Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP020618\ Data File : PP023466.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 05 Feb 2018 21:46 Operator : UA/AJ Sample : HSTDICC1500 Misc : ALS Vial : 15 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 06 02:12:32 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 01:18:47 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.589 11.369 706.0E6 836.7E6 1363.271 1371.628 Target Compounds 1) T Dalapon 3.012 2.575 1044.3E6 1071.2E6 1270.749 1267.898 2) T 3,5-DICHL... 9.994 9.485 999.5E6 1039.3E6 1268.829 1273.807 3) T 4-Nitroph... 11.169 10.528 443.2E6 475.4E6 1264.887 1276.525 5) T DICAMBA 11.908 11.666 2819.9E6 2970.2E6 1266.410 1269.977 6) T MCPP 12.250 11.878 191.6E6 199.9E6 134.191 134.493m 7) T MCPA 12.507 12.273 281.5E6 292.0E6 131.002 131.472 8) T DICHLORPROP 13.092 12.778 698.9E6 774.3E6 1301.725 1326.003 9) T 2,4-D 13.453 13.264 874.9E6 994.7E6 1286.916 1284.480 10) T Pentachlo... 13.838 13.823 9800.6E6 10278.8E6 1174.811 1175.833 11) T 2,4,5-TP ... 14.706 14.421 4275.9E6 4557.4E6 1241.976 1241.565 12) T 2,4,5-T 15.106 15.053 4052.7E6 3902.0E6 1246.664 1248.803 13) T 2,4-DB 15.853 15.648 528.7E6 573.2E6 1308.742 1313.149 14) T DINOSEB 17.319 16.048 3008.1E6 3169.8E6 1261.088 1257.399 15) T Picloram 17.132 17.395 6260.4E6 6293.8E6 1228.773 1225.073 16) T DCPA 17.689 17.271 4986.0E6 5415.7E6 1248.436 1239.068 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.