Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP022718\ Data File : PP024023.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 28 Feb 2018 6:19 Operator : UA/AJ Sample : J1654-01MS Misc : ALS Vial : 42 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 28 12:10:19 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.573 11.363 45867320 51697316 89.502 85.250 Target Compounds 1) T Dalapon 3.015 2.582 45861313 33099628 57.462 39.990 # 2) T 3,5-DICHL... 9.983 9.481 57411212 70884506 72.097 84.985 3) T 4-Nitroph... 11.155 10.526 24673497 27755817 57.384m 59.806 5) T DICAMBA 11.891 11.660 164.6E6 169.6E6 76.533 74.697 6) T MCPP 12.255 11.857 9979865 8327323 6.807m 5.175 7) T MCPA 12.472 12.246 12906706 11183655 5.860m 4.803m 8) T DICHLORPROP 13.075 12.770 41384108 42551661 77.909 72.478m 9) T 2,4-D 13.435 13.257 56600531 52494615 84.539 68.377 10) T Pentachlo... 13.823 13.816 592.4E6 656.9E6 72.875 76.303 11) T 2,4,5-TP ... 14.687 14.413 217.1E6 248.6E6 65.534 69.490 12) T 2,4,5-T 15.084 15.045 214.7E6 151.1E6 68.730m 49.035 # 13) T 2,4-DB 15.828 15.638 24692492 36575577 62.802m 84.605m# 14) T DINOSEB 17.295 16.040 50729681 39458030 22.103 16.041 # 15) T Picloram 17.107 17.385 333.2E6 349.8E6 68.433 70.225 16) T DCPA 17.661 17.261 206.5E6 281.5E6 52.664m 64.707 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.