Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP020618\ Data File : PP023486.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 06 Feb 2018 5:53 Operator : UA/AJ Sample : PB106061BS Misc : ALS Vial : 32 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 06 07:26:56 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.585 11.367 326.5E6 385.2E6 637.203 635.180 Target Compounds 1) T Dalapon 3.012 2.576 386.2E6 405.2E6 483.862 489.503 2) T 3,5-DICHL... 9.991 9.484 465.8E6 481.2E6 584.996 576.906 3) T 4-Nitroph... 11.166 10.527 202.9E6 215.8E6 471.869 465.032 5) T DICAMBA 11.904 11.665 1312.5E6 1362.3E6 610.351 599.872 6) T MCPP 12.238 11.869 82959373 87674487 56.581 54.489 7) T MCPA 12.493 12.261 123.8E6 128.2E6 56.203 55.051 8) T DICHLORPROP 13.088 12.776 316.9E6 345.8E6 596.643 589.003 9) T 2,4-D 13.448 13.263 404.5E6 457.3E6 604.235 595.597 10) T Pentachlo... 13.834 13.822 5099.0E6 5368.4E6 627.248 623.542 11) T 2,4,5-TP ... 14.701 14.420 2052.6E6 2211.7E6 619.684 618.219 12) T 2,4,5-T 15.102 15.052 1924.7E6 1837.7E6 616.019 596.553 13) T 2,4-DB 15.848 15.647 235.6E6 255.1E6 599.278 590.145 14) T DINOSEB 17.314 16.046 1364.1E6 1447.9E6 594.348 588.620 15) T Picloram 17.127 17.392 3003.5E6 3051.6E6 616.905 612.628 16) T DCPA 17.682 17.270 2398.2E6 2634.2E6 611.612 605.425 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.