Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP022718\ Data File : PP023983.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 27 Feb 2018 14:03 Operator : UA/AJ Sample : J1395-04MS Misc : ALS Vial : 8 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 28 04:17:04 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.574 11.363 202.2E6 225.8E6 394.538 372.387 Target Compounds 1) T Dalapon 3.014 2.582 184.7E6 260.4E6 231.370m 314.616m# 2) T 3,5-DICHL... 9.983 9.481 311.3E6 329.6E6 390.883 395.206 3) T 4-Nitroph... 11.157 10.524 3252742 6311078 7.565m 13.599 # 5) T DICAMBA 11.892 11.659 873.8E6 928.1E6 406.363 408.654 6) T MCPP 12.223 11.861 76174892 59303292 51.954m 36.857 # 7) T MCPA 12.476 12.252 78316448 76250080 35.556m 32.745 8) T DICHLORPROP 13.075 12.769 227.7E6 251.5E6 428.671 428.312m 9) T 2,4-D 13.435 13.257 279.5E6 323.4E6 417.506 421.275 10) T Pentachlo... 13.824 13.817 3233.9E6 3545.8E6 397.821 411.843 11) T 2,4,5-TP ... 14.688 14.412 1342.1E6 1520.5E6 405.178 425.023m 12) T 2,4,5-T 15.086 15.045 1235.3E6 1147.5E6 395.365 372.488 13) T 2,4-DB 15.828 15.640 142.1E6 164.6E6 361.341m 380.675 14) T DINOSEB 17.295 16.039 740.3E6 789.2E6 322.555 320.821 15) T Picloram 17.107 17.385 1605.3E6 1648.3E6 329.712 330.910 16) T DCPA 17.663 17.261 1147.7E6 1328.7E6 292.694 305.375 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.