Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP020618\ Data File : PP023493.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 06 Feb 2018 8:43 Operator : UA/AJ Sample : J1253-11MS Misc : ALS Vial : 39 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 06 12:34:37 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.583 11.367 260.1E6 300.4E6 507.555 495.365 Target Compounds 1) T Dalapon 3.014 2.571 56483226 442.4E6 70.771 534.533 # 2) T 3,5-DICHL... 9.991 9.484 58384563 63575813 73.320 76.223 3) T 4-Nitroph... 11.164 10.528 57598010 51119690 133.958 110.148 5) T DICAMBA 11.902 11.662 224.0E6 222.8E6 104.158 98.110m 6) T MCPP 12.263 11.861 40688352 8123732 27.751m 5.049 # 7) T MCPA 12.486 12.251 15057579 12505084 6.836 5.370m 8) T DICHLORPROP 13.087 12.775 47293438 43806281 89.033 74.615 9) T 2,4-D 13.447 13.262 63059075 71541477 94.185 93.186 10) T Pentachlo... 13.832 13.821 429.6E6 433.7E6 52.842 50.375 11) T 2,4,5-TP ... 14.699 14.418 159.5E6 176.9E6 48.154 49.458 12) T 2,4,5-T 15.100 15.051 189.1E6 299.0E6 60.533 97.072 # 13) T 2,4-DB 15.847 15.644 22437383 26154876 57.067m 60.501m 14) T DINOSEB 17.312 16.047 22810596 16709467 9.938 6.793m# 15) T Picloram 17.124 17.392 556.0E6 623.2E6 114.200m 125.121 16) T DCPA 17.681 17.268 317.8E6 416.0E6 81.058 95.603 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.