2 3.584 3.471 3.610 BV 185452 4279168 2.46% 1.022% 3 3.634 3.610 3.654 VV 124838 2473902 1.42% 0.591% 4 3.661 3.654 3.666 VV 51019 336927 0.19% 0.080% 5 3.671 3.666 3.677 VV 48668 220222 0.13% 0.053% 6 3.684 3.677 3.691 VV 26358 118632 0.07% 0.028% 7 4.098 4.048 4.188 PV 15591626 174270493 100.00% 41.630% 8 4.390 4.359 4.424 BV 219883 2647580 1.52% 0.632% 9 4.933 4.913 4.950 PV 218244 2303862 1.32% 0.550% 10 5.165 5.141 5.201 VV 1183350 12533993 7.19% 2.994% 11 5.222 5.201 5.228 VV 259870 2542159 1.46% 0.607% 12 5.243 5.228 5.279 VV 601483 8147371 4.68% 1.946% 13 5.398 5.380 5.446 VV 324044 6004081 3.45% 1.434% 14 5.527 5.509 5.557 VV 241159 4938471 2.83% 1.180% 15 5.684 5.666 5.710 VV 260861 4132300 2.37% 0.987% 16 5.820 5.791 5.871 VV 207429 4023927 2.31% 0.961% 17 6.049 6.009 6.061 BV 133423 1485637 0.85% 0.355% 18 6.075 6.061 6.093 VV 198568 2354036 1.35% 0.562% 19 6.112 6.093 6.154 VB 231393 2988760 1.72% 0.714% 20 6.264 6.228 6.285 BV 257252 2673272 1.53% 0.639% 21 6.525 6.486 6.571 BV 1059105 12822551 7.36% 3.063% 22 6.621 6.595 6.652 PV 118975 1732486 0.99% 0.414% 23 7.023 6.993 7.058 PV 218430 2549506 1.46% 0.609% 24 7.851 7.636 7.856 PV 28748 1071144 0.61% 0.256% 25 7.907 7.856 7.912 VV 52135 1102403 0.63% 0.263% 26 7.917 7.912 7.926 VV 51028 344111 0.20% 0.082% 27 7.933 7.926 7.937 VV 39424 232668 0.13% 0.056% 28 8.098 7.979 8.108 VV 50750 2897425 1.66% 0.692% 29 8.325 8.108 8.332 VV 97689 8344248 4.79% 1.993% 30 8.503 8.332 8.510 VV 113898 10747440 6.17% 2.567% 31 8.593 8.510 8.599 VV 109070 5673343 3.26% 1.355% 32 8.788 8.599 8.850 VV 139260 17549020 10.07% 4.192% 33 9.190 8.850 9.221 VV 109582 21924344 12.58% 5.237% 34 9.474 9.221 9.549 VV 4250308 82188840 47.16% 19.633% Sum of corrected areas: 418617384 Signal #2 : ECD2B.CH 1 2.741 2.711 2.793 VV 149264 2934089 1.22% 0.372% 2 3.348 3.305 3.456 PV 19513702 241410129 100.00% 30.576% 3 3.634 3.579 3.689 BV 319796 4886588 2.02% 0.619% 4 3.825 3.807 3.874 VV 341203 4784168 1.98% 0.606% 5 4.161 4.143 4.221 PV 203617 3970101 1.64% 0.503% 6 4.256 4.221 4.317 VV 1559978 20755785 8.60% 2.629% 7 4.391 4.339 4.449 BV 1062640 21418813 8.87% 2.713% 8 4.559 4.534 4.585 VV 557252 9340723 3.87% 1.183% 9 4.604 4.585 4.626 VV 385382 6997503 2.90% 0.886% 10 4.639 4.626 4.654 VV 407224 5458952 2.26% 0.691% 11 4.779 4.764 4.787 VV 247902 2654570 1.10% 0.336% 12 4.803 4.787 4.827 VV 473500 7896450 3.27% 1.000% 13 4.873 4.859 4.912 VV 272739 5869502 2.43% 0.743% 14 4.944 4.912 4.998 VV 474349 12319836 5.10% 1.560% 15 5.106 5.088 5.126 VV 282365 4416206 1.83% 0.559% 16 5.141 5.126 5.164 VV 443658 6493876 2.69% 0.822% 17 5.178 5.164 5.259 VV 406250 8221549 3.41% 1.041% 18 5.306 5.288 5.329 VV 231682 3979251 1.65% 0.504% 19 5.346 5.329 5.374 VV 273003 5087406 2.11% 0.644% 20 5.529 5.491 5.574 PV 1733847 22417006 9.29% 2.839% 21 6.056 6.034 6.109 PV 262365 3347444 1.39% 0.424% 22 7.650 7.557 7.666 PB 30985 857686 0.36% 0.109% 23 7.919 7.718 7.938 VV 46477 1825194 0.76% 0.231% 24 8.127 7.938 8.172 PV 5381591 75357429 31.22% 9.544% 25 8.177 8.172 8.189 VV 113519 994166 0.41% 0.126% 26 8.913 8.189 8.919 VV 393296 123357979 51.10% 15.624% 27 8.937 8.919 8.943 VV 394405 5501920 2.28% 0.697% 28 8.949 8.943 8.955 VV 385200 2768810 1.15% 0.351% 29 9.006 8.955 9.013 VV 386763 12985920 5.38% 1.645% 30 9.020 9.013 9.024 VV 390509 2656345 1.10% 0.336% 31 9.174 9.024 9.179 VV 387746 34812131 14.42% 4.409% 32 9.229 9.179 9.238 VV 380062 12932095 5.36% 1.638% 33 9.244 9.238 9.251 VV 381823 3018755 1.25% 0.382% 34 9.276 9.251 9.289 VV 379028 8274364 3.43% 1.048% 35 9.319 9.289 9.328 VV 360379 8192094 3.39% 1.038% 36 9.391 9.328 9.396 VV 331705 13492333 5.59% 1.709% 37 9.420 9.396 9.424 VV 315101 5411770 2.24% 0.685% 38 9.475 9.424 9.481 VV 284739 9804047 4.06% 1.242% 39 9.558 9.481 9.573 VV 293920 14740437 6.11% 1.867% 40 9.725 9.573 9.767 VV 369265 29743791 12.32% 3.767% 41 9.772 9.767 9.796 VV 235805 3638184 1.51% 0.461% 42 9.801 9.796 9.822 VV 193273 2649574 1.10% 0.336% 43 9.856 9.822 9.867 VV 143762 3724974 1.54% 0.472% 44 9.913 9.867 9.919 VV 112956 3427487 1.42% 0.434% 45 9.973 9.919 9.983 VV 76177 3112776 1.29% 0.394% 46 9.992 9.983 10.014 VV 73595 978731 0.41% 0.124% 47 10.047 10.014 10.052 VV 29707 626840 0.26% 0.079% Sum of corrected areas: 789545777