Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP022718\ Data File : PP024020.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 28 Feb 2018 5:06 Operator : UA/AJ Sample : J1688-06MSD Misc : ALS Vial : 39 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 28 06:51:47 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.573 11.363 216.5E6 240.8E6 422.492 397.051 Target Compounds 1) T Dalapon 3.015 2.584 260.6E6 289.1E6 326.571 349.225 2) T 3,5-DICHL... 9.983 9.481 329.7E6 365.5E6 414.087 438.266 3) T 4-Nitroph... 11.153 10.521 6264867 10673716 14.570 22.999m# 5) T DICAMBA 11.892 11.660 939.9E6 994.6E6 437.081 437.962 6) T MCPP 12.224 11.861 80805433 67186841 55.112m 41.756 7) T MCPA 12.475 12.253 85686343 82087825 38.902m 35.251 8) T DICHLORPROP 13.073 12.770 240.6E6 242.9E6 452.864m 413.703m 9) T 2,4-D 13.435 13.257 300.7E6 350.9E6 449.182 457.129 10) T Pentachlo... 13.824 13.817 3504.2E6 3755.0E6 431.067 436.150 11) T 2,4,5-TP ... 14.688 14.414 1520.5E6 1504.7E6 459.045 420.587 12) T 2,4,5-T 15.086 15.045 1346.3E6 1134.1E6 430.887 368.160m 13) T 2,4-DB 15.829 15.638 168.9E6 183.2E6 429.589 423.860m 14) T DINOSEB 17.295 16.040 780.5E6 830.4E6 340.041 337.566 15) T Picloram 17.107 17.385 1674.3E6 1705.4E6 343.898 342.372 16) T DCPA 17.663 17.262 1251.1E6 1433.4E6 319.069 329.445 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.