Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP020618\ Data File : PP023475.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 06 Feb 2018 1:25 Operator : UA/AJ Sample : J1257-03MSD Misc : ALS Vial : 23 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 06 02:43:32 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.586 11.367 166.4E6 195.4E6 324.797 322.253 Target Compounds 1) T Dalapon 3.014 2.578 42754510 328.0E6 53.569 396.227 # 2) T 3,5-DICHL... 9.991 9.482 23624939 13787037 29.668m 16.530m# 3) T 4-Nitroph... 11.165 10.527 6863430 28548399 15.963m 61.514m# 5) T DICAMBA 11.905 11.662 69425644 67325803 32.285 29.645m 6) T MCPP 12.266 11.880 36320428 724884 24.772m 0.451m# 7) T MCPA 12.487 12.269 3577096 5215854 1.624m 2.240m# 8) T DICHLORPROP 13.089 12.730 3481111 27910556 6.553m 47.540m# 9) T 2,4-D 13.450 13.261 17860269 19983497 26.676 26.029m 10) T Pentachlo... 13.834 13.821 210.3E6 188.9E6 25.865 21.946 11) T 2,4,5-TP ... 14.704 14.418 48175733 58846858 14.544 16.449m 12) T 2,4,5-T 15.103 15.052 48893316 222.9E6 15.649 72.351 # 13) T 2,4-DB 15.861 15.645 12258085 7935049 31.177m 18.355m# 14) T DINOSEB 17.316 16.006 7234482 33765158 3.152 13.726 # 15) T Picloram 17.132 17.392 442.2E6 402.2E6 90.832 80.747m 16) T DCPA 17.686 17.268 292.5E6 359.2E6 74.608 82.562m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.