Quantitation Report (Not Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP020618\ Data File : PP023460.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 05 Feb 2018 19:20 Operator : UA/AJ Sample : HEXANE Misc : ALS Vial : 1 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 06 02:26:54 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 0.000 11.373 0 3800772 N.D. 6.268 # Target Compounds 2) T 3,5-DICHL... 0.000 9.491 0 2834624 N.D. 3.398 # 3) T 4-Nitroph... 0.000 10.536 0 2919338 N.D. 6.290 # 5) T DICAMBA 11.900 11.668 9771435 6486078 4.544 2.856 # 8) T DICHLORPROP 0.000 12.780 0 3234742 N.D. 5.510 # 9) T 2,4-D 13.448 13.268 7954229 5381848 11.880 7.010 # 10) T Pentachlo... 13.830 13.824 15592884 20017059 1.918 2.325 11) T 2,4,5-TP ... 14.700 14.422 12728090 15783071 3.843 4.412 12) T 2,4,5-T 15.101 15.055 16714156 26035893 5.350 8.452 # 13) T 2,4-DB 0.000 15.651 0 2576106 N.D. 5.959 # 14) T DINOSEB 17.312 16.049 10726645 13650527 4.674 5.549 15) T Picloram 17.128 17.396 33006239 34393385 6.779 6.905 16) T DCPA 17.681 17.271 15557138 20248088 3.968 4.654 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.