Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP020618\ Data File : PP023474.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 06 Feb 2018 1:01 Operator : UA/AJ Sample : J1257-03MS Misc : ALS Vial : 22 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 06 02:40:03 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.586 11.366 167.3E6 191.9E6 326.487 316.375m Target Compounds 1) T Dalapon 3.014 2.574 43447838 330.6E6 54.438 399.411m# 2) T 3,5-DICHL... 9.992 9.482 21545517 14149425 27.057m 16.964m# 3) T 4-Nitroph... 11.164 10.529 6762187 26239148 15.727m 56.538m# 5) T DICAMBA 11.905 11.663 69297816 67049913 32.226 29.524m 6) T MCPP 12.266 11.882 32840866 653228 22.399m 0.406m# 7) T MCPA 12.489 12.261 3972940 4707041 1.804m 2.021m 8) T DICHLORPROP 13.090 12.731 3821241 25434296 7.194m 43.322m# 9) T 2,4-D 13.450 13.261 18181000 17459661 27.155 22.742m 10) T Pentachlo... 13.834 13.820 216.2E6 191.3E6 26.593m 22.222m 11) T 2,4,5-TP ... 14.703 14.418 50176465 60993047 15.148 17.049m 12) T 2,4,5-T 15.103 15.052 48963432 225.0E6 15.671 73.023 # 13) T 2,4-DB 15.854 15.644 11794532 8888332 29.998m 20.560m# 14) T DINOSEB 17.317 16.006 8094667 28070748 3.527 11.411 # 15) T Picloram 17.130 17.392 436.7E6 408.1E6 89.689m 81.936m 16) T DCPA 17.686 17.268 297.8E6 368.5E6 75.954 84.686m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.