Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP022718\ Data File : PP024019.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 28 Feb 2018 4:41 Operator : UA/AJ Sample : J1688-06MS Misc : ALS Vial : 38 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 28 06:49:53 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.573 11.363 218.0E6 240.2E6 425.386 396.079 Target Compounds 1) T Dalapon 3.014 2.583 263.2E6 290.7E6 329.797 351.263 2) T 3,5-DICHL... 9.983 9.481 331.3E6 365.9E6 416.089 438.676 3) T 4-Nitroph... 11.154 10.522 5825950 9058590 13.550 19.519 # 5) T DICAMBA 11.891 11.660 948.0E6 1001.2E6 440.847 440.853 6) T MCPP 12.223 11.861 83237567 66566013 56.771m 41.370 # 7) T MCPA 12.477 12.252 77504992 84521743 35.187 36.297 8) T DICHLORPROP 13.074 12.770 256.3E6 269.7E6 482.554 459.390m 9) T 2,4-D 13.434 13.257 304.7E6 354.7E6 455.113 462.007 10) T Pentachlo... 13.823 13.817 3535.5E6 3777.8E6 434.922 438.795 11) T 2,4,5-TP ... 14.687 14.413 1464.1E6 1525.7E6 442.017 426.454 12) T 2,4,5-T 15.086 15.045 1340.0E6 1149.2E6 428.875 373.033 13) T 2,4-DB 15.829 15.638 170.5E6 183.9E6 433.643 425.489m 14) T DINOSEB 17.294 16.038 784.9E6 821.2E6 341.974 333.854m 15) T Picloram 17.106 17.385 1680.5E6 1716.5E6 345.165 344.599 16) T DCPA 17.662 17.261 1263.7E6 1447.6E6 322.281 332.701 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.