Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP022718\ Data File : PP024024.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 28 Feb 2018 6:43 Operator : UA/AJ Sample : J1654-01MSD Misc : ALS Vial : 43 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 28 12:12:09 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.573 11.363 45994026 51497348 89.749 84.921 Target Compounds 1) T Dalapon 3.014 2.582 46181488 32933207 57.863 39.789 # 2) T 3,5-DICHL... 9.983 9.481 56989648 70694308 71.568 84.757 3) T 4-Nitroph... 11.157 10.526 26292792 27224129 61.150 58.660 5) T DICAMBA 11.892 11.661 164.2E6 168.8E6 76.368 74.322 6) T MCPP 12.256 11.857 6940034 8364572 4.733 5.199 7) T MCPA 12.474 12.246 12324578 11081091 5.595 4.759m 8) T DICHLORPROP 13.075 12.770 41082741 45230745 77.341 77.041m 9) T 2,4-D 13.434 13.256 54310600 57676698 81.118 75.127m 10) T Pentachlo... 13.823 13.817 590.1E6 652.1E6 72.586 75.740 11) T 2,4,5-TP ... 14.687 14.413 223.6E6 247.7E6 67.489 69.232 12) T 2,4,5-T 15.085 15.046 204.4E6 152.5E6 65.431m 49.497 13) T 2,4-DB 15.828 15.639 24011894 34942239 61.071m 80.827m# 14) T DINOSEB 17.294 16.040 45217821 39430089 19.701 16.029 15) T Picloram 17.107 17.383 326.1E6 326.1E6 66.983 65.468m 16) T DCPA 17.661 17.259 206.8E6 255.2E6 52.738m 58.663m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.