Area Percent Report Data Path : C:\MSDCHEM\1\DATA\PO030218\ Data File : PO042734.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 01 Mar 2018 17:47 Sample : AR1660CCC500 Misc : ALS Vial : 3 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Method : C:\MSDCHEM\1\METHODS\PCB.M Title : Signal #1 : ECD1A.CH peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total --- ----- ----- ---- --- ------- ------- ------ ------ 1 3.164 3.131 3.183 BV 224811 2589880 0.57% 0.039% 2 3.226 3.205 3.246 VV 376509 4408681 0.97% 0.066% 3 3.301 3.246 3.323 VV 229826 6877822 1.51% 0.103% 4 3.329 3.323 3.351 VV 107810 1496456 0.33% 0.022% 5 3.390 3.351 3.413 VV 113493 3070917 0.67% 0.046% 6 3.418 3.413 3.453 VB 76928 1104795 0.24% 0.017% 7 3.592 3.570 3.623 VV 199886 5000371 1.10% 0.075% 8 3.814 3.749 3.931 VV 420602 31971223 7.02% 0.479% 9 4.101 4.062 4.183 VV 41039082 455608800 100.00% 6.822% 10 4.299 4.261 4.338 VV 1040059 19575930 4.30% 0.293% 11 4.386 4.352 4.421 VV 1846642 27527863 6.04% 0.412% 12 4.459 4.421 4.556 VV 7173210 95187229 20.89% 1.425% 13 4.604 4.556 4.630 VV 1214665 19713271 4.33% 0.295% 14 4.782 4.753 4.798 VV 10394381 115126763 25.27% 1.724% 15 4.810 4.798 4.846 VV 5794821 71731259 15.74% 1.074% 16 4.868 4.846 4.884 VV 1488474 20421938 4.48% 0.306% 17 4.896 4.884 4.906 VV 826436 9098953 2.00% 0.136% 18 4.919 4.906 4.942 VV 1156505 17153145 3.76% 0.257% 19 4.968 4.942 5.028 VV 10639687 134809377 29.59% 2.019% 20 5.075 5.051 5.099 VV 715267 15597036 3.42% 0.234% 21 5.131 5.099 5.146 VV 3436575 45043871 9.89% 0.675% 22 5.158 5.146 5.197 VV 2470576 39288590 8.62% 0.588% 23 5.227 5.197 5.235 VV 15407945 169353155 37.17% 2.536% 24 5.247 5.235 5.284 VV 20179223 261168560 57.32% 3.911% 25 5.307 5.284 5.375 VV 12158723 176152385 38.66% 2.638% 26 5.402 5.375 5.446 VV 10978716 145422003 31.92% 2.178% 27 5.466 5.446 5.472 VV 1376615 15535653 3.41% 0.233% 28 5.492 5.472 5.515 VV 7902061 103875919 22.80% 1.555% 29 5.535 5.515 5.562 VV 7148132 116822401 25.64% 1.749% 30 5.572 5.562 5.629 VV 3760321 54650142 11.99% 0.818% 31 5.689 5.661 5.712 VV 9360375 124691986 27.37% 1.867% 32 5.727 5.712 5.751 VV 4324915 57618210 12.65% 0.863% 33 5.772 5.751 5.794 VV 3513261 43644447 9.58% 0.654% 34 5.825 5.794 5.866 VV 8232286 136775044 30.02% 2.048% 35 5.889 5.866 5.915 VV 2927415 40951934 8.99% 0.613% 36 5.942 5.915 5.963 VV 746178 16060289 3.53% 0.240% 37 6.006 5.963 6.012 VV 855365 16508556 3.62% 0.247% 38 6.055 6.012 6.071 VV 8840109 130875949 28.73% 1.960% 39 6.079 6.071 6.100 VV 4171621 51319265 11.26% 0.768% 40 6.117 6.100 6.184 VV 3142275 53902831 11.83% 0.807% 41 6.205 6.184 6.230 VV 1016437 13645993 3.00% 0.204% 42 6.268 6.230 6.296 VV 7596503 93330585 20.48% 1.398% 43 6.306 6.296 6.402 VV 490762 11692104 2.57% 0.175% 44 6.469 6.447 6.513 VV 267673 3578587 0.79% 0.054% 45 6.541 6.513 6.552 PV 1263105 13808457 3.03% 0.207% 46 6.569 6.552 6.600 VV 3022796 36642550 8.04% 0.549% 47 6.625 6.600 6.656 VV 3573127 42856870 9.41% 0.642% 48 6.683 6.656 6.720 VV 8731286 137545842 30.19% 2.060% 49 6.733 6.720 6.757 VV 2397647 28316752 6.22% 0.424% 50 6.786 6.757 6.874 VV 16773384 205328689 45.07% 3.075% 51 6.903 6.874 6.934 PV 2402413 29878455 6.56% 0.447% 52 6.970 6.934 7.007 VV 3160719 40477086 8.88% 0.606% 53 7.037 7.007 7.061 VV 21329029 256525362 56.30% 3.841% 54 7.078 7.061 7.098 VV 5794637 68124061 14.95% 1.020% 55 7.118 7.098 7.140 VV 5019783 59162123 12.99% 0.886% 56 7.163 7.140 7.183 VV 9176785 111494178 24.47% 1.670% 57 7.193 7.183 7.232 VV 1938905 23671024 5.20% 0.354% 58 7.269 7.232 7.284 VV 1938268 30813967 6.76% 0.461% 59 7.313 7.284 7.336 VV 20997746 288937431 63.42% 4.327% 60 7.344 7.336 7.366 VV 2942821 37718772 8.28% 0.565% 61 7.391 7.366 7.421 VV 16694352 204303285 44.84% 3.059% 62 7.447 7.421 7.496 VV 8524630 103079822 22.62% 1.544% 63 7.576 7.519 7.587 BV 3176418 36282493 7.96% 0.543% 64 7.611 7.587 7.659 VV 14035798 199583997 43.81% 2.989% 65 7.688 7.659 7.722 VV 7534374 99451140 21.83% 1.489% 66 7.740 7.722 7.773 VV 3692614 45050324 9.89% 0.675% 67 7.797 7.773 7.815 VV 679112 7940255 1.74% 0.119% 68 7.840 7.815 7.871 VV 4117703 51996297 11.41% 0.779% 69 7.912 7.871 7.941 VV 36587708 440992910 96.79% 6.604% 70 7.958 7.941 7.983 VV 1939822 25365563 5.57% 0.380% 71 8.000 7.983 8.049 VV 290487 6048864 1.33% 0.091% 72 8.197 8.149 8.225 BV 15140877 258948654 56.84% 3.878% 73 8.253 8.225 8.262 VV 6046546 96969948 21.28% 1.452% 74 8.267 8.262 8.336 VV 6027651 66201870 14.53% 0.991% 75 8.469 8.443 8.509 VV 450636 6263818 1.37% 0.094% 76 8.548 8.509 8.577 PV 440464 8965991 1.97% 0.134% 77 8.604 8.577 8.642 VV 3369596 47310993 10.38% 0.708% 78 8.840 8.802 8.883 PV 7866151 117717476 25.84% 1.763% 79 8.917 8.883 8.956 VV 408729 6952375 1.53% 0.104% 80 8.976 8.956 8.981 VV 20527 235487 0.05% 0.004% 81 9.194 9.018 9.235 BV 1889061 31595388 6.93% 0.473% 82 9.309 9.235 9.316 VV 153026 6856097 1.50% 0.103% 83 9.318 9.316 9.326 VV 148739 795889 0.17% 0.012% 84 9.334 9.326 9.374 VV 142374 3031596 0.67% 0.045% 85 9.425 9.374 9.433 VV 223051 5574215 1.22% 0.083% 86 9.481 9.433 9.586 VV 21243438 374941264 82.29% 5.614% 87 11.716 11.603 11.724 VV 332874 16524335 3.63% 0.247% 88 11.758 11.724 11.864 VV 327876 17832250 3.91% 0.267% Sum of corrected areas: 6678094382 Signal #2 : ECD2B.CH 1 2.540 2.506 2.563 BV 218332 2228112 0.32% 0.020% 2 2.676 2.654 2.688 BV 86185 874629 0.13% 0.008% 3 2.905 2.794 2.912 VV 122222 4349195 0.63% 0.039% 4 2.932 2.912 2.936 VV 152196 1861974 0.27% 0.017% 5 2.944 2.936 2.982 VV 157935 2289354 0.33% 0.020% 6 3.345 3.311 3.474 PV 51237620 625355492 90.32% 5.595% 7 3.547 3.528 3.593 BV 1475831 17709461 2.56% 0.158% 8 3.630 3.593 3.676 VV 2400597 31001196 4.48% 0.277% 9 3.701 3.676 3.770 VV 8841151 115147697 16.63% 1.030% 10 3.789 3.770 3.824 VV 315209 7136090 1.03% 0.064% 11 3.857 3.824 3.921 VV 1354484 24411885 3.53% 0.218% 12 3.984 3.939 4.039 VV 12853762 250133087 36.13% 2.238% 13 4.059 4.039 4.079 VV 1839193 26179208 3.78% 0.234% 14 4.091 4.079 4.109 VV 971045 13222071 1.91% 0.118% 15 4.127 4.109 4.139 VV 1364228 17370392 2.51% 0.155% 16 4.165 4.139 4.200 VV 11602860 175013457 25.28% 1.566% 17 4.211 4.200 4.239 VV 848188 14986184 2.16% 0.134% 18 4.277 4.239 4.290 VV 4491338 63372437 9.15% 0.567% 19 4.300 4.290 4.347 VV 3158773 49505293 7.15% 0.443% 20 4.390 4.347 4.426 VV 29371564 593720095 85.75% 5.312% 21 4.445 4.426 4.526 VV 14415342 250792229 36.22% 2.244% 22 4.559 4.526 4.583 VV 14771659 197774626 28.57% 1.769% 23 4.601 4.583 4.621 VV 11670422 151190426 21.84% 1.353% 24 4.640 4.621 4.658 VV 13156273 183912633 26.56% 1.645% 25 4.668 4.658 4.728 VV 5781752 94071221 13.59% 0.842% 26 4.805 4.766 4.827 VV 14409350 204986651 29.61% 1.834% 27 4.841 4.827 4.858 VV 6692483 87828281 12.69% 0.786% 28 4.873 4.858 4.902 VV 5782177 86834924 12.54% 0.777% 29 4.945 4.902 4.981 VV 12600999 241600270 34.90% 2.161% 30 5.014 4.981 5.048 VV 4668516 92668166 13.38% 0.829% 31 5.073 5.048 5.088 VV 1561259 31569841 4.56% 0.282% 32 5.108 5.088 5.122 VV 4150572 55247234 7.98% 0.494% 33 5.141 5.122 5.166 VV 14993579 201836395 29.15% 1.806% 34 5.180 5.166 5.202 VV 4499726 66866968 9.66% 0.598% 35 5.209 5.202 5.216 VV 1787921 14763852 2.13% 0.132% 36 5.231 5.216 5.258 VV 2446209 45068283 6.51% 0.403% 37 5.285 5.258 5.321 VV 11338168 170198159 24.58% 1.523% 38 5.348 5.321 5.354 VV 1653894 29042008 4.19% 0.260% 39 5.369 5.354 5.403 VV 2005151 49219401 7.11% 0.440% 40 5.427 5.403 5.490 VV 1819287 74271603 10.73% 0.664% 41 5.508 5.490 5.562 VV 1276809 43236429 6.24% 0.387% 42 5.586 5.562 5.622 VV 2786989 56067528 8.10% 0.502% 43 5.649 5.622 5.659 VV 5339116 69810674 10.08% 0.625% 44 5.685 5.659 5.707 VV 16176757 262885936 37.97% 2.352% 45 5.724 5.707 5.769 VV 6084613 125611854 18.14% 1.124% 46 5.798 5.769 5.843 VV 26885301 362096103 52.30% 3.239% 47 5.857 5.843 5.878 VV 1042007 18304411 2.64% 0.164% 48 5.897 5.878 5.908 VV 2196997 27782445 4.01% 0.249% 49 5.926 5.908 5.956 VV 5394179 77722809 11.23% 0.695% 50 5.984 5.956 6.093 VV 34231364 472532680 68.25% 4.227% 51 6.129 6.093 6.180 VV 27627740 382055131 55.18% 3.418% 52 6.202 6.180 6.225 VV 3341418 48917100 7.07% 0.438% 53 6.248 6.225 6.273 VV 7877497 108068753 15.61% 0.967% 54 6.300 6.273 6.319 VV 29006895 409329342 59.12% 3.662% 55 6.336 6.319 6.367 VV 26385931 372155431 53.75% 3.329% 56 6.389 6.367 6.498 VV 12801612 192546337 27.81% 1.723% 57 6.524 6.498 6.559 VV 4536753 69732137 10.07% 0.624% 58 6.588 6.559 6.614 VV 20036582 266788871 38.53% 2.387% 59 6.625 6.614 6.647 VV 2422727 31643876 4.57% 0.283% 60 6.681 6.647 6.709 VV 10293982 150743822 21.77% 1.349% 61 6.729 6.709 6.745 VV 5095859 67481358 9.75% 0.604% 62 6.758 6.745 6.791 VV 4171892 63829116 9.22% 0.571% 63 6.831 6.791 6.871 VV 51340444 692357317 100.00% 6.194% 64 6.883 6.871 6.908 VV 1339728 20554881 2.97% 0.184% 65 6.929 6.908 6.989 VV 1919009 35110180 5.07% 0.314% 66 7.102 7.041 7.138 PV 11014778 158573856 22.90% 1.419% 67 7.166 7.138 7.291 VV 29811288 454139539 65.59% 4.063% 68 7.319 7.291 7.334 VV 257562 6277268 0.91% 0.056% 69 7.361 7.334 7.403 VV 812219 18453873 2.67% 0.165% 70 7.423 7.403 7.439 VV 784271 12012633 1.74% 0.107% 71 7.451 7.439 7.486 VV 643808 11452989 1.65% 0.102% 72 7.522 7.486 7.588 VV 4705260 71029485 10.26% 0.635% 73 7.656 7.611 7.688 VV 10885420 146806823 21.20% 1.313% 74 7.700 7.688 7.759 VV 768405 14534960 2.10% 0.130% 75 7.918 7.844 7.965 PV 2423041 32526317 4.70% 0.291% 76 8.130 7.965 8.214 PV 31227271 407521635 58.86% 3.646% 77 8.558 8.428 8.562 BV 152946 6786340 0.98% 0.061% 78 8.640 8.562 8.646 VV 259438 10350051 1.49% 0.093% 79 8.658 8.646 8.663 VV 258453 2461311 0.36% 0.022% 80 8.695 8.663 8.699 VV 314037 6085717 0.88% 0.054% 81 8.952 8.699 8.957 VV 495260 58676314 8.47% 0.525% 82 8.991 8.957 9.008 VV 511856 14821082 2.14% 0.133% 83 9.045 9.008 9.050 VV 526417 12895690 1.86% 0.115% 84 9.334 9.050 9.339 VV 665082 103250766 14.91% 0.924% 85 9.437 9.339 9.442 VV 680903 40824062 5.90% 0.365% 86 9.451 9.442 9.458 VV 682906 6400288 0.92% 0.057% 87 9.540 9.458 9.546 VV 719441 36910332 5.33% 0.330% 88 9.568 9.546 9.573 VV 735575 11725879 1.69% 0.105% 89 9.653 9.573 9.659 VV 756448 37482499 5.41% 0.335% 90 9.674 9.659 9.686 VV 745943 11728068 1.69% 0.105% 91 9.694 9.686 9.704 VV 750794 8012326 1.16% 0.072% 92 9.710 9.704 9.714 VV 751785 4243327 0.61% 0.038% 93 9.739 9.714 9.746 VV 749756 14332739 2.07% 0.128% 94 9.765 9.746 9.770 VV 764814 10716639 1.55% 0.096% 95 9.994 9.770 10.001 VV 779280 105795999 15.28% 0.946% 96 10.006 10.001 10.016 VV 790103 7171782 1.04% 0.064% 97 10.028 10.016 10.045 VV 777474 13166976 1.90% 0.118% 98 10.065 10.045 10.074 VV 778835 13455047 1.94% 0.120% 99 10.128 10.074 10.151 VV 767914 34805031 5.03% 0.311% 100 10.572 10.151 10.584 VV 697502 187774185 27.12% 1.680% 101 10.826 10.584 10.843 VV 565970 94180316 13.60% 0.843% 102 10.853 10.843 10.872 VV 563126 9416666 1.36% 0.084% 103 10.889 10.872 10.922 VV 539539 15873443 2.29% 0.142% 104 10.978 10.922 10.991 VV 527855 21436206 3.10% 0.192% 105 11.002 10.991 11.009 VV 497428 5309962 0.77% 0.048% 106 11.120 11.009 11.172 VV 454333 44026698 6.36% 0.394% 107 11.193 11.172 11.202 VV 416283 7384477 1.07% 0.066% 108 11.533 11.202 11.595 VV 261448 74500820 10.76% 0.667% 109 11.681 11.595 11.712 VV 161684 11561574 1.67% 0.103% 110 11.893 11.712 11.902 VV 24561 7927554 1.15% 0.071% Sum of corrected areas: 11177794544