Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042732.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 16:00 Sample : J1712-01 Misc : ALS Vial : 12 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.166 3.119 3.201 BV 206260 4376590 3.59% 1.400% 2 3.222 3.201 3.252 PV 1754498 18611563 15.28% 5.954% 3 3.376 3.352 3.390 PV 219918 3448481 2.83% 1.103% 4 3.576 3.547 3.593 VV 386919 6986591 5.74% 2.235% 5 3.614 3.593 3.676 VV 378368 13316965 10.94% 4.260% 6 3.696 3.676 3.729 VV 355238 7630030 6.27% 2.441% 7 3.759 3.729 3.787 PV 236432 5321916 4.37% 1.703% 8 3.799 3.787 3.806 VV 229037 2332787 1.92% 0.746% 9 3.828 3.806 3.847 VV 264758 5668700 4.65% 1.813% 10 4.098 4.045 4.193 PV 11163104 121782555 100.00% 38.959% 11 4.391 4.375 4.409 PV 170117 1950805 1.60% 0.624% 12 4.537 4.508 4.555 PV 253379 3033666 2.49% 0.970% 13 4.934 4.898 4.951 PV 257030 3277193 2.69% 1.048% 14 5.165 5.134 5.188 PV 779937 8519688 7.00% 2.726% 15 5.244 5.229 5.278 VV 106632 1291154 1.06% 0.413% 16 5.489 5.416 5.508 PV 88761 1758350 1.44% 0.563% 17 5.530 5.508 5.548 PV 78842 722232 0.59% 0.231% 18 5.683 5.656 5.704 BV 96493 1217524 1.00% 0.389% 19 5.821 5.789 5.831 PV 37349 437900 0.36% 0.140% 20 6.049 5.999 6.065 PV 98561 869553 0.71% 0.278% 21 6.263 6.234 6.283 PV 146130 1588176 1.30% 0.508% 22 6.528 6.478 6.561 VV 79407 1564944 1.29% 0.501% 23 6.621 6.600 6.648 VV 189225 2193119 1.80% 0.702% 24 6.781 6.762 6.808 PV 115105 1368826 1.12% 0.438% 25 6.898 6.872 6.938 PV 87011 1261639 1.04% 0.404% 26 7.030 6.986 7.053 BV 104894 1475465 1.21% 0.472% 27 7.310 7.278 7.330 PV 128208 1580462 1.30% 0.506% 28 7.838 7.759 7.863 PV 38101 1051900 0.86% 0.337% 29 7.907 7.863 7.929 PV 142930 2085166 1.71% 0.667% 30 7.951 7.929 7.979 VV 40276 797949 0.66% 0.255% 31 8.012 7.979 8.021 VV 17491 310061 0.25% 0.099% 32 8.115 8.021 8.149 VB 34449 1338529 1.10% 0.428% 33 8.567 8.476 8.572 VV 24682 572199 0.47% 0.183% 34 8.603 8.572 8.620 VV 28813 547467 0.45% 0.175% 35 8.713 8.620 8.717 VV 18332 1025205 0.84% 0.328% 36 8.833 8.717 8.852 VB 40987 1707297 1.40% 0.546% 37 9.189 8.879 9.211 BV 58158 4915836 4.04% 1.573% 38 9.474 9.211 9.546 VV 4054533 74652472 61.30% 23.882% Sum of corrected areas: 312590955 Signal #2 : ECD2B.CH 1 2.589 2.569 2.639 PV 211597 7074279 5.23% 0.917% 2 2.832 2.812 2.883 PV 272531 8311394 6.14% 1.078% 3 2.959 2.933 3.011 PV 191166 5872260 4.34% 0.762% 4 3.348 3.322 3.451 VV 10895517 135264243 100.00% 17.542% 5 3.634 3.615 3.693 VV 189319 2786196 2.06% 0.361% 6 3.744 3.725 3.767 VV 217874 2554021 1.89% 0.331% 7 3.825 3.803 3.864 VV 181500 2419651 1.79% 0.314% 8 4.162 4.119 4.198 PV 101161 2597831 1.92% 0.337% 9 4.256 4.229 4.302 VV 811432 10765127 7.96% 1.396% 10 4.388 4.350 4.409 VV 171726 3464226 2.56% 0.449% 11 4.442 4.409 4.464 VV 95064 2269850 1.68% 0.294% 12 4.558 4.493 4.584 PV 86865 2082249 1.54% 0.270% 13 4.605 4.584 4.621 VV 114314 1536031 1.14% 0.199% 14 4.640 4.621 4.689 VB 111185 2161438 1.60% 0.280% 15 4.805 4.786 4.836 VV 129292 2575687 1.90% 0.334% 16 4.873 4.836 4.901 PV 102606 2301230 1.70% 0.298% 17 4.944 4.901 4.969 VV 134745 3350309 2.48% 0.434% 18 5.013 4.991 5.064 VV 95136 2536322 1.88% 0.329% 19 5.106 5.064 5.119 VV 115981 2276526 1.68% 0.295% 20 5.141 5.119 5.162 VV 264532 3872137 2.86% 0.502% 21 5.178 5.162 5.196 VV 143100 1738463 1.29% 0.225% 22 5.285 5.264 5.306 PV 114105 1543837 1.14% 0.200% 23 5.349 5.306 5.374 VV 88883 2487008 1.84% 0.323% 24 5.389 5.374 5.426 VB 53516 916460 0.68% 0.119% 25 5.531 5.511 5.557 VV 114633 2044518 1.51% 0.265% 26 5.672 5.649 5.705 VV 252892 5303610 3.92% 0.688% 27 5.798 5.772 5.863 VV 215578 7126470 5.27% 0.924% 28 5.980 5.944 6.033 VV 258650 6118351 4.52% 0.793% 29 6.127 6.085 6.168 VV 161943 3413763 2.52% 0.443% 30 6.299 6.271 6.319 PV 145999 1677773 1.24% 0.218% 31 6.829 6.809 6.860 VV 151785 1959554 1.45% 0.254% 32 7.165 7.131 7.203 VV 105843 1593988 1.18% 0.207% 33 7.653 7.601 7.677 PV 37181 554204 0.41% 0.072% 34 7.919 7.687 7.946 PV 60409 1501001 1.11% 0.195% 35 7.982 7.946 7.989 VV 19216 174281 0.13% 0.023% 36 8.128 7.989 8.176 PV 5368187 76515065 56.57% 9.923% 37 8.680 8.176 8.685 VV 430551 87012971 64.33% 11.285% 38 8.817 8.685 8.824 VV 465317 37094670 27.42% 4.811% 39 9.241 8.824 9.246 VV 508294 121520184 89.84% 15.760% 40 9.278 9.246 9.282 VV 497623 10621295 7.85% 1.377% 41 9.293 9.282 9.304 VV 507071 6491394 4.80% 0.842% 42 9.310 9.304 9.314 VV 492163 2935544 2.17% 0.381% 43 9.327 9.314 9.333 VV 493390 5308892 3.92% 0.688% 44 9.355 9.333 9.359 VV 474405 7423200 5.49% 0.963% 45 9.426 9.359 9.444 VV 464370 23362912 17.27% 3.030% 46 9.459 9.444 9.473 VV 449704 7503595 5.55% 0.973% 47 9.493 9.473 9.497 VV 426887 6211370 4.59% 0.806% 48 9.621 9.497 9.628 VV 407744 31503342 23.29% 4.086% 49 9.731 9.628 9.759 VV 480217 32131653 23.75% 4.167% 50 9.765 9.759 9.770 VV 397049 2460318 1.82% 0.319% 51 9.773 9.770 9.803 VV 381684 7043135 5.21% 0.913% 52 9.806 9.803 9.815 VV 355566 2552116 1.89% 0.331% 53 9.966 9.815 9.971 VV 274596 27994707 20.70% 3.631% 54 10.026 9.971 10.038 VV 252087 9885316 7.31% 1.282% 55 10.073 10.038 10.099 VV 211812 7596635 5.62% 0.985% 56 10.117 10.099 10.123 VV 177392 2416467 1.79% 0.313% 57 10.138 10.123 10.152 VV 167973 2730464 2.02% 0.354% 58 10.268 10.196 10.280 VV 95001 4964267 3.67% 0.644% 59 10.334 10.280 10.348 VV 64008 2659184 1.97% 0.345% 60 10.378 10.348 10.393 VV 39417 920412 0.68% 0.119% Sum of corrected areas: 771083394