Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP020618\ Data File : PP023494.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 06 Feb 2018 9:07 Operator : UA/AJ Sample : J1253-11MSD Misc : ALS Vial : 40 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 06 12:39:19 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.583 11.367 259.2E6 298.6E6 505.797 492.479 Target Compounds 1) T Dalapon 3.012 2.570 54084406 452.2E6 67.765 546.273 # 2) T 3,5-DICHL... 9.989 9.483 72336796 62721817 90.841m 75.199 3) T 4-Nitroph... 11.164 10.528 61067073 54077247 142.026 116.521 5) T DICAMBA 11.902 11.662 222.2E6 218.2E6 103.336 96.073m 6) T MCPP 12.260 11.861 105.1E6 8085814 71.681m 5.025 # 7) T MCPA 12.485 12.251 14633122 11613030 6.643 4.987m 8) T DICHLORPROP 13.087 12.774 46690158 40048203 87.898 68.214 9) T 2,4-D 13.446 13.261 62105547 70636226 92.761 92.007 10) T Pentachlo... 13.831 13.818 458.6E6 432.8E6 56.411 50.276m 11) T 2,4,5-TP ... 14.698 14.418 152.7E6 178.0E6 46.104m 49.759 12) T 2,4,5-T 15.100 15.051 188.4E6 308.5E6 60.300 100.148 # 13) T 2,4-DB 15.847 15.643 15533526 23095658 39.508m 53.424m# 14) T DINOSEB 17.311 16.048 20550294 14584151 8.954 5.929m# 15) T Picloram 17.122 17.390 543.9E6 578.9E6 111.714m 116.228m 16) T DCPA 17.680 17.266 319.5E6 417.3E6 81.487 95.905m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.