Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP022718\ Data File : PP023980.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 27 Feb 2018 12:21 Operator : UA/AJ Sample : J1196-05 Misc : ALS Vial : 5 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 28 13:06:30 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.574 11.363 286.7E6 336.6E6 559.484 555.144 Target Compounds 5) T DICAMBA 11.893 11.660 420.9E6 449.6E6 195.723 197.993 9) T 2,4-D 13.435 13.257 392.8E6 405.9E6 586.685 528.644 10) T Pentachlo... 13.825 13.817 5634.2E6 5910.7E6 693.090 686.532 11) T 2,4,5-TP ... 14.689 14.413 2583.7E6 2851.3E6 780.017 796.995 12) T 2,4,5-T 15.088 14.959 1968.4E6 2110.7E6 630.015 685.162m 13) T 2,4-DB 15.831 15.640 235.1E6 264.3E6 597.822 611.482 14) T DINOSEB 17.298 16.040 1251.5E6 1232.7E6 545.259 501.141 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.